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Beilstein J. Org. Chem. 2012, 8, 1191–1199, doi:10.3762/bjoc.8.132
Graphical Abstract
Scheme 1: Diverse synthesis of indoles using Bartoli reactions. aSee [24].
Figure 1: Nitroarenes on solid supports. In red: Nitroarenes failed to give indoles. aResin has been reported...
Figure 2: Temperature optimization with Grignard reagent 2{b}.
Figure 3: Temperature optimization with Grignard reagent 2{a}. Isolated yield.
Figure 4: Optimization studies of ester 1{h} with a Grignard reagent 2{d} to give indole 3{h,d} and methyl 3-...
Scheme 2: Stille reaction on solid supports.
Scheme 3: Suzuki reaction on solid supports.
Scheme 4: Sonogashira–Hagihara reaction on solid supports.