2 article(s) from Eguaogie, Olga
Examples of equipment used to perform mechanochemistry on nucleoside and nucleotide substrates (not...
Jump to Figure 1
Jump to Figure 2
Nucleoside tritylation effected by hand grinding in a heated mortar and pestle.
Jump to Scheme 1
Persilylation of ribonucleoside hydroxy groups (and in situ acylation of cytidine) in a MBM.
Jump to Scheme 2
Nucleoside amine and carboxylic acid Boc protection using an improvised attritor-type mill.
Jump to Scheme 3
Nucleobase Boc protection via transient silylation using an improvised attritor-type mill.
Jump to Scheme 4
Chemoselective N-acylation of an aminonucleoside using LAG in a MBM.
Jump to Scheme 5
Azide–alkyne cycloaddition reactions performed in a copper vessel in a MBM.
Jump to Scheme 6
a) Custom-machined copper vessel and zirconia balls used to perform CuAAC reactions (showing: upper...
Jump to Figure 3
Thiolate displacement reactions of nucleoside derivatives in a MBM.
Jump to Scheme 7
Selenocyanate displacement reactions of nucleoside derivatives in a MBM.
Jump to Scheme 8
Nucleobase glycosidation reactions and subsequent deacetylation performed in a MBM.
Jump to Scheme 9
Regioselective phosphorylation of nicotinamide riboside in a MBM.
Jump to Scheme 10
Preparation of nucleoside phosphoramidites in a MBM using ionic liquid-stabilised chlorophosphorami...
Jump to Scheme 11
Preparation of a nucleoside phosphite triester using LAG in a MBM.
Jump to Scheme 12
Internucleoside phosphate coupling linkages in a MBM.
Jump to Scheme 13
Preparation of ADPR analogues using in a MBM.
Jump to Scheme 14
Synthesis of pyrophosphorothiolate-linked dinucleoside cap analogues in a MBM to effect hydrolytic ...
Jump to Scheme 15
Early low temperature mechanised ball mill as described by Mudd et al. – adapted from reference .
Jump to Figure 4
Co-crystal grinding of alkylated nucleobases in an amalgam mill (N.B. no frequency was recorded in ...
Jump to Scheme 16
Materials used to prepare a smectic phase.
Jump to Figure 5
Structures of 5-fluorouracil (5FU) and nucleoside analogue prodrugs subject to mechanochemical co-c...
Jump to Figure 6
Preparation of DNA-SWNT complex in a MBM.
Jump to Scheme 17
Beilstein J. Org. Chem. 2018, 14, 955–970, doi:10.3762/bjoc.14.81
Model reactions of 5′-chloro-5′-deoxyadenosine (1a) with 4-methoxybenzylthiolate salts used to opti...
Thiolate displacement reactions of 5′-derivatised nucleosides using VBM.
Selenocyanate displacement reactions of 5′-derivatised nucleosides using liquid-assisted grinding (...
Beilstein J. Org. Chem. 2017, 13, 87–92, doi:10.3762/bjoc.13.11
Subscribe to our Latest Articles RSS Feed.
Register and get informed about new articles.
Follow the Beilstein-Institut