Effect of radiation-induced vacancy saturation on the first-order phase transformation in nanoparticles: insights from a model

• Aram Shirinyan and
• Yuriy Bilogorodskyy

Beilstein J. Nanotechnol. 2024, 15, 1453–1472, doi:10.3762/bjnano.15.117

• based on the fact that the movement of dislocations is impeded by particle surfaces (grain boundaries) quite rapidly. For example, a transmission electron microscopy study (irradiation with Kr ions at 1 MeV at room temperature and an average defect generation rate of about 2 × 10−3 dpa·s−1) showed that

• film through in situ ion irradiation, observed using atomic-resolution transmission electron microscopy [16]. The gold sample was irradiated with 2.8 MeV Au4+ ions at 200 °C with a fluence of approximately 1014 ions·cm−2 (equivalent to a dose of 10 dpa). A combination of surface- and radiation-induced

• et al. used transmission electron microscopy to investigate nanoscale Pd under 240 keV Kr ion irradiation with a flux of 1013 ions·cm−2·s−1. Pd had grain sizes, d, ranging from 10 to 100 nm. The authors found that the defect density increases with increasing grain size d, and the slope between defect

Various CVD-grown ZnO nanostructures for nanodevices and interdisciplinary applications

• The-Long Phan,
• Le Viet Cuong,
• Vu Dinh Lam and
• Ngoc Toan Dang

Beilstein J. Nanotechnol. 2024, 15, 1390–1399, doi:10.3762/bjnano.15.112

• results prove that ZnO exhibits many novel nanostructures that can foster the development of next-generation optoelectronic nanodevices and new applications in biological and biomedical fields. Keywords: chemical vapour deposition; electron microscopy; Raman and photoluminescent spectra; ZnO

• down to collect white products formed on Si substrates. They were characterized by scanning electron microscopy (SEM, JEOL-6330F) and energy-dispersive X-ray (EDX) spectroscopy. Renishaw’s RS and PL spectrometers operating with laser wavelengths of 488 and 325 nm were also employed to study phonon

A biomimetic approach towards a universal slippery liquid infused surface coating

• Ryan A. Faase,
• Madeleine H. Hummel,
• AnneMarie V. Hasbrook,
• Andrew P. Carpenter and
• Joe E. Baio

Beilstein J. Nanotechnol. 2024, 15, 1376–1389, doi:10.3762/bjnano.15.111

• 2.5% glutaraldehyde in 0.1 M sodium cacodylate buffer overnight. Samples were then rinsed twice in 0.1 M cacodylate buffer for 15 min each. Samples were dehydrated in a graded series of ethanol (10%, 30%, 50%, 70%, 90%, 95%, and 100%) for 10–15 min each, followed by critical point drying (Electron

• Microscopy Sciences). Samples were sputter-coated with gold/palladium (Cressington 108A) and imaged on a scanning electron microscope (SEM) (FEI Quanta 600F). ImageJ was used to measure fiber diameter and clot density. Clot density was determined by drawing a line through the image and counting the number of

Green synthesis of carbon dot structures from Rheum Ribes and Schottky diode fabrication

• Muhammed Taha Durmus and
• Ebru Bozkurt

Beilstein J. Nanotechnol. 2024, 15, 1369–1375, doi:10.3762/bjnano.15.110

• Cary Eclipse fluorescence spectrophotometer were used for transmission electron microscopy (TEM), zeta potential measurements, X-ray diffractometry (XRD), Fourier-transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), micro-Raman spectroscopy, PVD thermal evaporation, scanning

• electron microscopy (SEM), I–V/C–V measurements, UV–vis spectroscopy, and steady-state fluorescence spectroscopy, respectively. CDs synthesis 2.5 g of the powdered Rheum ribes plant was placed in an autoclave bottle, and 50 mL of pure water was added to the bottle. This aqueous solution was placed in an

Out-of-plane polarization induces a picosecond photoresponse in rhombohedral stacked bilayer WSe₂

• Guixian Liu,
• Yufan Wang,
• Zhoujuan Xu,
• Zhouxiaosong Zeng,
• Lanyu Huang,
• Cuihuan Ge and
• Xiao Wang

Beilstein J. Nanotechnol. 2024, 15, 1362–1368, doi:10.3762/bjnano.15.109

• . To enrich the basic characterizations of WSe2, we conducted Raman spectroscopy and scanning electron microscopy (SEM) measurements (Supporting Information File 1, Note 5). The broken symmetry leads to an asymmetric distribution of photogenerated carriers, resulting in a non-zero photocurrent even

