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3 article(s) from Caporaso, Marina

Efficient mechanochemical synthesis of regioselective persubstituted cyclodextrins

Laszlo Jicsinszky,
Marina Caporaso,
Katia Martina,
Emanuela Calcio Gaudino and
Giancarlo Cravotto

Full Research Paper
Published 10 Nov 2016

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1. Graphical Abstract
2. Scheme 1: Synthesis of per-6-derivatized CDs. Ball milling conditions: 1500 steel balls of 1 mm diameter and ...
  
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Graphical Abstract

Beilstein J. Org. Chem. 2016, 12, 2364–2371, doi:10.3762/bjoc.12.230

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Enabling technologies and green processes in cyclodextrin chemistry

Giancarlo Cravotto,
Marina Caporaso,
Laszlo Jicsinszky and
Katia Martina

Review
Published 15 Feb 2016

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1. Graphical Abstract
2. Figure 1: (a) Multihorn-flow US reactor, (b) Cavitational turbine, (c) Pilot-scale BM, (d) High-pressure MW r...
  
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3. Figure 2: Trends in CD papers and CD use in green chemical processes.
  
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4. Figure 3: Distribution of energy efficient methods in CD publications.
  
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5. Figure 4: Document type dealing with CD chemistry under non-conventional techniques (conference proceedings a...
  
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6. Figure 5: Document type dealing with sustainable technologies in CD publications.
  
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7. Scheme 1: Synthesis of 6^I-(p-toluenesulfonyl)-β-CD.
  
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8. Scheme 2: Example of CuAAC with 6^I-azido-6^I-deoxy-β-CD and phenylacetylene.
  
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9. Scheme 3: Synthesis of 6^I-benzylureido-6^I-deoxy-per-O-acetyl-β-CD.
  
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10. Scheme 4: Synthesis of 3^I-azido-3^I-deoxy-altro-α, β- and γ-CD.
  
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11. Scheme 5: Synthesis of 2-2’ bridged bis(β-CDs). Reaction conditions: 1) TBDMSCl, imidazole, dry pyridine, sti...
  
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12. Scheme 6: Insoluble reticulated CD polymer.
  
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13. Scheme 7: CD-HDI cross linked polymers.
  
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14. Scheme 8: Derivatization of 6^I-(p-toluenesulfonyl)-β-CD by tosyl displacement.
  
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15. Scheme 9: Synthetic scheme for the preparation of heptakis(6-amino-6-deoxy)-β-CD, heptakis(6-deoxy-6-ureido)-...
  
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16. Scheme 10: Structure of CD derivatives obtained via MW-assisted CuAAC.
  
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17. Scheme 11: Preparation of SWCN CD-DOTA carrier.
  
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Graphical Abstract

Beilstein J. Org. Chem. 2016, 12, 278–294, doi:10.3762/bjoc.12.30

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Pd/C-catalyzed aerobic oxidative esteriﬁcation of alcohols and aldehydes: a highly efficient microwave-assisted green protocol

Marina Caporaso,
Giancarlo Cravotto,
Spyros Georgakopoulos,
George Heropoulos,
Katia Martina and
Silvia Tagliapietra

Full Research Paper
Published 26 Jun 2014

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1. Graphical Abstract
2. Scheme 1: Reaction pathway of aerobic oxidative esteriﬁcation of alcohols.
  
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3. Figure 1: Screening of different catalysts and bases in the catalytic oxidative esterification of benzylalcoh...
  
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4. Scheme 2: Catalyst regeneration and oxidative esterification of benzaldehyde (2^nd cycle).
  
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Beilstein J. Org. Chem. 2014, 10, 1454–1461, doi:10.3762/bjoc.10.149

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