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Beilstein J. Org. Chem. 2017, 13, 779–792, doi:10.3762/bjoc.13.77
Ring opening of L-LA in the presence of cyclodextrins.
(a) ELSD chromatogram of crude β-CD-LA reaction mixture and (b) MALDI–MS spectrum of fraction f5.
MALDI–MS spectra of the fractionated α-, β- and γ-CD-LA products – fractions precipitated in THF: (...
MALDI–MS spectra of the fractionated α-, β- and γ-CD-LA products – fractions soluble in THF: (a) α-...
1H NMR spectrum of fractions precipitated in THF of (A) α-CD-LA, (B) β-CD-LA and (C) γ-CD-LA.
13C NMR spectra of (A) β-CD-LA F2 fraction and (B) β-CD-LA F1 fraction.
DEPT135-NMR experiment of (A) β-CD-LA F2 fraction and (B) β-CD-LA F1 fraction.