Enhancing higher-order modal response in multifrequency atomic force microscopy with a coupled cantilever system

• Wendong Sun,
• Jianqiang Qian,
• Yingzi Li,
• Yanan Chen,
• Zhipeng Dou,
• Rui Lin,
• Peng Cheng,
• Xiaodong Gao,
• Quan Yuan and
• Yifan Hu

Beilstein J. Nanotechnol. 2024, 15, 694–703, doi:10.3762/bjnano.15.57

• parameters Several commercial rectangular multifrequency AFM cantilevers of different sizes from different manufacturers are summarized in [24]. In the ANSYS Workbench finite element simulation, the material used in the simulation is silicon, with a Young's modulus of 166 GPa and a density of 2330 kg/m3. We

Gold nanomakura: nanoarchitectonics and their photothermal response in association with carrageenan hydrogels

• Nabojit Das,
• Vikas,
• Akash Kumar,
• Sanjeev Soni and
• Raja Gopal Rayavarapu

Beilstein J. Nanotechnol. 2024, 15, 678–693, doi:10.3762/bjnano.15.56

• nanomakura shape was determined by the surfactant capping, clearly indicating the effect of carbon tail length. The breaking of symmetry was due to a gradual decrease in micelle density on the edges giving the shape of a pillow as shown in Figure 6 The highest intensity of {111} observed in the XRD

• structures, micelles with longer carbon tail lengths form more compact bilayer structures and vice versa. Also, the density of mixed micellar structure of CTAB is higher and is followed by MTAB and DTAB, respectively; thus, resulting in the formation of AuNMs of different aspect ratios. The corroboration of

• particles per 1 mL has been used to maintain the reproducibility of particle density in the hydrogel. A volume of 1 mL of the sample showing 4 OD was achieved by pooling the required number of pellets, and was dispersed into 7 mL of k-carrageenan making the solution blue in colour. Finally, the solution was

Functional fibrillar interfaces: Biological hair as inspiration across scales

• Guillermo J. Amador,
• Brett Klaassen van Oorschot,
• Caiying Liao,
• Jianing Wu and
• Da Wei

Beilstein J. Nanotechnol. 2024, 15, 664–677, doi:10.3762/bjnano.15.55

• review include the hair and fur of mammals, the feathers of birds, the trichomes of plants, the setae of arthropods, and the ultrastructures of single-celled organisms. Figure 1A shows how the total hair mass mh scales with body mass mb. For mh, a material density of 1 g·cm−3 was assumed. A relationship

• have presumably persisted because of their thermal insulation properties. In mammals, the thickness and packing density of hair arrays was found to coincide with the geometrical parameters that minimize convective heat loss, with the hair diameter d scaling as [5][24]. In aquatic mammals, hair

• morphology, including shape and packing density, differ from terrestrial mammals in order to maintain a trapped air layer within the arrays of hair when submerged in water [30]. Hairs of aquatic animals have been found to be flatter, shorter, and packed in higher densities. Additionally, mammals that also

Laser synthesis of nanoparticles in organic solvents – products, reactions, and perspectives

• Theo Fromme,
• Sven Reichenberger,
• Katharine M. Tibbetts and
• Stephan Barcikowski

Beilstein J. Nanotechnol. 2024, 15, 638–663, doi:10.3762/bjnano.15.54

• . Optical breakdown occurs when the free-electron density surpasses a critical value, resulting in a high-density plasma, and the optical breakdown threshold is significantly reduced in the presence of metal nanoparticles [49][81][82]. Supercontinuum emission can occur at low fluences, when pulses shorter

• than 100 fs are used, and will produce a low-density plasma [83]. More recently, the Vogel group studied the energy spectrum of laser-induced conduction band electrons in water by introducing a simplified splitting scheme and corresponding rate equations, well suited also for the calculation of energy

• the ionic strength of the added salts and the obtained gold particle size (Figure 2). The surface oxidation increased with the anion’s surface charge density until a plateau of around 60% was reached. A further increase in ionic strength showed no change in surface oxidation, which was attributed to

Comparative analysis of the ultrastructure and adhesive secretion pathways of different smooth attachment pads of the stick insect Medauroidea extradentata (Phasmatodea)

• Julian Thomas,
• Stanislav N. Gorb and
• Thies H. Büscher

Beilstein J. Nanotechnol. 2024, 15, 612–630, doi:10.3762/bjnano.15.52

• blue. In addition, the blue colour intensity corresponds to the relative electron density of the tissue in TEM [57][58][59]. Cason’s triple stain allows for the differentiation of differently sclerotized regions from brown over orange to yellow (with a decreasing degree of sclerotization) to resilin

