Surface functionalization of 3D-printed plastics via initiated chemical vapor deposition

• Christine Cheng and
• Malancha Gupta

Beilstein J. Nanotechnol. 2017, 8, 1629–1636, doi:10.3762/bjnano.8.162

• PLA and flat PPFDA due to surface roughness [34]. Penetration of polymer through the lattice was also confirmed by deposition on the silicon wafer piece underneath the lattice. We used Fourier transform infrared spectroscopy (FTIR) (Figure 2b) to compare the spectra of the PPFDA film deposited on the

Oxidative chemical vapor deposition of polyaniline thin films

• Yuriy Y. Smolin,
• Masoud Soroush and
• Kenneth K. S. Lau

Beilstein J. Nanotechnol. 2017, 8, 1266–1276, doi:10.3762/bjnano.8.128

• pentachloride as oxidant. Microscopy and spectroscopy indicate that oCVD processing conditions influence the PANI film chemistry, oxidation, and doping level. Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and X-ray photoelectron spectroscopy (XPS) indicate that a substrate

• components that might lead to unfavorable electrochemical properties. Thin film characterization As-deposited and washed PANI films were analyzed by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), and scanning electron microscopy (SEM). FTIR spectra were acquired using

Vapor-phase-synthesized fluoroacrylate polymer thin films: thermal stability and structural properties

• Paul Christian and
• Anna Maria Coclite

Beilstein J. Nanotechnol. 2017, 8, 933–942, doi:10.3762/bjnano.8.95

• Supporting Information File 1, while a full description of the setup can be found in a previous publication [17]. As substrates, silicon wafers with a native oxide layer (thickness 1.7 nm) were used after being cut into 2 × 2 cm2 pieces. Fourier transform infrared spectroscopy (FTIR) was performed on a

Optical and photocatalytic properties of TiO₂ nanoplumes

• Viviana Scuderi,
• Massimo Zimbone,
• Maria Miritello,
• Giuseppe Nicotra,
• Giuliana Impellizzeri and
• Vittorio Privitera

Beilstein J. Nanotechnol. 2017, 8, 190–195, doi:10.3762/bjnano.8.20

• reported in [21] indicated that the nanoplumes are made of TiO2. In addition, an accurate characterization of the nanoplumes performed by X-ray diffraction (XRD) measurements, X-ray Fourier transform infrared spectroscopy (FTIR), and photoelectron spectroscopy (XPS), revealed that after the etching the

A novel electrochemical nanobiosensor for the ultrasensitive and specific detection of femtomolar-level gastric cancer biomarker miRNA-106a

• Maryam Daneshpour,
• Kobra Omidfar and
• Hossein Ghanbarian

Beilstein J. Nanotechnol. 2016, 7, 2023–2036, doi:10.3762/bjnano.7.193

• , Freescale) analysis. In order to study structural and elemental properties, X-ray diffraction (XRD) (Philips, pw 1800, Netherlands) and energy-dispersive X-ray diffraction (EDX) were carried out. These NPs were also characterized using Fourier transform infrared spectroscopy (FTIR) to study the chemical

Organoclay hybrid materials as precursors of porous ZnO/silica-clay heterostructures for photocatalytic applications

• Marwa Akkari,
• Pilar Aranda,
• Abdessalem Ben Haj Amara and
• Eduardo Ruiz-Hitzky

Beilstein J. Nanotechnol. 2016, 7, 1971–1982, doi:10.3762/bjnano.7.188

• diffractometer using monochromatic Cu Kα radiation, scanning from 2 to 70° in 2θ degrees with steps of 0.02 degrees. The average size of the crystallites was calculated by using the Debye–Scherrer formula [33]. Fourier transform infrared spectroscopy (FTIR) was performed in a Bruker IFS 260 66v/S

Ammonia gas sensors based on In₂O₃/PANI hetero-nanofibers operating at room temperature

• Qingxin Nie,
• Zengyuan Pang,
• Hangyi Lu,
• Yibing Cai and
• Qufu Wei

Beilstein J. Nanotechnol. 2016, 7, 1312–1321, doi:10.3762/bjnano.7.122

• morphology of In(NO3)3/PVP, In2O3/PANI composite nanofibers and pure PANI were investigated by scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), transmission electron microscopy (TEM) and current–voltage (I–V) measurements. The gas sensing properties

Multiwalled carbon nanotube hybrids as MRI contrast agents

• Nikodem Kuźnik and
• Mateusz M. Tomczyk

Beilstein J. Nanotechnol. 2016, 7, 1086–1103, doi:10.3762/bjnano.7.102

• form (i.e., γ-Fe2O3 and Fe3O4 in the hybrids with SPIO). Fourier transform infrared spectroscopy (FTIR) and thermogravimetric analysis (TGA), supported again by TEM, were applied to monitor the effects of wrapping with organic moieties. Infrared spectroscopy has commonly been used to follow the

