1 article(s) from Battilocchio, Claudio
Raspberry Pi® (RPi) computer operating in the laboratory, shown here without its protective case. U...
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Two step approach to piperazine-2-carboxamide via hydrolysis followed by reduction. (a) Retrosynthe...
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Heterogeneous hydration of pyrazine-2-carbonitrile with hydrous zirconia.
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FlowIR™ profile for the reactor output after hydration of pyrazine-2-carbonitrile using hydrous zir...
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(a) Fluidic setup for the zirconia catalysed hydration of aromatic nitrile. (b) Raspberry Pi® micro...
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Flowchart describing the control sequence for operating and monitoring the hydration reaction. The ...
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Profile for a 3 hour reaction simulating a long run. The absorbance shown is that at 1685 cm−1, whi...
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Reactor setup for optimisation reactions. A multi-position valve (V2) was used for collecting sampl...
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Representation of the control sequence for running experiments under a set of conditions. (See Supporting Information File 3 for...
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Reduction products of piperazine-2-carboxamide.
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(a) In-line reservoir schematic. The liquid level is measured by observation of a plastic float. (b...
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Flow set up for the automated machine assisted synthesis of (R,S)-piperidine-2-carboxamide.
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Control sequence for the two-step process.
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Chart of monitored parameters over a 15 hour reaction. The output from the hydrolysis step is direc...
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Beilstein J. Org. Chem. 2014, 10, 641–652, doi:10.3762/bjoc.10.56
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