Integration of enabling methods for the automated flow preparation of piperazine-2-carboxamide

Richard J. Ingham, Claudio Battilocchio, Joel M. Hawkins and Steven V. Ley

Beilstein J. Org. Chem. 2014, 10, 641–652. doi:10.3762/bjoc.10.56

Supporting Information

Supporting Information File 1: Experimental data.
Format: PDF Size: 1.2 MB Download
Supporting Information File 2: Control sequence for extended period hydrolysis experiment with monitoring. Alternate web version: http://gist.github.com/richardingham/0a58a291bad2e3b9009f
Format: TXT Size: 4.3 KB Download
Supporting Information File 3: Control sequence for performing DoE experiments. Alternate web version: http://gist.github.com/richardingham/83401127622036c6afd0
Format: TXT Size: 4.2 KB Download
Supporting Information File 4: Control sequence for performing DoE experiments using intermediate from a reservoir. Alternate web version: http://gist.github.com/richardingham/f2117b9dc7504d6e1942
Format: TXT Size: 10.1 KB Download
Supporting Information File 5: Flow chart representation of the control sequence for performing DoE experiments using intermediate from a reservoir.
Format: PNG Size: 138.3 KB Download
Supporting Information File 6: Control sequence for performing two-step hydrogenation process with control and monitoring. Alternate web version: http://gist.github.com/richardingham/31f6f8efa47771c2ed02
Format: TXT Size: 5.6 KB Download
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