Beilstein J. Nanotechnol.2011,2, 638–644, doi:10.3762/bjnano.2.67
usually the inverse miniemulsion technique has to be applied. Here, water soluble precursor compounds (e.g., Ti- or Si-glycolates, Zr or Ce-salts) for sol–gelsynthesis and, if desired, templating surfactants, such as CTAB, are dissolved in water, acting as the dispersed phase. After miniemulsification
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Figure 1:
Scheme of the synthesis of CeO2/Si(O)C core–shell nanoparticles via miniemulsion technique.
Beilstein J. Nanotechnol.2010,1, 14–20, doi:10.3762/bjnano.1.3
using microwave irradiation.
Results and Discussion
The ZnO nanoparticles obtained through the sol–gelsynthesis (see section Experimental) are shown in Figure 1a and Figure 1b as transmission electron microscopy (TEM) micrographs. The low-resolution TEM micrograph exhibits spherical nanoparticles with
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Figure 1:
(a) Low-resolution TEM micrograph of ZnO nanoparticles, (b) electron diffraction pattern of the ZnO...