Facile chemical routes to mesoporous silver substrates for SERS analysis

Elina A. Tastekova, Alexander Y. Polyakov, Anastasia E. Goldt, Alexander V. Sidorov, Alexandra A. Oshmyanskaya, Irina V. Sukhorukova, Dmitry V. Shtansky, Wolgang Grünert and Anastasia V. Grigorieva

Beilstein J. Nanotechnol. 2018, 9, 880–889. doi:10.3762/bjnano.9.82

Supporting Information

Experimental details.

Supporting Information File 1: Details:
1. Micrographs of the products obtained in different reagent ratios.
2. Micrographs of the reduction products obtained using H2O2 and N2H6SO4 instead of NaBH4.
3. Nitrogen adsorption plot for the Ag mesoporous nanocube sample synthesized with the molar ratio of 1:4 Ag2O/NaBH4.
4. XRD data for a bare Ag2O film and mesoporous Ag film synthesized with the molar ratio of 1:10 Ag2O/NaBH4 in 15 min reduction processing.
5. Experimental details on the wettability contact angle measurements.
6. XPS survey spectra for mesoporous aggregates.
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Picture with graphical abstract, title and authors for social media postings and presentations.

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