• of the tarsomeres internally extend into the corresponding tarsomere. The structure connecting the two attachment pads shows morphological similarities with the attachment pad. In the µCT, the outer hull of this structure exhibits high radiodensity and the inner body shows lesser density (Figure 4A

Stiffness calibration of qPlus sensors at low temperature through thermal noise measurements

• Laurent Nony,
• Sylvain Clair,
• Daniel Uehli,
• Aitziber Herrero,
• Jean-Marc Themlin,
• Andrea Campos,
• Franck Para,
• Alessandro Pioda and
• Christian Loppacher

Beilstein J. Nanotechnol. 2024, 15, 580–602, doi:10.3762/bjnano.15.50

• relies both on numerical simulations and experimental results. A thorough analysis of the thermal noise power spectral density of the qPlus fluctuations leads to an estimated stiffness of the first flexural eigenmode of ≃2000 N/m, with a maximum uncertainty of 10%, whereas the static stiffness of the

• Information File 2 reminds fundamental elements of signal processing applied to discrete time signals, which include the power spectral density (PSD), a key tool for the stiffness calibration. Supporting Information File 3 reminds the expression of the thermal noise PSD of a SHO in thermal equilibrium within

• mass mprobe is to be estimated then. In this framework, the probe is assumed to behave as an equivalent SHO; then, the static stiffness is derived from f1 according to: . The quantity is the effective mass of the fundamental eigenmode of the probe; mprobe = ρwtl is calculated from the density ρ

Radiofrequency enhances drug release from responsive nanoflowers for hepatocellular carcinoma therapy

• Yanyan Wen,
• Ningning Song,
• Yueyou Peng,
• Weiwei Wu,
• Qixiong Lin,
• Minjie Cui,
• Rongrong Li,
• Qiufeng Yu,
• Sixue Wu,
• Yongkang Liang,
• Wei Tian and
• Yanfeng Meng

Beilstein J. Nanotechnol. 2024, 15, 569–579, doi:10.3762/bjnano.15.49

• (Solarbio Life Sciences, Beijing, China) at 37 °C for 30 min. Cytotoxicity assays The Huh-7 cells were seeded onto 4-chamber cell culture slides (Nalge Nunc International, Rochester, NY, USA) at a density of 1.0 × 106 cells/chamber. The cells were incubated at 37 °C in 5% CO2 for 24 h. The DMEM medium was

Directed growth of quinacridone chains on the vicinal Ag(35 1 1) surface

• Niklas Humberg,
• Lukas Grönwoldt and
• Moritz Sokolowski

Beilstein J. Nanotechnol. 2024, 15, 556–568, doi:10.3762/bjnano.15.48

• Figure 2c. We suppose that the adsorption of a QA molecule at the step edge on the upper/lower terrace induces a local change in the electron density at the step edge. This favors a specific adsorption site of a second QA molecule with the same chirality and azimuthal orientation at the step edge on the

• chains of the orientations A–D in areas with a high density of unidirectional steps. Nevertheless, on the small terraces, the formation of chains with orientation E may be kinetically inhibited because of a lack of space, which hinders the diffusion of the molecules to the growing endpoints of the chains

• the azimuthal orientations of the chains relative to the step edges [37]. The chains of NDCA grow along the [10] direction of the substrate and are, thus, orthogonal to the direction of the step edges, which are oriented along the [01] direction. Density functional theory calculations have shown that

On the additive artificial intelligence-based discovery of nanoparticle neurodegenerative disease drug delivery systems

• Shan He,
• Julen Segura Abarrategi,
• Harbil Bediaga,
• Sonia Arrasate and
• Humberto González-Díaz

Beilstein J. Nanotechnol. 2024, 15, 535–555, doi:10.3762/bjnano.15.47

• donor atoms from P_VSA-like descriptors), Dn17 = Vxcoat (McGowan volume), Dn18 = VvdwMGcoat (van der Waals volume from McGowan volume), Dn19 = VvdwZAZcoat (van der Waals volume from the Zhao–Abraham–Zissimos equation), and Dn20 = PDIcoat (packing density index). PT data preprocessing Apart from the

Cholesterol nanoarchaeosomes for alendronate targeted delivery as an anti-endothelial dysfunction agent

• Horacio Emanuel Jerez,
• Yamila Roxana Simioni,
• Kajal Ghosal,
• Maria Jose Morilla and
• Eder Lilia Romero

