Ultrathin water layers on mannosylated gold nanoparticles

• Maiara A. Iriarte Alonso,
• Jorge H. Melillo,
• Silvina Cerveny,
• Yujin Tong and
• Alexander M. Bittner

Beilstein J. Nanotechnol. 2025, 16, 2183–2198, doi:10.3762/bjnano.16.151

• overnight sample incubation to reach 90 ± 5% RH, corresponding to very wet climate or air during precipitation. In addition, we refer to “hydrophilic conditions” in AFM for hydrophilic surfaces (APDMES silicon) scanned by a silicon tip. We found a vertical resolution (∆z) of 0.04 nm and a surface roughness

Exploring the potential of polymers: advancements in oral nanocarrier technology

• Rousilândia de Araujo Silva,
• Igor Eduardo Silva Arruda,
• Luise Lopes Chaves,
• Mônica Felts de La Roca Soares and
• Jose Lamartine Soares Sobrinho

Beilstein J. Nanotechnol. 2025, 16, 1751–1793, doi:10.3762/bjnano.16.122

• commonly used methods for the preparation of PNs employing preformed polymers. These methods typically begin with the formulation of an emulsifying system, a step common to all techniques, followed by the formation of NPs through a process that varies depending on the method, such as solvent precipitation

• specific polymer classes, depending on their physicochemical properties and solubility behavior. Nanoprecipitation is frequently employed for synthetic polymers such as PLGA and PCL, which are soluble in organic solvents and undergo controlled precipitation in aqueous media, enabling efficient

• other and produced through polymerization reactions such as addition, condensation, ring-opening polymerization, emulsion, precipitation, and others [57]. Monomers determine the decomposition products of polymers in the body and, consequently, their toxicity and biocompatibility. This is why synthesis

Prospects of nanotechnology and natural products for cancer and immunotherapy

• Jan Filipe Andrade Santos,
• Marcela Bernardes Brasileiro,
• Pamela Danielle Cavalcante Barreto,
• Ligiane Aranha Rocha and
• José Adão Carvalho Nascimento Júnior

Beilstein J. Nanotechnol. 2025, 16, 1644–1667, doi:10.3762/bjnano.16.116

• nanoparticles were obtained by precipitation and freeze-drying and were analyzed by HPLC and DLS. Additionally, the in vivo studies performed in a mice model with breast cancer tumor (4T1 cell) showed that the drug exhibits a level of biosafety while reaching 44% tumor inhibition [75]. Polysaccharide

Nanotechnology-based approaches for the removal of microplastics from wastewater: a comprehensive review

• Nayanathara O Sanjeev,
• Manjunath Singanodi Vallabha and
• Rebekah Rubidha Lisha Rabi

Beilstein J. Nanotechnol. 2025, 16, 1607–1632, doi:10.3762/bjnano.16.114

• . Common chemical treatment techniques include coagulation, flocculation, precipitation, and electrocoagulation [18]. Even though both physical and chemical methods are found to be effective in the removal of MPs, they pose several challenges on the remediation of MPs, such as blocking pores and surfaces

• -precipitation involves solvent displacement method, where acetone, ethanol, hexane are some of the solvents used [75]. In electrospinning, nanofibers are generated [76]. In parallel, green synthesis utilises biological entities such as plant extracts or microorganisms as reducing agents to produce eco-friendly

Photocatalytic degradation of ofloxacin in water assisted by TiO₂ nanowires on carbon cloth: contributions of H₂O₂ addition and substrate absorbability

• Iram Hussain,
• Lisha Zhang,
• Zhizhen Ye and
• Jin-Ming Wu

Beilstein J. Nanotechnol. 2025, 16, 1567–1579, doi:10.3762/bjnano.16.111

• deposition, electrophoretic deposition, and electrochemical deposition are extensively utilized for the synthesis of TiO2 nanowire arrays, owing to their advantageous physical properties and varied applications [14][15]. Our previous study accomplished the precipitation of TiO2 nanowire arrays, with

• and deionized water alternately in an ultrasonic bath, followed by drying at 60 °C. After that, it was immersed in 200 mL of a 30 wt % H2O2 solution, containing 60 mg of melamine, 4 mL of 65 wt % HNO3, and 1 g of titanium sponge, at 80 °C for 24 h to facilitate the precipitation of hydrogen titanate