Hymenoptera and biomimetic surfaces: insights and innovations

• Vinicius Marques Lopez,
• Carlo Polidori and
• Rhainer Guillermo Ferreira

Beilstein J. Nanotechnol. 2024, 15, 1333–1352, doi:10.3762/bjnano.15.107

Nanoarchitectonics with cetrimonium bromide on metal nanoparticles for linker-free detection of toxic metal ions and catalytic degradation of 4-nitrophenol

• Akash Kumar and
• Raja Gopal Rayavarapu

Beilstein J. Nanotechnol. 2024, 15, 1312–1332, doi:10.3762/bjnano.15.106

• two minor peaks at 55.04° and 73.14°, which correspond to the (220) and (311) planes; these were also observed in other studies with CTAB-capped silver nanoparticles [44]. These peaks might be related to the formation of AgO in the nanoparticles, which is reported elsewhere [44]. Transmission electron

• microscopy (TEM) enables precise nanoparticle size and shape measurements. TEM images show that AuNR1 and AuNR2 have a rod-like shape with different sizes, whereas AuNS and AgNS are spherical (Figure 3a–d). The mean sizes of CTAB-AgNS and CTAB-AuNS are 27.4 ± 4.6 and 21.1 ± 3.6 nm, respectively (Figure 3e

Mn-doped ZnO nanopowders prepared by sol–gel and microwave-assisted sol–gel methods and their photocatalytic properties

• Cristina Maria Vlăduț,
• Crina Anastasescu,
• Silviu Preda,
• Oana Catalina Mocioiu,
• Simona Petrescu,
• Jeanina Pandele-Cusu,
• Dana Culita,
• Veronica Bratan,
• Ioan Balint and
• Maria Zaharescu

Beilstein J. Nanotechnol. 2024, 15, 1283–1296, doi:10.3762/bjnano.15.104

• samples were thermally treated at 350 °C and 500 °C for 1 h each. Scanning electron microscopy The morphology and chemical composition (inset) of the thermally treated samples is illustrated in Figure 4. Homogeneously distributed, quasi-spherical nanoparticles (mean size diameter of 70 nm) are observed in

• morphologies and the compositions of the calcined samples were evaluated by scanning electron microscopy (SEM-EDS), using a FEI Quanta 3D FEG instrument equipped with the Octane Elect EDS system. The powder samples were placed on double-sided carbon tape and recorded without coating at accelerating voltages of

Functional morphology of cleaning devices in the damselfly Ischnura elegans (Odonata, Coenagrionidae)

• Silvana Piersanti,
• Gianandrea Salerno,
• Wencke Krings,
• Stanislav Gorb and
• Manuela Rebora

Beilstein J. Nanotechnol. 2024, 15, 1260–1272, doi:10.3762/bjnano.15.102

• , situated on the foreleg tibiae, were observed using scanning electron microscopy, and the presence and distribution of resilin, an elastomeric protein that enhances cuticle flexibility, were analyzed using confocal laser scanning microscopy. Eye and antennal grooming behavior were analyzed to evaluate the

• used to clean the head and, especially, the eyes and the antennae. The microstructures were observed using scanning electron microscopy (SEM), and the presence and distribution of resilin, an elastomeric protein that enhances cuticle deformability and flexibility (review in [36]), were analyzed using

• % glutaraldehyde in sodium cacodylate buffer (Electron Microscopy Sciences, Hatfield, PA, USA) with a pH of 7.2, repeatedly rinsed in sodium cacodylate buffer and post-fixed for 1 h at 4 °C in 1% osmium tetroxide in sodium cacodylate buffer (Electron Microscopy Sciences). Fixed samples were repeatedly rinsed in

Dual-functionalized architecture enables stable and tumor cell-specific SiO₂NPs in complex biological fluids

• Iris Renata Sousa Ribeiro,
• Raquel Frenedoso da Silva,
• Romênia Ramos Domingues,
• Adriana Franco Paes Leme and
• Mateus Borba Cardoso

