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1 article(s) from Goessler, Walter

Unusual behavior in the reactivity of 5-substituted-1H-tetrazoles in a resistively heated microreactor

Bernhard Gutmann,
Toma N. Glasnov,
Tahseen Razzaq,
Walter Goessler,
Dominique M. Roberge and
C. Oliver Kappe

Beilstein J. Org. Chem. 2011, 7, 503–517, doi:10.3762/bjoc.7.59

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Scheme 1: Azide–nitrile cycloaddition under batch microwave conditions.

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Figure 1: HPLC-UV chromatograms (215 nm) of crude reaction mixtures from the cycloaddition of diphenylacetoni...

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Figure 2: HPLC-UV chromatogram (215 nm) showing the decomposition of tetrazole 2 in NMP/AcOH/H₂O 5:3:2 (0.125...

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Scheme 2: Possible decomposition mechanisms for tetrazole 2 in NMP/AcOH/H₂O.

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Scheme 3: Reaction steps for the degradation of tetrazole 2 and the corresponding rate equations.

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Figure 3: Decomposition of tetrazole 2 at 240 °C in a NMP/AcOH/H₂O 5:3:2 mixture (0.125 M) (points: experimen...

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Figure 4: Decomposition of tetrazole 2 in a 4 mL resistance heated stainless steel coil at a nominal temperat...

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Scheme 4: Mizoroki–Heck coupling under continuous flow conditions.

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Scheme 5: Nucleophilic aromatic substitution of 4-fluoro-1-nitrobenzene (15) with pyrrolidine (16) under cont...

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Figure 5: Nucleophilic aromatic substitution reaction of 1-fluoro-4-nitrobenzene (15) with pyrrolidine (16) i...

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Published 21 Apr 2011

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