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Search for "co-condensation" in Full Text gives 8 result(s) in Beilstein Journal of Nanotechnology.

Antimicrobial metal-based nanoparticles: a review on their synthesis, types and antimicrobial action

  • Matías Guerrero Correa,
  • Fernanda B. Martínez,
  • Cristian Patiño Vidal,
  • Camilo Streitt,
  • Juan Escrig and
  • Carol Lopez de Dicastillo

Beilstein J. Nanotechnol. 2020, 11, 1450–1469, doi:10.3762/bjnano.11.129

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  • -wrapped Ag nanowires using the chemical vapor deposition method in order to investigate their broad-spectrum and robust antimicrobial properties. The cryochemical synthesis method includes a simultaneous evaporation of a metallic and a volatile component (e.g., an organic monomer), followed by co
  • -condensation of the vapors on the cold surface of the vacuum reactor. Sergeev et al. [45] obtained Ag nanoparticles with sizes ranging from 20 to 150 nm using this technique. The electrochemical anodization method is based on the reactions that occur between the electrode and the electrolyte. In this method
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Published 25 Sep 2020

Highly ordered mesoporous silica film nanocomposites containing gold nanoparticles for the catalytic reduction of 4-nitrophenol

  • Mohamad Azani Jalani,
  • Leny Yuliati,
  • Siew Ling Lee and
  • Hendrik O. Lintang

Beilstein J. Nanotechnol. 2019, 10, 1368–1379, doi:10.3762/bjnano.10.135

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  • from gold(III) chloride trihydrate (HAuCl4) solution have been used as a precursor for post-synthetic grafting upon mixing with mesoporous silica [20]. Another method is to utilize the co-condensation reaction by the mixing solution of HAuCl4 with surfactants and silica sources during the sol–gel
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Published 05 Jul 2019

Surface roughness rather than surface chemistry essentially affects insect adhesion

  • Matt W. England,
  • Tomoya Sato,
  • Makoto Yagihashi,
  • Atsushi Hozumi,
  • Stanislav N. Gorb and
  • Elena V. Gorb

Beilstein J. Nanotechnol. 2016, 7, 1471–1479, doi:10.3762/bjnano.7.139

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  • and co-condensation [10]. Briefly, precursor solutions were prepared by mixing C10 and TMOS in an ethanol/hydrochloric acid solution for 24 h at room temperature (25 ± 2 °C). The typical molar ratio of the precursor solution was 0.73 C10:2.92 TMOS:32 EtOH:14 H2O:7.7 × 10−3 HCl. The precursor solution
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Published 18 Oct 2016

The surface properties of nanoparticles determine the agglomeration state and the size of the particles under physiological conditions

  • Christoph Bantz,
  • Olga Koshkina,
  • Thomas Lang,
  • Hans-Joachim Galla,
  • C. James Kirkpatrick,
  • Roland H. Stauber and
  • Michael Maskos

Beilstein J. Nanotechnol. 2014, 5, 1774–1786, doi:10.3762/bjnano.5.188

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  • (organosiloxane) nanoparticles: Poly(organosiloxane) NPs are synthesized in an aqueous dispersion by co-condensation of mixtures of dialkyldialkoxysilanes and alkyltrialkoxysilanes in the presence of a surfactant. By sequential addition of mixtures with different ratios of bi- to tri-functional monomers
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Published 15 Oct 2014

Distribution of functional groups in periodic mesoporous organosilica materials studied by small-angle neutron scattering with in situ adsorption of nitrogen

  • Monir Sharifi,
  • Dirk Wallacher and
  • Michael Wark

Beilstein J. Nanotechnol. 2012, 3, 428–437, doi:10.3762/bjnano.3.49

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  • ; SANS; surface functionalization; Introduction Regarding functionalization with organic groups, Si-MCM-41 often suffers from pore blocking at the pore mouths and inhomogeneous distribution of the functional groups in the case of post-synthetic grafting [1][2][3] or, if the co-condensation route is
  • inhomogeneous distribution of the groups in the pores, resulting still in strong contrast matching. Samples functionalized by co-condensation, however, exhibited almost no contrast matching, proving a very homogeneous distribution of the SO3H-groups along the channels and explaining the observed higher proton
  • SO3H/H2SO4 solution used for the functionalization first spreads uniformly in the whole pore network before significant reaction at the benzene rings in the walls takes place. Analogous results were found for homogeneously SO3H-modified Si-MCM-41 (co-condensation route) by SANS measurements with in
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Published 30 May 2012