Beilstein J. Nanotechnol. 2024, 15, 1238–1252, doi:10.3762/bjnano.15.100

• ), SiO2NPs-ZW-NH2 (with ZW + APTES), and SiO2NPs-ZW-FO (with ZW + APTES + folate). Characterization of SiO2NPs Scanning electron microscopy (SEM) micrographs were obtained in a high-resolution FEI Inspect F50 microscope. A NP suspension (7 μL) was deposited directly onto a copper substrate, dried, and

Enhanced catalytic reduction through in situ synthesized gold nanoparticles embedded in glucosamine/alginate nanocomposites

• Chi-Hien Dang,
• Le-Kim-Thuy Nguyen,
• Minh-Trong Tran,
• Van-Dung Le,
• Nguyen Minh Ty,
• T. Ngoc Han Pham,
• Hieu Vu-Quang,
• Tran Thi Kim Chi,
• Tran Thi Huong Giang,
• Nguyen Thi Thanh Tu and
• Thanh-Danh Nguyen

Beilstein J. Nanotechnol. 2024, 15, 1227–1237, doi:10.3762/bjnano.15.99

• a Bruker Tensor 27 FTIR spectrophotometer, which scanned wavelengths from 500 to 4000 cm−1. KBr pellets were used for the measurements. For morphological investigations of the nanocomposites, scanning electron microscopy (SEM) was performed using a SEM-S4800 instrument; transmission electron

• microscopy (TEM) and selected area electron diffraction (SAED) were carried out using a JEOL JEM-2100 instrument. Crystal structure characterizations of AuNPs were carried out via XRD diffraction. Zeta potential and dynamic light scattering (DLS) measurements were carried out on gel solutions (1.0 mg·mL−1

Synthesis, characterization and anticancer effect of doxorubicin-loaded dual stimuli-responsive smart nanopolymers

• Ömür Acet,
• Pavel Kirsanov,
• Burcu Önal Acet,
• Inessa Halets-Bui,
• Dzmitry Shcharbin,
• Şeyda Ceylan Cömert and
• Mehmet Odabaşı

Beilstein J. Nanotechnol. 2024, 15, 1189–1196, doi:10.3762/bjnano.15.96

• . Characterizations of the synthesized nanostructures were carried out including zeta potential measurements, Fourier-transform infrared spectroscopy, and scanning electron microscopy. The loading capacity of the nanopolymers for DOX was investigated, and encapsulation and release studies were carried out. In a final

• . Scanning electron microscopy (SEM, Leo 440) was utilized for morphological characterizations of the SNPs; lyophilized SNPs were coated with gold, and the samples were placed in the SEM. The zeta potential the of DOX-SNPs was measured by using a Nano Zetasizer (NanoS, Malvern Instruments, London, UK

Unveiling the potential of alginate-based nanomaterials in sensing technology and smart delivery applications

• Shakhzodjon Uzokboev,
• Khojimukhammad Akhmadbekov,
• Ra’no Nuritdinova,
• Salah M. Tawfik and
• Yong-Ill Lee

Beilstein J. Nanotechnol. 2024, 15, 1077–1104, doi:10.3762/bjnano.15.88

• scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The shape and size of the nanoparticles can be determined by these two methods [59]. TEM is extensively utilized and can differentiate between nanocapsules and nanospheres, as well as measure the thickness of the nanocapsule

Effect of wavelength and liquid on formation of Ag, Au, Ag/Au nanoparticles via picosecond laser ablation and SERS-based detection of DMMP

• Sree Satya Bharati Moram,
• Chandu Byram and
• Venugopal Rao Soma

Beilstein J. Nanotechnol. 2024, 15, 1054–1069, doi:10.3762/bjnano.15.86

• was meticulously evaluated by analyzing the ablation rates, surface plasmon resonance peak positions, and particle size distributions of the obtained colloids. The nanoparticles (NPs) were characterized using the techniques of UV–visible absorption, transmission electron microscopy, and energy

• imaging due to the nonconductive nature of the FP substrate. FESEM energy-dispersive X-ray spectroscopy (EDX) mapping investigations were conducted on Ag/Au alloy NPs deposited on a Si substrate by drop casting 10 µL to avoid confusion in the data caused by the Au coating. Transmission electron microscopy

• studies of as-synthesized nanoparticles Transmission electron microscopy analysis was implemented to study the size and shape of laser-fabricated NPs. Figure 2 shows the TEM images of Ag NPs synthesized in DW at different laser wavelengths: (a) 355, (b) 532, and (c) 1064 nm. It should be noted that the

