3 article(s) from North, Michael
The synthesis of F-1.
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View of the crystal structure of F-1 (F-1a phase), with representation of atoms by thermal ellipsoi...
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View of the crystal structure of F-1 (F-1a’ phase), with representation of the atoms via thermal el...
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SEM image of F-1.
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SEM image of F-1 with an F-1a phase.
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TGA-DSC analysis of a sample of F-1. The TGA plot is shown in green, the DSC curve is shown in blue...
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Uncrystallized F-1 or F-1 with an F-1a phase promoted the two- and three-phase reactions of styrene...
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CAHOF F-1-promoted reactions of cyclohexene oxide (5) with alcohols and water.
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F-1-promoted Diels–Alder reaction.
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Beilstein J. Org. Chem. 2020, 16, 1124–1134, doi:10.3762/bjoc.16.99
Synthesis of cyclic and polycarbonates.
Bifunctional aluminium–salen complexes, including those studied in this work.
Synthesis of salen ligands 8a and 8b.
The preparation of aluminum complexes 1, 2 and 10.
Possible formation of a dinuclear complex from 1 by treatment with H2O and Et3N.
MALDI–TOF spectrum of poly(hexene carbonate) prepared using catalyst 2. The peak at 565 Daltons cor...
GPC trace of poly(cyclohexene carbonate) prepared using catalyst 2. The chromatogram was obtained i...
Beilstein J. Org. Chem. 2015, 11, 1614–1623, doi:10.3762/bjoc.11.176
Synthesis and transformation of nonracemic silyl-protected cyanohydrins.
Highly active metal(salen) complexes for asymmetric cyanohydrin synthesis.
Synthesis of cyclic carbonates.
Synthesis of cyanohydrin trimethylsilyl ethers and acetates.
Equilibrium between bimetallic and monometallic Ti(salen) complexes.
Second-order kinetics plot for the addition of TMSCN to benzaldehyde at 0 °C catalysed by complex 2...
Plot of k2obs against , showing that the reactions are first order with respect to the concentratio...
Eyring plot to determine the activation parameters for catalyst 2 in propylene carbonate. The red a...
51V NMR spectra of complex 2 recorded at 50 °C. a) Spectrum in CDCl3; b) spectrum in CDCl3 with 500...
Structures consistent with the 51V NMR spectra.
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Bimetallic aluminium(salen) complex for asymmetric cyanohydrin synthesis.
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Rate determining transition states for asymmetric cyanohydrin synthesis: a) when Lewis base catalys...
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Hammett correlations with catalyst 2 at 0 °C. Data in red are obtained in dichloromethane , whilst ...
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Beilstein J. Org. Chem. 2010, 6, 1043–1055, doi:10.3762/bjoc.6.119
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