Beilstein J. Nanotechnol.2012,3, 360–367, doi:10.3762/bjnano.3.42
achieved, acetylene gas (200 sccm) is inserted through a nozzle in the chamber under an Ar atmosphere.
SEM image of the MWCNTs after growth on a stainless-steel substrate. The MWCNTs are randomly oriented, and no traces of other carbonaceous materials were detected in the large scanned area.
(a) Low
-resolution TEM image assessing the multiwalled nature of the carbon nanotubes synthesized on SS. (b) High-resolution TEM picture of a single MWCNT with 19 walls. The inset displays the Fast Fourier Transform of the TEM image reported in (b). The two spots, at a semidistance of 0.35 nm, represent the parallel
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Figure 1:
(a) Photograph of the chemical vapour deposition chamber used to synthesize MWCNTs. The reactor com...
Beilstein J. Nanotechnol.2010,1, 14–20, doi:10.3762/bjnano.1.3
using microwave irradiation.
Results and Discussion
The ZnO nanoparticles obtained through the sol–gel synthesis (see section Experimental) are shown in Figure 1a and Figure 1b as transmission electron microscopy (TEM) micrographs. The low-resolution TEM micrograph exhibits spherical nanoparticles with
the concentration after photoirradiation.
(a) Low-resolution TEM micrograph of ZnO nanoparticles, (b) electron diffraction pattern of the ZnO nanoparticles, (c) high-resolution TEM micrograph of a ZnO nanoparticle showing the lattice fringes, (d) low-resolution TEM micrograph of ZnO nanorods, and (e
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Figure 1:
(a) Low-resolution TEM micrograph of ZnO nanoparticles, (b) electron diffraction pattern of the ZnO...