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Beilstein J. Org. Chem. 2026, 22, 175–184, doi:10.3762/bjoc.22.11
Graphical Abstract
Figure 1: Synthesis of 25CN-NBOH·HCl (1·HCl). a) 2C-CN is available in 4 steps from 2C-H [12]: 1) TFAA, TEA, DCM;...
Figure 2: a) Single-crystal X-ray structure of 1·HCl. Displacement ellipsoids of the nonhydrogen atoms are sh...
Figure 3: SCXRD and XRPD spectra of different preparations of 1·HCl. Blue: SCXRD spectrum of 1·HCl. Red, gree...
Figure 4: TGA and DSC thermograms of 1·HCl.
Figure 5: Calculated pH-dependent species distribution curves for 25CN-NBOH (1).
Figure 6: a) Structure of the truncated model compound used for DFT calculations, with explicit water molecul...