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1 article(s) from Acan, Ali S

An undecacyclic carbon-centered hydrocarbon radical: synthesis and investigation

Ali S. Acan,
Johannes Werner and
Joachim Podlech

Beilstein J. Org. Chem. 2026, 22, 1196–1204, doi:10.3762/bjoc.22.95

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Graphical Abstract

Figure 1: CP-PAH radicals synthesized in our group.

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Scheme 1: Synthesis of the nucleophilic outmost ring systems.

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Scheme 2: Suzuki coupling and establishment of the undecacyclic ring system.

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Scheme 3: Finalization of the radical synthesis.

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Figure 2: CW (continuous wave) X-band (9.4214 GHz) EPR spectrum of 7 in toluene (1 mM) at ambient temperature...

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Figure 3: Calculated spin densities of 7; blue: α spin, green: β spin (isovalue: 0.004 electrons per bohr; ca...

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Scheme 4: Resonance formulas of radical 7. Fully intact benzene rings are highlighted in blue; the indacene u...

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Figure 4: Calculated SOMOs of α (left) and β electrons (right) for radical 7 (also termed SOMO and SUMO in th...

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Figure 5: Cyclic voltammogram of 7 recorded in THF at room temperature (vs Fc/Fc⁺, v (THF) = 100 mV s⁻¹; Pt/[...

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Figure 6: UV–vis spectrum of radical 7 in CH₂Cl₂: measured (top), calculated (bottom).

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Figure 7: NICS(1)_πzz-XY-scan of radical 7 (calculated without mesityl and methyl groups).

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Figure 8: ACID isosurface plot of 7 (calculated without mesityl and methyl groups; isosurface value 0.02).

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Published 25 Aug 2026

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