Beilstein J. Nanotechnol. 2024, 15, 517–534, doi:10.3762/bjnano.15.46

• . Finally, the absorbance was measured at 550 nm as stated before. Uptake of nanovesicles The uptake of RhPE-labelled nanovesicles by THP-1 monocytes and macrophages was measured by flow cytometry. Briefly, THP-1 monocytes were seeded on 24-well culture plates at a density of 1 × 106 cells per well (150 µL

• ), and THP-1 macrophages were seeded on 24-well culture plates at a density of 1.5 × 105 cells per well and grown for 24 h. Then, the cells were incubated with 100 μg/mL TL of RhPE nanovesicles in complete medium for 1 and 5 h at 37 °C. After incubation, THP-1 macrophages were trypsinized. THP-1

• (Flowing Software, Finland). Plasma membrane order Effects of nanovesicle uptake on THP-1 macrophages and HUVEC plasma membrane order were determined by measuring the Laurdan generalized polarization (GP) [83]. Briefly, THP-1 macrophages and HUVECs grown at a density of 1–1.5 × 104 cells/cm2 on 96-well

Electron-induced deposition using Fe(CO)₄MA and Fe(CO)₅ – effect of MA ligand and process conditions

• Hannah Boeckers,
• Atul Chaudhary,
• Petra Martinović,
• Amy V. Walker,
• Lisa McElwee-White and
• Petra Swiderek

Beilstein J. Nanotechnol. 2024, 15, 500–516, doi:10.3762/bjnano.15.45

Aero-ZnS prepared by physical vapor transport on three-dimensional networks of sacrificial ZnO microtetrapods

• Veaceslav Ursaki,
• Tudor Braniste,
• Victor Zalamai,
• Emil Rusu,
• Vladimir Ciobanu,
• Vadim Morari,
• Daniel Podgornii,
• Pier Carlo Ricci,
• Rainer Adelung and
• Ion Tiginyanu

Beilstein J. Nanotechnol. 2024, 15, 490–499, doi:10.3762/bjnano.15.44

• 10 × 10 mm2 to prepare 2 mm thick sample tablets. In order to increase the mechanical stability, the tablets with a density of 0.5 g/cm3 were annealed at 1000 °C for 1 h in air. Morphology analysis was carried out with a VEGA TESCAN 5130 SEM instrument equipped with an EDX detector from Oxford

Sidewall angle tuning in focused electron beam-induced processing

• Sangeetha Hari,
• Willem F. van Dorp,
• Johannes J. L. Mulders,
• Piet H. F. Trompenaars,
• Pieter Kruit and
• Cornelis W. Hagen

Beilstein J. Nanotechnol. 2024, 15, 447–456, doi:10.3762/bjnano.15.40

• . The SE1 are distributed close to the primary beam, while the low-density SE2 are spread out over a much larger area. For simplicity, the spatial distribution of low-energy electrons around the point of impact of the primary beam with the substrate is assumed to be of a Gaussian shape. Depending on the

Heat-induced morphological changes in silver nanowires deposited on a patterned silicon substrate

• Elyad Damerchi,
• Sven Oras,
• Edgars Butanovs,
• Allar Liivlaid,
• Mikk Antsov,
• Boris Polyakov,
• Annamarija Trausa,
• Veronika Zadin,
• Andreas Kyritsakis,
• Loïc Vidal,
• Karine Mougin,
• Siim Pikker and
• Sergei Vlassov

Beilstein J. Nanotechnol. 2024, 15, 435–446, doi:10.3762/bjnano.15.39

• nanoscale devices [8]. When deposited on a transparent substrate in the form of a low-density mesh, metal NWs can provide electrical conductivity while retaining sufficient transparency. The growing demand for transparent conductive materials has stimulated numerous studies aimed at the design, preparation

Classification and application of metal-based nanoantioxidants in medicine and healthcare

• Nguyen Nhat Nam,
• Nguyen Khoi Song Tran,
• Tan Tai Nguyen,
• Nguyen Ngoc Trai,
• Nguyen Phuong Thuy,
• Hoang Dang Khoa Do,
• Nhu Hoa Thi Tran and
• Kieu The Loan Trinh

Beilstein J. Nanotechnol. 2024, 15, 396–415, doi:10.3762/bjnano.15.36

• antioxidant appearing in low-density lipoprotein and human blood plasma contributing to the decrease of oxidative stress. Its mechanism of action relies on the ability to transfer the phenolic H atom to a peroxyl radical (ROO•) much more rapidly than the propagation reactions [50][51][52][53]. Despite the

