2 article(s) from Friščić, Tomislav
Graphical Abstract
Scheme 1: Milling synthesis of 2,3-diphenylquinoxaline from benzil and ortho-phenylenediamine [40].
Scheme 2: Movement of the milling jar and sample holder under milling conditions.
Figure 1: Time-resolved Raman spectrum for the double condensation of o-phenylenediamine and benzil to form 2...
Figure 2: Section of the time-resolved Raman spectrum for the model mechanochemical reaction conducted at 30 ...
Figure 3: (Left) Estimated contribution of each component for each Raman spectrum over time of the synthesis ...
Figure 4: The effect of milling frequency on the milling condensation of benzil and o-phenylenediamine to for...
Figure 5: The reproducibility of varying milling frequency on the neat mechanochemical condensation of benzil...
Figure 6: The effect of milling frequency on the internal jar temperature measured immediately after reaction...
Graphical Abstract
Scheme 1: Developed syntheses for accessing by mechanochemistry: (a) mPEG–OTs, (b) mPEG–Br, (c) mPEG–SH, (d) ...
Figure 1: 1H NMR of sample mPEG2000–OTs (Table 1, entry 5) in CDCl3 showing mPEG end group shift after tosylation.