• carbon cloth substrate via a heterogeneous nucleation mechanism [19][20]. Figure S1 in Supporting Information File 1 shows the homogeneous precipitation of hydrogen titanate nanowires on the carbon cloth. Subsequent calcination in air at 450 °C transformed the hydrogen titanate structures into anatase

Dendrimer-modified carbon nanotubes for the removal and recovery of heavy metal ions from water

• Thao Quynh Ngan Tran,
• Huu Trung Nguyen,
• Subodh Kumar and
• Xuan Thang Cao

Beilstein J. Nanotechnol. 2025, 16, 1522–1532, doi:10.3762/bjnano.16.107

• metal contamination. Consequently, the efficient removal of heavy metal ions remains a critical research challenge. Various methods have been employed including membrane filtration [1], flocculation [2], adsorption [3][4], precipitation [5], electrolytic removal [6], ion exchange [7], reduction [8], and

Laser processing in liquids: insights into nanocolloid generation and thin film integration for energy, photonic, and sensing applications

• Akshana Parameswaran Sreekala,
• Pooja Raveendran Nair,
• Jithin Kundalam Kadavath,
• Bindu Krishnan,
• David Avellaneda Avellaneda,
• M. R. Anantharaman and
• Sadasivan Shaji

Beilstein J. Nanotechnol. 2025, 16, 1428–1498, doi:10.3762/bjnano.16.104

The role of biochar in combating microplastic pollution: a bibliometric analysis in environmental contexts

• Tuan Minh Truong Dang,
• Thao Thu Thi Huynh,
• Guo-Ping Chang-Chien and
• Ha Manh Bui

Beilstein J. Nanotechnol. 2025, 16, 1401–1416, doi:10.3762/bjnano.16.102

• derived from hardwood using an open-fire stove exhibited a relatively low surface area of 292.8 m2·g−1. Modified biochar synthesis strategies aim to enhance adsorption capacity while maintaining stable pore volume. For instance, magnetic biochar (MBC) synthesized from peanut shells using co-precipitation

Enhancing the therapeutical potential of metalloantibiotics using nano-based delivery systems

• Alejandro Llamedo,
• Marina Cano,
• Raquel G. Soengas and
• Francisco J. García-Alonso

Beilstein J. Nanotechnol. 2025, 16, 1350–1366, doi:10.3762/bjnano.16.98

• been suggested that the antibacterial action is strongly related to bioavailability and stability. In fact, the poor water solubility, the degradation (precipitation) by chloride in the bloodstream, the interaction with sulfur-containing proteins, and the rapid clearance by macrophages are the main

Crystalline and amorphous structure selectivity of ignoble high-entropy alloy nanoparticles during laser ablation in organic liquids is set by pulse duration

• Robert Stuckert,
• Felix Pohl,
• Oleg Prymak,
• Ulrich Schürmann,
• Christoph Rehbock,
• Lorenz Kienle and
• Stephan Barcikowski

Beilstein J. Nanotechnol. 2025, 16, 1141–1159, doi:10.3762/bjnano.16.84

• structure as lower cooling rates would lead to the precipitation of carbon species to the surface of the particles, which was discussed by Abdelhafiz et al. in the context of high-entropy oxide materials via CTS [100]. Of course, carbon diffusion into the particle core after its cooldown may not be excluded

Fabrication of metal complex phthalocyanine and porphyrin nanoparticle aqueous colloids by pulsed laser fragmentation in liquid and their potential application to a photosensitizer for photodynamic therapy

• Taisei Himeda,
• Risako Kunitomi,
• Ryosuke Nabeya,
• Tamotsu Zako and
• Tsuyoshi Asahi

Beilstein J. Nanotechnol. 2025, 16, 1088–1096, doi:10.3762/bjnano.16.80

• any precipitation for longer than one week. The aqueous F-127 solution at 0.1 wt % concentration, which is about one tenth of the critical micelle concentration, was enough to fabricate nanoparticles with excellent dispersion stability and high production efficiency. We examined the photosensitized

• by nanosecond laser fragmentation in Pluronic F-127 (0.1 wt %) aqueous solution. The MPc nanoparticles exhibited a strong absorption band in NIR. The prepared nanoparticles with a hydrodynamic diameter of about 60 nm dispersed stably in PBS and cell culture media without any precipitation over the

