2 article(s) from Kitson, Philip J
Prusa i3 RepRap printer modified for the automated synthesis of ibuprofen. Left: Full view of robot...
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Synthetic route chosen for automated synthesis robot.
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Top: The three reaction vessels printed for ibuprofen synthesis on different scales; bottom left: i...
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The digitisation of the synthesis of ibuprofen. This flow diagram shows the individual steps of the...
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Beilstein J. Org. Chem. 2016, 12, 2776–2783, doi:10.3762/bjoc.12.276
Schematic representation of the 3D-printed reactionware devices employed in this work showing the i...
Flow system setup, where a R1 is connected to the syringe pumps and the ATR-IR flow cell with stand...
Carbonyl compounds and primary amines used in the syntheses reported in this work. Carbonyl compoun...
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ATR-IR spectra of the synthesis of compounds 3b (on the left) and 3d (on the right). The spectrum o...
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(a) IR spectra of benzaldehyde at different concentrations. The solvent peak at 1022 cm−1 remains c...
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Comparison of the IR spectra of imine 3a, derived from benzaldehyde (1a) and aniline (2a), synthesi...
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Representation of the setup for the two-step flow reaction employed in this work. The first reactor...
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Example of an ATR-IR graph in which an imine spectrum is compared with the reduced imine spectrum.
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Beilstein J. Org. Chem. 2013, 9, 951–959, doi:10.3762/bjoc.9.109
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