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1 article(s) from Plunkett, Kyle N

Supramolecular assembly of hypervalent iodine macrocycles and alkali metals

Krishna Pandey,
Lucas X. Orton,
Grayson Venus,
Waseem A. Hussain,
Toby Woods,
Lichang Wang and
Kyle N. Plunkett

Beilstein J. Org. Chem. 2025, 21, 1095–1103, doi:10.3762/bjoc.21.87

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Graphical Abstract

Figure 1: (A) Our previous work: Assembly and disassembly of phenylalanine hypervalent iodine macrocycles (Ph...

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Figure 2: Two conformations of the HIM were found. One conformation projected all three benzyl groups in a ve...

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Figure 3: A) Chemical structure of HIM 1: Three iodine atoms and three inward projected ester carbonyls curcu...

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Figure 4: ¹H NMR titration experiment of 1 with LiBArF₂₀ at an incremental equivalency in CDCl₃ and (CD₃)₂CO ...

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Figure 5: Crystal structures of HIM 1 and LiBArF₂₀ (A) and NaBArF₂₄ (B). BARF cation is omitted for clarity. ...

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Figure 6: Alternative view of the crystal structure of the HIM 1 and LiBArF₂₀ complex. BArF₂₀ anion is omitte...

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Figure 7: Isotherms of 1 titrated with NaBArF₂₄ orLiBArF₂₀. The solid lines are the predicted model fits for ...

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Figure 8: Lithium complex 2 (red) overlaid with lithium complex 3 (blue). In lithium complex 2, one benzyl ri...

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Published 30 May 2025

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