Inorganic–organic hybrid materials through post-synthesis modification: Impact of the treatment with azides on the mesopore structure

  • Miriam Keppeler,
  • Jürgen Holzbock,
  • Johanna Akbarzadeh,
  • Herwig Peterlik and
  • Nicola Hüsing

Beilstein J. Nanotechnol. 2011, 2, 486–498, doi:10.3762/bjnano.2.52

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  • Salzburg, Hellbrunner Str. 34, A-5020 Salzburg, Austria 10.3762/bjnano.2.52 Abstract Hybrid, hierarchically organized, monolithic silica gels, comprising periodically arranged mesopores and a cellular macroscopic network, have been prepared through a co-condensation reaction of tetrakis(2-hydroxyethyl
  • even functional groups such as polymerizable moieties or metal-coordinating groups can be introduced [24]. These groups are typically incorporated either by post-synthetic grafting processes or by co-condensation reactions of different alkoxysilanes. The impact of these synthesis steps on the final
  • second step. For this approach, it is assumed that structural changes are minimal [25]. For the co-condensation approach, in which tetraalkoxysilanes [Si(OR)4] are condensed to form an inorganic network in the presence of organically substituted tri-alkoxysilanes [R'–Si(OR)3], network formation and thus
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Published 26 Aug 2011

Novel acridone-modified MCM-41 type silica: Synthesis, characterization and fluorescence tuning

  • Maximilian Hemgesberg,
  • Gunder Dörr,
  • Yvonne Schmitt,
  • Andreas Seifert,
  • Zhou Zhou,
  • Robin Klupp Taylor,
  • Sarah Bay,
  • Stefan Ernst,
  • Markus Gerhards,
  • Thomas J. J. Müller and
  • Werner R. Thiel

Beilstein J. Nanotechnol. 2011, 2, 284–292, doi:10.3762/bjnano.2.33

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  • been successfully prepared by co-condensation of an appropriate organic precursor with tetraethyl orthosilicate (TEOS) under alkaline sol–gel conditions. The resulting material was fully characterized by means of X-ray diffraction (XRD), N2-adsorption–desorption, transmission electron microscopy (TEM
  • scandium triflate, which makes the material a good candidate for solid state sensors and optics. The successful synthesis of highly ordered MCM materials through co-condensation was found to be dependent on the chemical interaction of the different precursors. Keywords: acridone; co-condensation
  • functionalized either by in situ post-sol–gel modification or by direct co-condensation of different types of organic precursors [3]. The latter method often leads to a more homogeneous distribution of the desired functionalization within the material. It also provides the possibility to characterize application
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Published 09 Jun 2011

On the reticular construction concept of covalent organic frameworks

  • Binit Lukose,
  • Agnieszka Kuc,
  • Johannes Frenzel and
  • Thomas Heine

Beilstein J. Nanotechnol. 2010, 1, 60–70, doi:10.3762/bjnano.1.8

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  • and the corresponding linkers. This process requires a release of three or six water molecules in case of t or l topology, respectively. Co-condensation of the above molecular units with compounds such as 2,3,6,7,10,11-hexahydroxytriphenylene (HHTP), hexahydroxybenzene (HHB) and dodecahydroxycoronene
  • (DHC) (Figure 5) gives rise to COFs made of connectors II, III and IV, respectively, and the corresponding linkers. Self-condensation of tetrahydroxydiborane (THDB) and co-condensation of HHB with THDB result in the formation of the reference structures, REF-I and REF-III, respectively. In relation to
  • the corresponding connector/linker topologies, these building blocks satisfy the following equations of the co-condensation reaction for COF formation: with a stochiometry appropriate for one unit cell. The number of covalent bonds formed between the building blocks is equivalent to the number of
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Published 22 Nov 2010
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