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1 article(s) from Wu, Jian-Li

Recent advances in amidyl radical-mediated photocatalytic direct intermolecular hydrogen atom transfer

Hao-Sen Wang,
Lin Li,
Xin Chen,
Jian-Li Wu,
Kai Sun,
Xiao-Lan Chen,
Ling-Bo Qu and
Bing Yu

Beilstein J. Org. Chem. 2025, 21, 1306–1323, doi:10.3762/bjoc.21.100

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Graphical Abstract

Figure 1: (a) BDE of C–H. (b) Direct functionalization of C–H catalyzed by transition-metal. (c) Direct funct...

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Figure 2: (a) Amidyl radical-enabled hydrogen atom transfer. (b) Substituent effects to amidyl radical proper...

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Figure 3: Representative photocatalysts discussed in this review.

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Scheme 1: Alkylation of C(sp³)–H catalyzed by amidyl radical under visible light.

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Scheme 2: Direct heteroarylation of C(sp³)–H catalyzed by amidyl radical under visible light.

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Scheme 3: Alkylation of C(sp³)–H catalyzed by amidyl radical and metal-free photocatalyst under visible light....

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Scheme 4: Alkylation of C(sp³)–H, Si–H, and Ge–H catalyzed by amidyl radical under visible light.

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Scheme 5: Direct heteroarylation of C(sp³)–H catalyzed by synergistic promotion of amidyl radical and photoca...

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Scheme 6: Direct B–H functionalization of icosahedral carboranes catalyzed by amidyl radical under visible li...

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Scheme 7: Nucleophilic amination of C(sp³)–H enabled by amidyl radical under visible light.

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Scheme 8: Direct heteroarylation of C(sp³)–H and C(sp³)–H without the presence of strong bases, acids, or oxi...

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Scheme 9: Xanthylation of C(sp³)–H addressed by amidyl radical under visible light.

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Scheme 10: Xanthylation of C(sp³)–H in polyolefins addressed by amidyl radical under visible light.

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Scheme 11: Site-selective C(sp³)–H bromination implemented by amidyl radical under visible light.

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Scheme 12: Site-selective chlorination of C(sp³)–H in natural products implemented by amidyl radical under vis...

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Scheme 13: Alkylation of C(sp³)–H catalyzed by amidyl radical photocatalyst under visible light.

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Review

Published 27 Jun 2025

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