• squares), and the pure colloids with F-127 added (red circles) evaluated by absorption measurements. A decrease in absorbance at 620 nm means precipitation of the nanoparticles. (a) Absorption spectra of the CoPc colloid (0.005 wt %) fabricated in F-127 solution of different concentrations (0, 0.1, and 5

Supramolecular hydration structure of graphene-based hydrogels: density functional theory, green chemistry and interface application

• Hon Nhien Le,
• Duy Khanh Nguyen,
• Minh Triet Dang,
• Huyen Trinh Nguyen,
• Thi Bang Tam Dao,
• Trung Do Nguyen,
• Chi Nhan Ha Thuc and
• Van Hieu Le

Beilstein J. Nanotechnol. 2025, 16, 806–822, doi:10.3762/bjnano.16.61

• then sonicated for 15 min. A volume of 500 mL of the as-prepared GO/Zn2+ dispersion was dropped into the 500 mL SG dispersion. The mixture was agitated for 15 min and sonicated for 15 min. Then, the reaction was adjusted to pH 10 using ammonia solution for Zn(OH)2 precipitation and kept stirring for 1

• exhibited sharp characteristic peaks of the Zn(OH)2 crystal at 2θ = 20.2°, 20.94°, 25.07°, 27.23°, 27.83°, and 32.97° [40][41][42]. Zinc hydroxide nanocrystals (ZH) were formed on the nanocomposite during the precipitation by alkaline ammonia in the synthesis process (see Methods section). The constituents

Morphology and properties of pyrite nanoparticles obtained by pulsed laser ablation in liquid and thin films for photodetection

• Akshana Parameswaran Sreekala,
• Bindu Krishnan,
• Rene Fabian Cienfuegos Pelaes,
• David Avellaneda Avellaneda,
• Josué Amílcar Aguilar-Martínez and
• Sadasivan Shaji

Beilstein J. Nanotechnol. 2025, 16, 785–805, doi:10.3762/bjnano.16.60

• NPs obtained in acetone is comparable to the reported work on Ag, we observed precipitation within a few minutes. The precipitation of FeS2 NPs in acetone can be attributed either to the relatively low viscosity (0.306 mPa·s) of acetone, which means that NPs have higher mobility, increasing the

• or steric stabilization, leading to agglomeration and precipitation. This behavior contrasts with metallic Ag NPs, which remain stable in acetone due to stronger electrical double layers and surface charge. According to the literature, in the case of nanosecond (ns) laser pulses, the laser energy can

Aprepitant-loaded solid lipid nanoparticles: a novel approach to enhance oral bioavailability

• Mazhar Hussain,
• Muhammad Farooq,
• Muhammad Asad Saeed,
• Muhammad Ijaz,
• Sherjeel Adnan,
• Zeeshan Masood,
• Muhammad Waqas,
• Wafa Ishaq and
• Nabeela Ameer

Beilstein J. Nanotechnol. 2025, 16, 652–663, doi:10.3762/bjnano.16.50

• analysis. APT-loaded SLNs were prepared by the precipitation method and characterized by physicochemical studies including particle size and zeta potential measurements, drug content, encapsulation efficiency and solubility studies, Fourier-transform infrared spectroscopy (FTIR), scanning electron

• as hot homogenization, cold homogenization, and solvent evaporation are used to prepare SLNs, but precipitation is the most compatible method for compound, polymer, and lipid. The precipitation method consists of dissolving the lipid with organic solvents and adding water to cause supersaturation of

• solid lipids in the mixture, which leads to precipitation of SLNs [12]. The precipitation method has the advantage of simple, rapid, reproducible, cost-effective, and easy handling for producing SLNs with good scale-up potential [13]. In the present study, we prepared SLNs containing APT with better

Quantification of lead through rod-shaped silver-doped zinc oxide nanoparticles using an electrochemical approach

• Ravinder Lamba,
• Gaurav Bhanjana,
• Neeraj Dilbaghi,
• Vivek Gupta and
• Sandeep Kumar

Beilstein J. Nanotechnol. 2025, 16, 422–434, doi:10.3762/bjnano.16.33

• they were fabricated using a low-temperature co-precipitation method. The resulting Ag@ZnO NRs had good optical properties, nanorod morphologies, and high crystallinity with no impurities. Technological advancements are leading people to use lightweight electronics and affordable sensors

