An advanced structural characterization of templated meso-macroporous carbon monoliths by small- and wide-angle scattering techniques

• Felix M. Badaczewski,
• Marc O. Loeh,
• Torben Pfaff,
• Dirk Wallacher,
• Daniel Clemens and
• Bernd M. Smarsly

Beilstein J. Nanotechnol. 2020, 11, 310–322, doi:10.3762/bjnano.11.23

• templates were infiltrated by two different carbon precursors, namely a mesophase pitch and a formaldehyde resole. The template was removed with hydrofluoric acid. Further information can be found in a recent study [41]. SANS data with a very good signal-to-noise ratio were acquired utilizing the V16

A review of demodulation techniques for multifrequency atomic force microscopy

• David M. Harcombe,
• Michael G. Ruppert and
• Andrew J. Fleming

Beilstein J. Nanotechnol. 2020, 11, 76–91, doi:10.3762/bjnano.11.8

• [28][31]. Motivated by improving high-speed MF-AFM demodulation capabilities, a multifrequency Kalman filter was developed [32]. It outperformed a commercially available lock-in amplifier in terms of both tracking bandwidth and noise performance. However, a major disadvantage of the Kalman filter is

• measurement noise. However, multifrequency AFM applications require an additional metric due to the large number of potentially closely spaced frequencies. For example, higher-harmonic imaging with single-frequency excitation results in small harmonic amplitudes that must be estimated in the presence of both

• noise and much larger fundamental and/or harmonic components [19][36]. The performance of the demodulator in this regard can be quantified by a metric herein referred to as the off-mode rejection (OMR). OMR is defined as the gain ratio between a modeled carrier frequency fi and another frequency fj as

Gold and silver dichroic nanocomposite in the quest for 3D printing the Lycurgus cup

• Lars Kool,
• Floris Dekker,
• Anton Bunschoten,
• Glen J. Smales,
• Brian R. Pauw,
• Aldrik H. Velders and
• Vittorio Saggiomo

Beilstein J. Nanotechnol. 2020, 11, 16–23, doi:10.3762/bjnano.11.2

• . The space between the start of the collimation until the detector is a continuous, uninterrupted vacuum to reduce background. Solid samples were fixed in place, within the evacuated sample chamber, whilst liquid samples were flowed through a low-noise cell equipped with SiN windows. The resulting data

Self-assembly of a terbium(III) 1D coordination polymer on mica

• Quentin Evrard,
• Giuseppe Cucinotta,
• Felix Houard,
• Guillaume Calvez,
• Yan Suffren,
• Carole Daiguebonne,
• Olivier Guillou,
• Andrea Caneschi,
• Matteo Mannini and
• Kevin Bernot

Beilstein J. Nanotechnol. 2019, 10, 2440–2448, doi:10.3762/bjnano.10.234

• it is. The static magnetic measurements of [Tb(hfac)3·2H2O]n and [Tb(hfac)3·2H2O]n@mica have been performed at 1.8 K using a conventional SQUID magnetometer (Figure S2, Supporting Information File 1). A very good signal-to-noise ratio is observed on the deposits, which validates the use of TbIII as a

Integration of sharp silicon nitride tips into high-speed SU8 cantilevers in a batch fabrication process

• Nahid Hosseini,
• Matthias Neuenschwander,
• Oliver Peric,
• Santiago H. Andany,
• Jonathan D. Adams and
• Georg E. Fantner

Beilstein J. Nanotechnol. 2019, 10, 2357–2363, doi:10.3762/bjnano.10.226

• results exclusively from the tip geometry, the noise suppression threshold is set at 100 pm which is superior to the measured image noise of 40 pm. Additionally, borders of the image are also excluded from the estimation to prevent edge artefacts. The inset of Figure 2a shows the result of the Gwyddion

A novel method to remove impulse noise from atomic force microscopy images based on Bayesian compressed sensing

• Yingxu Zhang,
• Yingzi Li,
• Zihang Song,
• Zhenyu Wang,
• Jianqiang Qian and
• Junen Yao

Beilstein J. Nanotechnol. 2019, 10, 2346–2356, doi:10.3762/bjnano.10.225

• , China School of Physics, Beihang University, Beijing 100191, China 10.3762/bjnano.10.225 Abstract A novel method based on Bayesian compressed sensing is proposed to remove impulse noise from atomic force microscopy (AFM) images. The image denoising problem is transformed into a compressed sensing

• matrices with some rows removed, are constructed by recording the position of the noise-free pixels. Third, the Bayesian compressed sensing reconstruction algorithm is applied to recover the image. Different from traditional compressed sensing reconstruction methods in AFM, each row of the AFM image is