Bacteriorhodopsin–ZnO hybrid as a potential sensing element for low-temperature detection of ethanol vapour

• Saurav Kumar,
• Sudeshna Bagchi,
• Senthil Prasad,
• Anupma Sharma,
• Ritesh Kumar,
• Rishemjit Kaur,
• Jagvir Singh and
• Amol P. Bhondekar

Beilstein J. Nanotechnol. 2016, 7, 501–510, doi:10.3762/bjnano.7.44

• nonhybrid structures, as is evident from Figure 2c,d. The structural and optical properties of ZnO-TF, ZnO-NR and their hybrid structures were assessed using UV–vis spectroscopy, photoluminescence spectroscopy (PL), Raman spectroscopy and Fourier transform infrared spectroscopy (FTIR). Figure 3 shows the

Plasma fluorination of vertically aligned carbon nanotubes: functionalization and thermal stability

• Claudia Struzzi,
• Mattia Scardamaglia,
• Axel Hemberg,
• Luca Petaccia,
• Jean-François Colomer,
• Rony Snyders and
• Carla Bittencourt

Beilstein J. Nanotechnol. 2015, 6, 2263–2271, doi:10.3762/bjnano.6.232

• ][12][13][14][15]. A key characteristic of fluorine-based species is the different chemical interactions in carbon–fluorine bond formation [16][17]. Primarily covalent bonding occurs as a result of the plasma process, which is easily verified by different techniques such as Fourier transform infrared

• spectroscopy (FTIR), Raman spectroscopy and X-ray photoelectron spectroscopy (XPS) [10][18][19]. Although a large number of fluorination strategies and characterization routes have been reported, the choice of the precursor gas is a crucial issue that should not be underestimated due to the risk of

Temperature-dependent breakdown of hydrogen peroxide-treated ZnO and TiO₂ nanoparticle agglomerates

• Sinan Sabuncu and
• Mustafa Çulha

Beilstein J. Nanotechnol. 2015, 6, 1897–1903, doi:10.3762/bjnano.6.193

• stored at room temperature. Fourier transform infrared spectroscopy (FTIR) measurements FTIR analysis was performed using a Thermo Scientific, Nicolet iS50 FTIR instrument (Massachusetts, USA) in attenuated total reflectance mode with a diamond plate and ZnSe lens. The samples were dried at 90 °C on a

Radiation losses in the microwave K_u band in magneto-electric nanocomposites

• Talwinder Kaur,
• Sachin Kumar,
• Jyoti Sharma and
• A. K. Srivastava

Beilstein J. Nanotechnol. 2015, 6, 1700–1707, doi:10.3762/bjnano.6.173

• structural, magnetic and radiation absorbance properties of synthesized compounds have been investigated by using X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), electron spin resonance spectroscopy (ESR), transmission electron microscopy (TEM), vibrating sample magnetometry (VSM

Synthesis, characterization and in vitro biocompatibility study of Au/TMC/Fe₃O₄ nanocomposites as a promising, nontoxic system for biomedical applications

• Hanieh Shirazi,
• Maryam Daneshpour,
• Soheila Kashanian and
• Kobra Omidfar

Beilstein J. Nanotechnol. 2015, 6, 1677–1689, doi:10.3762/bjnano.6.170

• , chitosan/TMC-containing, magnetic nanoparticles and their respective characterization using transmission electron microscopy (TEM), ultraviolet–visible absorption spectroscopy (UV–vis), X-ray diffraction spectroscopy (XRD), Fourier transform infrared spectroscopy (FTIR), a vibrating sample magnetometer

Structural, optical, opto-thermal and thermal properties of ZnS–PVA nanofluids synthesized through a radiolytic approach

• Alireza Kharazmi,
• Nastaran Faraji,
• Roslina Mat Hussin,
• Elias Saion,
• W. Mahmood Mat Yunus and
• Kasra Behzad

Beilstein J. Nanotechnol. 2015, 6, 529–536, doi:10.3762/bjnano.6.55

• investigate the physical and chemical properties of the samples. Fourier transform infrared spectroscopy (FTIR) was used to determine the chemical structure and bonding conditions of the final products, transmission electron microscopy (TEM) for determining the shape morphology and average particle size

• effusivity of the samples, from which, for the first time, the values of specific heat and thermal diffusivity of the samples were then calculated. Keywords: Fourier transform infrared spectroscopy (FTIR); specific heat; thermal conductivity; thermal effusivity; ZnS nanoparticles; Introduction Over the

Conformal SiO₂ coating of sub-100 nm diameter channels of polycarbonate etched ion-track channels by atomic layer deposition

• Nicolas Sobel,
• Christian Hess,
• Manuela Lukas,
• Anne Spende,
• Bernd Stühn,
• M. E. Toimil-Molares and
• Christina Trautmann