Bolometric IR photoresponse based on a 3D micro-nano integrated CNT architecture

• Yasameen Al-Mafrachi,
• Sandeep Yadav,
• Sascha Preu,
• Jörg J. Schneider and
• Oktay Yilmazoglu

Beilstein J. Nanotechnol. 2024, 15, 1030–1040, doi:10.3762/bjnano.15.84

• stability, retaining reliability at temperatures reaching up to 200 °C. This exceptional thermal resilience makes it ideally suited for demanding high-temperature applications, showing its potential across various industries. Transmission electron microscopy (TEM) and Raman characterizations of the VACNTs

• . (a) Scanning electron microscopy image and (b) 3D close-up of the pixel-based CNT microbolometer. (a) TEM image showing DWCNTs and (b) Raman spectrum of the VACNTs. Schematic of the device under test (DUT) and measurement setups to characterize the CNT-based microbolometer. (a) Sample 1 with metal

Entry of nanoparticles into cells and tissues: status and challenges

• Kirsten Sandvig,
• Tore Geir Iversen and
• Tore Skotland

Beilstein J. Nanotechnol. 2024, 15, 1017–1029, doi:10.3762/bjnano.15.83

• in an invagination of the cell. This can be performed by different methods. If electron microscopy (EM) is used, it is important that serial sectioning is performed. Otherwise, one may see a particle which is apparently internalized, since it is far from the cell surface, but it might still be in an

• [29]. Other microscopy techniques that are useful for such studies are correlative light and electron microscopy (CLEM) [30], confocal microscopy with Z-stacks [4], and structured illumination microscopy (SIM) which can also demonstrate in which organelles the NPs are localized. The SIM image shown in

Beyond biomimicry – next generation applications of bioinspired adhesives from microfluidics to composites

• Dan Sameoto

Beilstein J. Nanotechnol. 2024, 15, 965–976, doi:10.3762/bjnano.15.79

• within channels is distributed between more fibers surrounding the channels. Panel (b) shows a scanning electron microscopy image of a 5 × 7 mm gecko gasket design for electrophoresis. Panel (c) is a compilation image of multiple applications for the gecko gaskets, including microfluidics integrated on

Therapeutic effect of F127-folate@PLGA/CHL/IR780 nanoparticles on folate receptor-expressing cancer cells

• Thi Ngoc Han Pham,
• Phuong-Thao Dang-Luong,
• Hong-Phuc Nguyen,
• Loc Le-Tuan,
• Xuan Thang Cao,
• Thanh-Danh Nguyen,
• Vy Tran Anh and
• Hieu Vu_Quang

Beilstein J. Nanotechnol. 2024, 15, 954–964, doi:10.3762/bjnano.15.78

• scattering (DLS) and zeta potential spectra measurements were carried out in three replicates on a nanoPartica Horiba SZ-100 (Japan) with a scattering angle of 90° at 25 °C to determine the size distribution and stability of the nanocomposites. Scanning electron microscopy (SEM) The F127-folate@PLGA/CHL

Facile synthesis of Fe-based metal–organic frameworks from Fe₂O₃ nanoparticles and their application for CO₂/N₂ separation

• Van Nhieu Le,
• Hoai Duc Tran,
• Minh Tien Nguyen,
• Hai Bang Truong,
• Toan Minh Pham and
• Jinsoo Kim

Beilstein J. Nanotechnol. 2024, 15, 897–908, doi:10.3762/bjnano.15.74

• and yield of the as-prepared MIL-100(Fe) materials, including thermogravimetric analysis (TGA), Fourier-transform infrared (FTIR) spectroscopy, powder X-ray diffraction (PXRD) measurements, determination of textural properties, scanning electron microscopy (SEM), and X-ray photoelectron spectroscopy

Water-assisted purification during electron beam-induced deposition of platinum and gold

• Cristiano Glessi,
• Fabian A. Polman and
• Cornelis W. Hagen

Beilstein J. Nanotechnol. 2024, 15, 884–896, doi:10.3762/bjnano.15.73

• % ratio correction can be found in Supporting Information File 1 (pp S3–S5). TEM A TEM lamella was prepared in a TFS Helios dual-beam system. A PtCx layer was deposited from MeCpPtMe3 as a protection layer. Transmission electron microscopy (TEM) and STEM-EDX analysis were performed in an FEI Titan Cubed

The effect of age on the attachment ability of stick insects (Phasmatodea)