• reconstructed separately in the proposed method, which will not reduce the quality of the reconstructed image. The denoising experiments are conducted to demonstrate that the proposed method can remove the impulse noise from AFM images while preserving the details of the image. Compared with other methods, the

Atomic force acoustic microscopy reveals the influence of substrate stiffness and topography on cell behavior

• Yan Liu,
• Li Li,
• Xing Chen,
• Ying Wang,
• Meng-Nan Liu,
• Jin Yan,
• Liang Cao,
• Lu Wang and
• Zuo-Bin Wang

Beilstein J. Nanotechnol. 2019, 10, 2329–2337, doi:10.3762/bjnano.10.223

• acoustic images depict more details of the real nanostructures at higher contrast and lower noise. Influences of substrate stiffness on L929 cell morphology and migration After substrate fabrication, we cultured L929 cells on the undeveloped SU-8 films of different stiffness and on a reference glass

Nitrogen-vacancy centers in diamond for nanoscale magnetic resonance imaging applications

• Alberto Boretti,
• Lorenzo Rosa,
• Jonathan Blackledge and
• Stefania Castelletto

Beilstein J. Nanotechnol. 2019, 10, 2128–2151, doi:10.3762/bjnano.10.207

• technique that can dramatically increase the signal-to-noise ratio (SNR) in traditional MRI. The method is being applied to small injectable endogenous molecules, which can be used to monitor transient in vivo metabolic events in real time. Among all methodologies, the emergence of hyperpolarized 13C

• magnetic textures (e.g., domain walls and skyrmions), spin waves in ferromagnets and superconducting vortices, and electrical noise currents in metals have been proved feasible with NV magnetometry. Probing static magnetic textures (i.e., the static spin configuration of a magnetic system) is crucial for

• magnetic power spectral density of a system and can be used as a magnetic noise sensor. This supplies a relationship to be set up between the magnetic noise spectrum to the spin and current fluctuations in a material. As such, it could be used to measure the thermal spin noise in low dimensional materials

Ion mobility and material transport on KBr in air as a function of the relative humidity

• Dominik J. Kirpal,
• Korbinian Pürckhauer,
• Alfred J. Weymouth and
• Franz J. Giessibl

Beilstein J. Nanotechnol. 2019, 10, 2084–2093, doi:10.3762/bjnano.10.203

• water film and the water meniscus that forms around the tip–sample contact cause damping forces on the probe, which result in higher noise [7]. The hydrophobicity of sapphire reduces the meniscus effect. The impact that hydrophobicity or hydrophilicity of the tip material can have is demonstrated by

Review of advanced sensor devices employing nanoarchitectonics concepts

• Katsuhiko Ariga,
• Tatsuyuki Makita,
• Masato Ito,
• Taizo Mori,
• Shun Watanabe and
• Jun Takeya

Beilstein J. Nanotechnol. 2019, 10, 2014–2030, doi:10.3762/bjnano.10.198

• -noise ratio in mercury ion detection with a detection limit of 0.01 ppb and a very short detection time constant of 3 s. This nanoarchitectonic design can maximize the intrinsic potential of black phosphorus and other materials. Sensors for physical conditions Not limited to particular chemicals, the

Optimization and performance of nitrogen-doped carbon dots as a color conversion layer for white-LED applications

• Tugrul Guner,
• Hurriyet Yuce,
• Didem Tascioglu,
• Eren Simsek,
• Umut Savaci,
• Aziz Genc,
• Servet Turan and
• Mustafa M. Demir

Beilstein J. Nanotechnol. 2019, 10, 2004–2013, doi:10.3762/bjnano.10.197

• ratio approaches unity while the overall emission reaches the lowest level, the resulting LER is reduced again to only 196 lm/W. The reason for this decrease may be the very low PL intensity (blue line in Figure 3a), which results in a low signal-to-noise ratio (S/N). The low S/N possibly causes an

Gold-coated plant virus as computed tomography imaging contrast agent

• Alaa A. A. Aljabali,
• Mazhar S. Al Zoubi,
• Khalid M. Al-Batanyeh,
• Ali Al-Radaideh,
• Mohammad A. Obeid,
• Abeer Al Sharabi,
• Walhan Alshaer,
• Bayan AbuFares,
• Tasnim Al-Zanati,
• Murtaza M. Tambuwala,
• Naveed Akbar and
• David J. Evans

Beilstein J. Nanotechnol. 2019, 10, 1983–1993, doi:10.3762/bjnano.10.195

• noise [27]. The accumulation of such concentration of the contrast agent is very difficult [28]. Therefore, the need to develop different forms on nanoparticles that are densely loaded with CT contrast agents for use in clinical settings will be of great value. The work reported here explores the

Magnetic properties of biofunctionalized iron oxide nanoparticles as magnetic resonance imaging contrast agents