• three key components: (1) edaravone and nanoceria were responsible for ROS scavenging; (2) poly(ethylene glycol) increased biocompatibility, monodispersity, and extended the half-life in the bloodstream; and (3) angiopep-2 served as targeting ligand, which specifically binds to the low-density

Insect attachment on waxy plant surfaces: the effect of pad contamination by different waxes

• Elena V. Gorb and
• Stanislav N. Gorb

Beilstein J. Nanotechnol. 2024, 15, 385–395, doi:10.3762/bjnano.15.35

• [8] tests up to precise measurements of attachment forces with different experimental techniques, such as pulling [9] and centrifugal [10] setups. It has been demonstrated that not only the presence of wax projections on the plant cuticle surface, but also their size, distribution, and density

On the mechanism of piezoresistance in nanocrystalline graphite

• Sandeep Kumar,
• Simone Dehm and
• Ralph Krupke

Beilstein J. Nanotechnol. 2024, 15, 376–384, doi:10.3762/bjnano.15.34

• density of defects in the form of grain boundaries. It holds an advantage over graphene in easily achieving wafer-scale growth with controlled thickness. In this study, we explore the piezoresistivity in thin films of nanocrystalline graphite. Simultaneous measurements of sheet resistance and externally

Investigating ripple pattern formation and damage profiles in Si and Ge induced by 100 keV Ar⁺ ion beam: a comparative study

• Indra Sulania,
• Harpreet Sondhi,
• Tanuj Kumar,
• Sunil Ojha,
• G R Umapathy,
• Ambuj Mishra,
• Ambuj Tripathi,
• Richa Krishna,
• Devesh Kumar Avasthi and
• Yogendra Kumar Mishra

Beilstein J. Nanotechnol. 2024, 15, 367–375, doi:10.3762/bjnano.15.33

• to induce that type of energy deposition in the Ge lattice. This way, the defects can be produced and the substrate can be amorphized. The roughness and growth exponents have been deduced from the RMS surface roughness and power spectral density data to understand the mechanism of ripple formation on

• Si and Ge. From the slope, n, of the linear part of power spectral density (PSD) curves, one may find the roughness parameter α using the formula α = (n − 1)/d, where d is the dimension of PSD [40]. In our case it is 2. Further, from the log plot of RMS roughness as a function of ion fluence, the

• nm (A) and 170 nm (B) with an integral density of point defects of ≈0.17 × 1018 per cm2 and 0.38 × 1017 per cm2 for Ge and Si, respectively, as calculated by DICADA. This may be due to the tailing effects where an incoming ion comes to rest after travelling a certain distance inside the target

Modulated critical currents of spin-transfer torque-induced resistance changes in NiCu/Cu multilayered nanowires

• Mengqi Fu,
• Roman Hartmann,
• Julian Braun,
• Sergej Andreev,
• Torsten Pietsch and
• Elke Scheer

Beilstein J. Nanotechnol. 2024, 15, 360–366, doi:10.3762/bjnano.15.32

• , Supporting Information File 1). It results from Joule heating due to the high current density rather than from spin-related effects. Therefore, in order to visualize the spin-related features, the reduced differential resistance (dV/dI)red was obtained by subtracting the background curve measured at µ0H

• be of the order of 107 A/cm2, which is comparable to the reported values in trilayer [18][29] or multilayer [16][26] magnetic nanowires. For more details of the signatures of STT in the hysteresis loops and the estimation method of the current density see Supporting Information File 1. Ic+, Ic−, and

• magnetic fields. Supporting Information See Supporting Information File 1 for a detailed description of the setups of AAO template preparation and electrolytic nanowire deposition, an estimation of the thickness of NiCu and Cu layers and the current density in the measured device, a detailed description

Controllable physicochemical properties of WO_x thin films grown under glancing angle

• Rupam Mandal,
• Aparajita Mandal,
• Alapan Dutta,
• Rengasamy Sivakumar,
• Sanjeev Kumar Srivastava and
• Tapobrata Som

Beilstein J. Nanotechnol. 2024, 15, 350–359, doi:10.3762/bjnano.15.31

• variability in bandgap energies, we recall that the optical bandgap of this class of materials is a function of defect density and stoichiometric composition, which is mainly governed by the OV concentration within the films [39][40]. To probe any possible variation in OV concentration and stoichiometry

• revealed from the XRD studies, as-deposited NS-WOx films are amorphous in nature, whereas post-growth vacuum-annealed (at 673 K for 1 h) films show an amorphous-to-crystalline structural phase transition. XPS analysis confirms an increasing concentration of defect density in the form of oxygen vacancies