Beilstein J. Nanotechnol. 2015, 6, 472–479, doi:10.3762/bjnano.6.48

• photoelectron spectroscopy (XPS) and Fourier-transform infrared spectroscopy (FTIR). The hydrophilicity of SiO2-coated PC membranes was tested by contact angle measurements. Experimental Figure 1 displays schematically the three main steps involved in the fabrication of SiO2 coated track-etched membranes. These

Tunable white light emission by variation of composition and defects of electrospun Al₂O₃–SiO₂ nanofibers

• Jinyuan Zhou,
• Gengzhi Sun,
• Hao Zhao,
• Xiaojun Pan,
• Zhenxing Zhang,
• Yujun Fu,
• Yanzhe Mao and
• Erqing Xie

Beilstein J. Nanotechnol. 2015, 6, 313–320, doi:10.3762/bjnano.6.29

• -SEM, Hitachi S4800), transmission electron microscopy (TEM, JEM 3000F, JOEL), Fourier transform infrared spectroscopy (FTIR, IFS66v/S, 400–4000 cm−1), and fluorescence spectroscopy (RF-540, Shi-Madzu) using a 15 mW, 325 nm, He–Cd laser (spot size of about 1 mm) in addition to a spectroscopy with a FLS

Size-dependent density of zirconia nanoparticles

• Agnieszka Opalinska,
• Iwona Malka,
• Wojciech Dzwolak,
• Tadeusz Chudoba,
• Adam Presz and
• Witold Lojkowski

Beilstein J. Nanotechnol. 2015, 6, 27–35, doi:10.3762/bjnano.6.4

• correlated with a larger contribution of the low density surface layer to the average density. To prove the existence of such a layer, the material was synthesized using 50% heavy water. Fourier transform infrared spectroscopy (FTIR) permitted the identification of the –OD groups created during synthesis. It

Enhanced photocatalytic hydrogen evolution by combining water soluble graphene with cobalt salts

• Jing Wang,
• Ke Feng,
• Hui-Hui Zhang,
• Bin Chen,
• Zhi-Jun Li,
• Qing-Yuan Meng,
• Li-Ping Zhang,
• Chen-Ho Tung and
• Li-Zhu Wu

Beilstein J. Nanotechnol. 2014, 5, 1167–1174, doi:10.3762/bjnano.5.128

• initial concentration of cobalt salts added. And hydrogen constantly evolves even after 20 h irradiation. Results and Discussion Fourier transform infrared spectroscopy (FTIR) is employed to characterize GO and G-SO3. As shown in Figure 1, compared to GO, G-SO3 has typical absorptions at 1177, 1123 and

Nanodiamond-DGEA peptide conjugates for enhanced delivery of doxorubicin to prostate cancer

• Amanee D Salaam,
• Patrick Hwang,
• Roberus McIntosh,
• Hadiyah N Green,
• Ho-Wook Jun and
• Derrick Dean

Beilstein J. Nanotechnol. 2014, 5, 937–945, doi:10.3762/bjnano.5.107

• -DGEA conjugates and ND-DGEA+DOX system were characterized to confirm successful bonding of ND to DGEA and adsorption of DOX, respectively. Transmission electron microscopy (TEM, FEI Tecnai T12) was used to qualitatively confirm the conjugation and adsorption. Fourier transform infrared spectroscopy

• (FTIR, Nicolet Thermo Scientific) was used to confirm the chemical bonding of ND to DGEA and the presence of DOX on the ND-DGEA surface; spectra were collected from 400–3500 cm−1 at ambient temperature in attenuated total reflectance mode (ATR) with 64 scans per sample. A Zeta-sizer Nano ZS (Malvern

A catechol biosensor based on electrospun carbon nanofibers

• Dawei Li,
• Zengyuan Pang,
• Xiaodong Chen,
• Lei Luo,
• Yibing Cai and
• Qufu Wei

Beilstein J. Nanotechnol. 2014, 5, 346–354, doi:10.3762/bjnano.5.39

• carbonization technique. And a polyphenol biosensor was fabricated by blending the obtained CNFs with laccase and Nafion. Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR) and field emission scanning electron microscope (FE-SEM) were, respectively, employed to investigate the structures and

Nano-FTIR chemical mapping of minerals in biological materials

• Sergiu Amarie,
• Paul Zaslansky,
• Yusuke Kajihara,
• Erika Griesshaber,
• Wolfgang W. Schmahl and
• Fritz Keilmann

Beilstein J. Nanotechnol. 2012, 3, 312–323, doi:10.3762/bjnano.3.35

• osteopathies. Keywords: biomineralization; chemical mapping; infrared spectroscopy; nanocrystals; optical near-field microscopy; Introduction Fourier-transform infrared spectroscopy (FTIR) [1] is a standard tool in chemical analysis. It can identify virtually any substance through the "fingerprint" of the