• Natalia E. Gervits,
• Andrey A. Gippius,
• Alexey V. Tkachev,
• Evgeniy I. Demikhov,
• Sergey S. Starchikov,
• Igor S. Lyubutin,
• Alexander L. Vasiliev,
• Vladimir P. Chekhonin,
• Maxim A. Abakumov,
• Alevtina S. Semkina and
• Alexander G. Mazhuga

Beilstein J. Nanotechnol. 2019, 10, 1964–1972, doi:10.3762/bjnano.10.193

• core–shell structure iron oxide nanoparticles of the same size has already been described and calculated based on magnetic measurements. In the HSA-coated sample, we also succeeded to observe the ZF-NMR signal, despite the very low iron content per unit volume and the resulting low signal-to-noise

Long-term entrapment and temperature-controlled-release of SF₆ gas in metal–organic frameworks (MOFs)

• Hana Bunzen,
• Andreas Kalytta-Mewes,
• Leo van Wüllen and
• Dirk Volkmer

Beilstein J. Nanotechnol. 2019, 10, 1851–1859, doi:10.3762/bjnano.10.180

• . The “translation” directive included in GULP was employed for automatizing the SF6 linear transition task in a single run (setting: translate 0.0 0.0 1.0 200 noise 0.05), during which a geometry-constrained linear F–S–F fragment placed along the transition path (as part of SF6) was moved in steps of c

Toxicity and safety study of silver and gold nanoparticles functionalized with cysteine and glutathione

• Barbara Pem,
• Igor M. Pongrac,
• Lea Ulm,
• Ivan Pavičić,
• Valerije Vrček,
• Darija Domazet Jurašin,
• Marija Ljubojević,
• Adela Krivohlavek and
• Ivana Vinković Vrček

Beilstein J. Nanotechnol. 2019, 10, 1802–1817, doi:10.3762/bjnano.10.175

• washing steps of the cells after treatment and before the staining procedures as indicated in the cell protocols. In the case of flow cytometry experiments, the settings on the flow cytometer were carefully established taking into account testing of the correct NP concentration range, system noise, and

Novel hollow titanium dioxide nanospheres with antimicrobial activity against resistant bacteria

• Carol López de Dicastillo,
• Cristian Patiño,
• María José Galotto,
• Yesseny Vásquez-Martínez,
• Claudia Torrent,
• Daniela Alburquenque,
• Alejandro Pereira and
• Juan Escrig

Beilstein J. Nanotechnol. 2019, 10, 1716–1725, doi:10.3762/bjnano.10.167

•  5. SPVP diffraction patterns showed a broad band with peak at 2θ equal to 20.3° (solid line) corresponding to the amorphous nature of the PVP polymer [30][31][32][33]. Because they were independent of the samples, the peaks at approximately 11.2, 30 and 40° corresponded to the noise baseline due to

Subsurface imaging of flexible circuits via contact resonance atomic force microscopy

• Wenting Wang,
• Chengfu Ma,
• Yuhang Chen,
• Lei Zheng,
• Huarong Liu and
• Jiaru Chu

Beilstein J. Nanotechnol. 2019, 10, 1636–1647, doi:10.3762/bjnano.10.159

• the second eigenmodes, respectively. The cantilever stiffness and the free resonance frequency were calibrated by utilizing the thermal noise method while others were provided by the respective manufacturers. Multilayer contact model The axisymmetric indentation of a tip contacting with a multilayered

• frequency tracking by using the DART mode, especially when certain oscillation nonlinearity, spurious frequency peaks and large noise are presented in the contact resonance spectra. However, the frequency decrease with increasing normal force is generally not so significant, and the contrast between areas

• softer cantilever is generally better to achieve a higher subsurface contrast for the flexible circuit sample under nearly the same experimental conditions. Although the contrast with a softer cantilever is much better, the imaging noise is also higher as shown in Figure 4d. In practice, choosing an

Development of a new hybrid approach combining AFM and SEM for the nanoparticle dimensional metrology

• Loïc Crouzier,
• Alexandra Delvallée,
• Sébastien Ducourtieux,
• Laurent Devoille,
• Guillaume Noircler,
• Christian Ulysse,
• Olivier Taché,
• Elodie Barruet,
• Christophe Tromas and
• Nicolas Feltin

Beilstein J. Nanotechnol. 2019, 10, 1523–1536, doi:10.3762/bjnano.10.150

• too strong interactions with the sample and subsequent NP displacements. For vibration considerations, each instrument sits on a massive concrete block decoupled from the building. Furthermore, the AFM instrument is placed in an enclosure to protect it against acoustic noise and installed on an anti

• humidity and temperature are well controlled and stabilized (50 ± 5% relative humidity and 20 ± 0.15 °C for temperature). These precautions combined with the instrument performances make it possible to obtain low drifts and to carry out measurements with low noise. Basic measuring principle and data

