1 article(s) from Goessler, Walter
- Full Research Paper
- Published 21 Apr 2011
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Graphical Abstract
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Scheme 1: Azide–nitrile cycloaddition under batch microwave conditions.
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Figure 1: HPLC-UV chromatograms (215 nm) of crude reaction mixtures from the cycloaddition of diphenylacetoni...
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Figure 2: HPLC-UV chromatogram (215 nm) showing the decomposition of tetrazole 2 in NMP/AcOH/H2O 5:3:2 (0.125...
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Scheme 2: Possible decomposition mechanisms for tetrazole 2 in NMP/AcOH/H2O.
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Scheme 3: Reaction steps for the degradation of tetrazole 2 and the corresponding rate equations.
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Figure 3: Decomposition of tetrazole 2 at 240 °C in a NMP/AcOH/H2O 5:3:2 mixture (0.125 M) (points: experimen...
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Figure 4: Decomposition of tetrazole 2 in a 4 mL resistance heated stainless steel coil at a nominal temperat...
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Scheme 4: Mizoroki–Heck coupling under continuous flow conditions.
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Scheme 5: Nucleophilic aromatic substitution of 4-fluoro-1-nitrobenzene (15) with pyrrolidine (16) under cont...
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Figure 5: Nucleophilic aromatic substitution reaction of 1-fluoro-4-nitrobenzene (15) with pyrrolidine (16) i...
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