2 article(s) from Podlech, Joachim
- Full Research Paper
- Published 22 Jan 2021
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Scheme 1: Biphenyl-derived mycotoxins.
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Scheme 2: Synthesis of arylboronates 6. Conditions: a) TBSCl, DMAP, imidazole, DMF, 50 °C, 4 h (96%); b) NBS,...
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Scheme 3: Synthesis of aryl bromides 9. Conditions: f) BBr3, −78 °C to rt, 18 h (71%); g) R = TBS: TBSCl, DMA...
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Scheme 4: Final steps in the synthesis of biaryl 1. Conditions: h) Pd(OAc)2, SPhos, Cs2CO3, dioxane/H2O 7:1, ...
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- Full Research Paper
- Published 02 Aug 2013
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Scheme 1: Imidate hydrochloride synthesis discovered by Pinner and Klein [1,2].
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Scheme 2: Mechanism of the Pinner reaction.
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Scheme 3: Transformations of imidate hydrochlorides.
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Scheme 4: Reaction used for optimizations.
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Scheme 5: Plausible mechanism of the Lewis acid-promoted Pinner reaction.
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Scheme 6: Synthesis of monaspilosin.
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Scheme 7: Proposed mechanism of the trimethylsilyl triflate-promoted Ritter reaction.
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