• Marie Grote,
• Stanislav N. Gorb and
• Thies H. Büscher

Beilstein J. Nanotechnol. 2024, 15, 867–883, doi:10.3762/bjnano.15.72

• projections. 8 Scanning Electron Microscopy (SEM) For inspection of the tarsal morphology of different age groups, samples were chosen after CLSM to compare regions of interest, such as altered autofluorescence or damage. Selected tarsi were transferred from glycerin into 50% ethanol via a gradual series of

A review on the structural characterization of nanomaterials for nano-QSAR models

• Salvador Moncho,
• Eva Serrano-Candelas,
• Jesús Vicente de Julián-Ortiz and
• Rafael Gozalbes

Beilstein J. Nanotechnol. 2024, 15, 854–866, doi:10.3762/bjnano.15.71

• ]. At the other extreme, there are studies where the only difference among the nanoforms used (without considering endpoint-related descriptors such as dose or time) is the size [58][59]. The size of nanoparticles is commonly measured by transmission electron microscopy (TEM). TEM images can provide

Intermixing of MoS₂ and WS₂ photocatalysts toward methylene blue photodegradation

• Maryam Al Qaydi,
• Nitul S. Rajput,
• Michael Lejeune,
• Abdellatif Bouchalkha,
• Mimoun El Marssi,
• Steevy Cordette,
• Chaouki Kasmi and
• Mustapha Jouiad

Beilstein J. Nanotechnol. 2024, 15, 817–829, doi:10.3762/bjnano.15.68

• binding energies). This means there is no chemical shift in the compounds, implying that the intermixing of Mo and W did not disturb the chemical environment, and the elements retained a stable chemical bond. Microstructure analysis Figure 4 shows scanning electron microscopy (SEM) images of all

• considered samples. The specimens were prepared by drop casting a solution of the exfoliated samples on lacey carbon transmission electron microscopy (TEM) grids. Additionally, agglomeration of the flakes can be usually observed as well, which could be due to the effect of the solvent used for drop casting

Synthesis of silver–palladium Janus nanoparticles using co-sputtering of independent sources: experimental and theorical study

• Maria J. Martínez-Carreón,
• Francisco Solís-Pomar,
• Abel Fundora,
• Claudio D. Gutiérrez-Lazos,
• Sergio Mejía-Rosales,
• Hector N. Fernández-Escamilla,
• Jonathan Guerrero-Sánchez,
• Manuel F. Meléndrez and
• Eduardo Pérez-Tijerina

Beilstein J. Nanotechnol. 2024, 15, 808–816, doi:10.3762/bjnano.15.67

• promote the synthesis of bimetallic Janus nanoparticles. The structural properties of the resulting nanoparticles were investigated by transmission electron microscopy (TEM), and the chemical composition was analyzed by TEM energy dispersive spectroscopy (TEM-EDS), which, together with structural analysis

• methods. MD and electron microscopy simulations show that the features observed in the electron micrographs of real Janus AgPd BNPs can be fairly reproduced if the Ag lattice is slightly rotated with respect to the Pd lattice. Using DFT approximations, we have proposed a set of structural models that

Electrospun polysuccinimide scaffolds containing different salts as potential wound dressing material

• Veronika Pálos,
• Krisztina S. Nagy,
• Rita Pázmány,
• Krisztina Juriga-Tóth,
• Bálint Budavári,
• Judit Domokos,
• Dóra Szabó,
• Ákos Zsembery and
• Angela Jedlovszky-Hajdu

Beilstein J. Nanotechnol. 2024, 15, 781–796, doi:10.3762/bjnano.15.65

• biological properties of the scaffolds developed for application as wound dressings. The scaffold systems obtained by PSI synthesis, salt addition, and fiber formation were first investigated by scanning electron microscopy. In almost all cases, different salts caused a decrease in the fiber diameter of PSI

• scanning electron microscopy (SEM), Fourier-transform infrared spectroscopy (FTIR), mechanical tests, investigation of salt dissolution from the scaffolds, examination of their antibacterial activity against four different bacterial strains (Escherichia coli, Pseudomonas aeruginosa, Bacillus subtilis, and

• . Scanning electron microscopy and energy-dispersive X-ray spectroscopy Scanning electron microscopy images were taken to determine the fiber diameters of salt-containing polymer scaffolds. They were made at the Budapest University of Technology and Economics, Department of Polymer Technology, applying a