• to take the full width at half maximum (FWHM) [19]. The profile FWHM depends on the accelerating voltage (or EHT) corresponding to the primary electron energy as shown in Figure 1. Above 4 kV, the signal-to-noise ratio, corresponding to the difference in grey level between the NP and the substrate

Energy distribution in an ensemble of nanoparticles and its consequences

• Dieter Vollath

Beilstein J. Nanotechnol. 2019, 10, 1452–1457, doi:10.3762/bjnano.10.143

• fit analysis. As the first example for determination of a particle size distribution based on the temperature profile of a physical process, the magnetic noise power of cobalt particles at a frequency of 100 Hz (according to Woods et al. [5]) was selected. In this example, 5 nm cobalt particles were

• scattered on a sheet of silicon oxide. Additionally, these particles were separated by an oleic acid coating of 2 nm. Woods et al. [5] determined the magnetic noise power as a function of temperature during the superparamagnetic transition. For this example, the experimental data obtained from 5 nm

• Figure 3, this assumption does not describe the course of the magnetic noise power properly. There is significant deviation at higher temperatures, representing larger particles. As fitting using a Weibull or a log-normal distribution did not lead to a satisfying result, an approximation using the sum of

Growth of lithium hydride thin films from solutions: Towards solution atomic layer deposition of lithiated films

• Ivan Kundrata,
• Karol Fröhlich,
• Lubomír Vančo,
• Matej Mičušík and
• Julien Bachmann

Beilstein J. Nanotechnol. 2019, 10, 1443–1451, doi:10.3762/bjnano.10.142

• original film was indeed LiH. Growth behaviour QCM used during the deposition showed a linearly decreasing trend in frequency, clearly distinguishable from background noise (Figure 8). Moreover, the periodical changes also correspond to the changing cycles. The sharp increase in frequency during water

Nanoscale spatial mapping of mechanical properties through dynamic atomic force microscopy

• Zahra Abooalizadeh,
• Leszek Josef Sudak and
• Philip Egberts

Beilstein J. Nanotechnol. 2019, 10, 1332–1347, doi:10.3762/bjnano.10.132

• (Figure 4c). While some contrast was observed in Figure 4d of the phase response, a closer examination of the line profile data in Figure 5b shows that no discernible peak or contrast can be detected from the uncovered or covered step edges in phase, as the noise or measured variation in the phase is the

Fabrication of phase masks from amorphous carbon thin films for electron-beam shaping

• Lukas Grünewald,
• Dagmar Gerthsen and
• Simon Hettler

Beilstein J. Nanotechnol. 2019, 10, 1290–1302, doi:10.3762/bjnano.10.128

• the central lobe [26]. In practice, this may result in a reduced signal-to-noise ratio and a compromise has to be found between a large kρ and sufficient intensity in the central lobe [25]. While the radial beam profile in form of a Bessel function is preserved upon propagation up to zmax, the

On the relaxation time of interacting superparamagnetic nanoparticles and implications for magnetic fluid hyperthermia

• Andrei Kuncser,
• Nicusor Iacob and
• Victor E. Kuncser

Beilstein J. Nanotechnol. 2019, 10, 1280–1289, doi:10.3762/bjnano.10.127

• ) from Figure 4a like dependencies. In this respect, a C++ program has been developed for automatically computing the number of magnetic switching events over a certain period (e.g., during 100 ns) from such time-dependent magnetization curves. Given a noise of 0.2 in Figure 4a like curves, any jump of

Molecular attachment to a microscope tip: inelastic tunneling, Kondo screening, and thermopower

• Rouzhaji Tuerhong,
• Mauro Boero and
• Jean-Pierre Bucher

Beilstein J. Nanotechnol. 2019, 10, 1243–1250, doi:10.3762/bjnano.10.124

• function of the gap resistance in Figure 4a, is a very sharp effect and corresponds to a sudden configurational change of the molecule in the STM gap. Simultaneously, a telegraphic noise appears at bias voltages larger than the side-peak threshold, which is often regarded as the signature of an unstable

Pure and mixed ordered monolayers of tetracyano-2,6-naphthoquinodimethane and hexathiapentacene on the Ag(100) surface

• Robert Harbers,
• Timo Heepenstrick,
• Dmitrii F. Perepichka and
• Moritz Sokolowski

Beilstein J. Nanotechnol. 2019, 10, 1188–1199, doi:10.3762/bjnano.10.118

• example. The four symmetry-equivalent domains are marked by A to D. The molecular rows are well visible. The domains exhibit local defects, mostly vacancies, where single molecules are missing. For this structure, STM images of good quality with a low level of noise were obtained easily. We interpret this