Comparative electron microscopy particle sizing of TiO₂ pigments: sample preparation and measurement

• Ralf Theissmann,
• Christopher Drury,
• Markus Rohe,
• Thomas Koch,
• Jochen Winkler and
• Petr Pikal

Beilstein J. Nanotechnol. 2024, 15, 317–332, doi:10.3762/bjnano.15.29

• -th particle, and ρ is the material density. The results presented in Table 5 and Figure 7 demonstrate that although each calculation method gives a slightly different SSA, they are very similar within a sample. The agreement between measured and calculated values is excellent; the measured values lie

• calculated as the diameter of a sphere of the same mass using the literature density of the material. The number of counts for each diameter were sorted into a histogram, similar to a particle size distribution from EM. In this way a number-based particle size distribution (number of particles as function of

Investigating structural and electronic properties of neutral zinc clusters: a G₀W₀ and G₀W₀Г₀⁽¹⁾ benchmark

• Sunila Bakhsh,
• Muhammad Khalid,
• Sameen Aslam,
• Muhammad Sohail,
• Muhammad Aamir Iqbal,
• Mujtaba Ikram and
• Kareem Morsy

Beilstein J. Nanotechnol. 2024, 15, 310–316, doi:10.3762/bjnano.15.28

• /bjnano.15.28 Abstract The structural and electronic properties of zinc clusters (Znn) for a size range of n = 2–15 are studied using density functional theory. The particle swarm optimization algorithm is employed to search the structure and to determine the ground-state structure of the neutral Zn

• clusters. The structural motifs are optimized using the density functional theory approach to ensure that the structures are fully relaxed. Results are compared with the literature to validate the accuracy of the prediction method. The binding energy per cluster is obtained and compared with the reported

• [4][5][6]. The majority of the research work on Zn clusters is focused on the vdW transition for the Zn clusters. For example, Wang et al. [7] investigated it by using the PW91 functional, which suggested that the transition starts from n = 8. Iokibe et al. [8] obtained a similar result using density

Exploring the relationships between physiochemical properties of nanoparticles and cell damage to combat cancer growth using simple periodic table-based descriptors

• Joyita Roy and
• Kunal Roy

Beilstein J. Nanotechnol. 2024, 15, 297–309, doi:10.3762/bjnano.15.27

• the production of antibodies [45]. The descriptor “Metal alpha” (αmetal) defines the core environment of the metal. This descriptor represents the ratio of the number of core electrons to the number of valence electrons. The Metal alpha descriptor describes the electron density of the metal. This

Ultrasensitive and ultrastretchable metal crack strain sensor based on helical polydimethylsiloxane

• Shangbi Chen,
• Dewen Liu,
• Weiwei Chen,
• Huajiang Chen,
• Jiawei Li and
• Jinfang Wang

Beilstein J. Nanotechnol. 2024, 15, 270–278, doi:10.3762/bjnano.15.25

• ion beam sputtering was obtained from Fuzhou Yingfei Xun Photoelectric Tech Co., Ltd, China; it possessed a density of 19.3 g·cm−3 and a conductivity of 4.52 × 107 S·m−1. Silver conductive adhesive, which was procured from Shenzhen Ausbond Co., LTD. (Guangdong, China), was employed to affix copper

Vinorelbine-loaded multifunctional magnetic nanoparticles as anticancer drug delivery systems: synthesis, characterization, and in vitro release study

• Zeynep Özcan and
• Afife Binnaz Hazar Yoruç

Beilstein J. Nanotechnol. 2024, 15, 256–269, doi:10.3762/bjnano.15.24

• the Fe3O4 NPs [45]. Various factors such as the crystal structure of the material, dimensions, morphology, and density of crystal defects significantly affect the magnetic properties [46]. The saturation magnetization (Ms) values of NPs measured at 298 K using a VSM are given in Figure 2c. The values

• aqueous solution, showing promising prospects for use in magnetically targeted therapy. Determination of photothermal stability and efficiency To evaluate the photothermal performance of the nanostructures, the NPs were irradiated with an 808 nm laser at a power density of 1 W/cm2 for 5 min. A slight

• effects. Determination of photothermal drug release To investigate the effect of NIR laser interaction on drug release, VNB/PDA/Fe3O4 NPs were irradiated with an 808 nm NIR laser at a power density of 1 W/cm2 for 5 min at different time intervals (15, 30, 45, 60, 120, 240, and 300 min). After exposing VNB