2 article(s) from Kitson, Philip J.
Prusa i3 RepRap printer modified for the automated synthesis of ibuprofen. Left: Full view of robot...
Jump to Figure 1
Synthetic route chosen for automated synthesis robot.
Jump to Scheme 1
Top: The three reaction vessels printed for ibuprofen synthesis on different scales; bottom left: i...
Jump to Figure 2
The digitisation of the synthesis of ibuprofen. This flow diagram shows the individual steps of the...
Jump to Scheme 2
Beilstein J. Org. Chem. 2016, 12, 2776–2783, doi:10.3762/bjoc.12.276
Schematic representation of the 3D-printed reactionware devices employed in this work showing the i...
Flow system setup, where a R1 is connected to the syringe pumps and the ATR-IR flow cell with stand...
Carbonyl compounds and primary amines used in the syntheses reported in this work. Carbonyl compoun...
Jump to Figure 3
ATR-IR spectra of the synthesis of compounds 3b (on the left) and 3d (on the right). The spectrum o...
Jump to Figure 4
(a) IR spectra of benzaldehyde at different concentrations. The solvent peak at 1022 cm−1 remains c...
Jump to Figure 5
Comparison of the IR spectra of imine 3a, derived from benzaldehyde (1a) and aniline (2a), synthesi...
Jump to Figure 6
Representation of the setup for the two-step flow reaction employed in this work. The first reactor...
Jump to Figure 7
Example of an ATR-IR graph in which an imine spectrum is compared with the reduced imine spectrum.
Jump to Figure 8
Beilstein J. Org. Chem. 2013, 9, 951–959, doi:10.3762/bjoc.9.109
Subscribe to our Latest Articles RSS Feed.
Register and get informed about new articles.
Follow the Beilstein-Institut