5 article(s) from Yusubov, Mekhman S.
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- Published 27 Sep 2019
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Figure 1: General structure of aryl-λ3-iodanes.
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Figure 2: Tpeak and ΔHdec-values for a range of N- and O-substituted iodanes.
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Figure 3: TGA/DSC curves of (a) benziodoxolone 1, (b) triazole 2 and (c) pyrazole 6.
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Figure 4: Decomposition enthalpy (ΔHdec) scale for pseudocyclic tosylates 1–15 and cyclic iodoso species 16 a...
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Figure 5: Correlation between the relative reactivity for pseudocyclic NHIs based on the reaction time in the...
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Figure 6: Tpeak and ΔHdec values for a range of N- and O-substituted iodanes.
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Figure 7: Decomposition enthalpy (ΔHdec) scale for (pseudo)cyclic mesitylen(phenyl)- λ3-iodanes 18–33.
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Figure 8: TGA/DSC curves for the benzimidazole based diaryliodonium salt 25.
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Figure 9: TGA/DSC curves for the cyclic triazole 32.
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Scheme 1: The thermal decomposition of (pseudo)cyclic N-heterocycle-stabilized mesityl(aryl)-λ3-iodanes 25 an...
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- Published 20 Jul 2018
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Scheme 1: Previously reported preparation of IBS (1) [17].
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Scheme 2: Oxidation of 2-iodobenzenesulfonate 5 by Oxone in water.
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Figure 1: X-ray structure of an independent crystal unit of IBS 6-K.
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Figure 2: Simplified representation of structure 6-K. Selected interatomic distances (Å): I(1)=O(1) 1.79; I(1...
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Scheme 3: Comparison of the oxidation of sodium 2-iodobenzenesulfonate (5) with NaIO4 and 2-iodobenzenesulfon...
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- Full Research Paper
- Published 08 May 2018
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Scheme 1: Representative examples of benziodoxoles and benziodazoles.
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Scheme 2: Preparation of bicyclic benziodazole 7a.
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Figure 1: X-ray crystal structure of compound 7a. Ellipsoids are drawn to the 50% probability level. Selected...
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Scheme 3: Benziodadiazole 7a mediated oxidatively assisted esterification and amidation reactions.
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- Full Research Paper
- Published 12 Apr 2018
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- Published 04 Jun 2007
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Figure 1: Hypervalent iodine reagents 1 – 6.
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Scheme 1: Iodine(III)-promoted iodination of arenes and concept of purification.
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Scheme 2: Proposed intermediates.
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