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1 article(s) from Krysiak, Yasar

Stereodiscrimination of guests in chiral organosilica aerogels studied by ESR spectroscopy

Sebastian Polarz,
Yasar Krysiak,
Martin Wessig and
Florian Kuhlmann

Beilstein J. Nanotechnol. 2025, 16, 2034–2054, doi:10.3762/bjnano.16.140

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Figure 1: Genealogy of the Materials used in the current study. Achiral materials as references (grey); mater...

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Scheme 1: Synthesis route to AlaNH₁₀oSil.

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Figure 2: Characterization of AlaNH₁₀oSIL. (a) SEM micrograph (scale bar = 1 μm). (b) N₂ physisorption isothe...

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Scheme 2: Synthesis route towards organosilica aerogels containing neighboring groups and chiral functionalit...

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Figure 3: cw-ESR spectra of (+)-3CP (black) and (−)-3CP (blue) dissolved in ethanol and infiltrated into achi...

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Figure 4: cw-ESR spectra of (+)-3CP (blue) and (−)-3CP (red) dissolved in ethanol and confined in SerNH₁₀oSIL...

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Figure 5: cw-ESR spectra of (+)-3CP (blue) and (−)-3CP (red) confined in SerNH₁₀SIL recorded at T = 213 K (da...

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Figure 6: (a) cw-ESR spectra of (+)-3CP (blue) and (−)-3CP (red) confined in AlaNH₁₀oSIL recorded at T = 223 ...

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Figure 7: (a) SEM micrograph of a single porous particle of the commercial Chiralpak IG-3 material; scale bar...

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Figure 8: HPLC chromatograms using Chiralpak IG-3 as a stationary phase of (+)-3CP (blue) and (−)-3CP (red) u...

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Figure 9: (a) Enlargement of the region of the ESR spectra of the spin probes dissolved in the ethanol/ penta...

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Figure 10: cw-ESR spectra recorded at different temperatures for SH-FmocAlaNH₁₀oSIL (a) and SH-AlaNH₁₀oSIL (b)...

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Figure 11: Temperature dependency of χ_ads (a) and selectivity factor (b) of (+)-3CP (blue) and (−)-3CP (red) i...

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Figure 12: Organosilica materials containing a spin probe attached to the surfaces.

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Figure 13: (a) ESR spectra recorded at T = 103 K for TEMPONH_xSIL with x = 0.01 (black), 0.02 (red), 0.05 (blue...

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Published 13 Nov 2025

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