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1 article(s) from Plasse, Kelsey

High-pressure activation for the solvent- and catalyst-free syntheses of heterocycles, pharmaceuticals and esters

Kelsey Plasse,
Valerie Wright,
Guoshu Xie,
R. Bernadett Vlocskó,
Alexander Lazarev and
Béla Török

Beilstein J. Org. Chem. 2025, 21, 1374–1387, doi:10.3762/bjoc.21.102

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Figure 1: Simplified schematic rendering of a high hydrostatic pressure reactor.

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Scheme 1: High pressure-initiated synthesis of 1,3-dihydrobenzimidazoles 3a–d. The yields are GC yields and t...

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Figure 2: Illustration of the cyclization reaction between chalcone (4) and 3-(trifluoromethyl)phenylhydrazin...

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Scheme 2: High pressure-initiated catalyst- and solvent-free synthesis of pyrazoles 6a–c from chalcone (4) an...

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Figure 3: Schematic representation of the cycling experiments: the major variables are the applied pressure, ...

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Scheme 3: High pressure-initiated synthesis of the active pharmaceutical ingredients in Tylenol® and Aspirin®...

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Scheme 4: High pressure-initiated esterification of alcohols 12a–g in a catalyst- and additional solvent-free...

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Scheme 5: High pressure-initiated large scale syntheses of N-aryl- and N-alkylpyrroles at about 100 g scale.

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Published 02 Jul 2025

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