• experiments. Conclusion In conclusion, a low-temperature co-precipitation technique was utilized to yield highly crystalline nanorods of ZnO doped with Ag. A variety of techniques were employed to analyze the physical and chemical characteristics of as-synthesized Ag@ZnO NRs. The results demonstrate that the

Engineered PEG–PCL nanoparticles enable sensitive and selective detection of sodium dodecyl sulfate: a qualitative and quantitative analysis

• Soni Prajapati and
• Ranjana Singh

Beilstein J. Nanotechnol. 2025, 16, 385–396, doi:10.3762/bjnano.16.29

• precipitation step is essential for purifying the nanoparticles and achieving a stable, solid-state product that can be easily collected and dried. Finally, the synthesized PEG–PCL NPs are characterized to assess their size and uniformity. Dynamic light scattering (DLS) techniques measure the average particle

Fabrication and evaluation of BerNPs regarding the growth and development of Streptococcus mutans

• Tuyen Huu Nguyen,
• Hong Thanh Pham,
• Kieu Kim Thanh Nguyen,
• Loan Hong Ngo,
• Anh Ngoc Tuan Mai,
• Thu Hoang Anh Lam,
• Ngan Thi Kim Phan,
• Dung Tien Pham,
• Duong Thuy Hoang,
• Thuc Dong Nguyen and
• Lien Thi Xuan Truong

Beilstein J. Nanotechnol. 2025, 16, 308–315, doi:10.3762/bjnano.16.23

• inhibitory activity against pathogenic bacteria have been reported. In 2022, Nguyen et al. fabricated berberine nanoparticles (BerNPs) by antisolvent precipitation (ASP) using glycerol as a safe organic solvent and evaluated their antibacterial activity on S. aureus and E. coli O157:H7 [12]. Additionally

• demonstrated superior efficiency in producing nanoscale berberine. Tran et al. employed the ball milling technique to produce BerNPs, achieving a particle size of 570.7 nm [23]. Piri et al. utilized the anti-solvent precipitation method, yielding BerNPs with an average particle size of 75 nm [24]. BerNPs were

• . mutans was reported with a MIC of 1024 µg/mL and a MBC of 2054 µg/mL [29]. Antibacterial activities of berberine and BerNPs have been documented by various researchers. Nguyen et al. indicated that BerNPs prepared via the antisolvent precipitation method achieved MBC values of 2 and 5 mg/mL against

Emerging strategies in the sustainable removal of antibiotics using semiconductor-based photocatalysts

• Yunus Ahmed,
• Keya Rani Dutta,
• Parul Akhtar,
• Md. Arif Hossen,
• Md. Jahangir Alam,
• Obaid A. Alharbi,
• Hamad AlMohamadi and
• Abdul Wahab Mohammad

Beilstein J. Nanotechnol. 2025, 16, 264–285, doi:10.3762/bjnano.16.21

• advanced methods, including sol–gel, hydrothermal, solvothermal, precipitation and template-assisted techniques [53]. The synthesis method chosen often depends on factors such as the desired crystal structure, particle size, surface area, and photocatalytic activity required for the specific application

Preferential enrichment and extraction of laser-synthesized nanoparticles in organic phases

• Theo Fromme,
• Maximilian L. Spiekermann,
• Florian Lehmann,
• Stephan Barcikowski,
• Thomas Seidensticker and
• Sven Reichenberger

Beilstein J. Nanotechnol. 2025, 16, 254–263, doi:10.3762/bjnano.16.20

• higher cooling rates (e.g., in an ice bath) would result in precipitation of the nanoparticle material in the interlayer of the two phases. After cooling to the biphasic state, the extinction of the gained colloidal phases was investigated by UV–vis measurements (Supporting Information File 1, Figure S1

• chosen to avoid precipitation of the nanoparticles at the phase boundaries. Heating cycles were performed in a 50 mL vessel, which was heated up to 85 °C with a temperature ramp of 5 °C/min and temperature was held for 15 min. For the cooling of the colloid to room temperature, the heating was turned off

Heterogeneous reactions in a HFCVD reactor: simulation using a 2D model

• Xochitl Aleyda Morán Martínez,
• José Alberto Luna López,
• Zaira Jocelyn Hernández Simón,
• Gabriel Omar Mendoza Conde,
• José Álvaro David Hernández de Luz and
• Godofredo García Salgado

Beilstein J. Nanotechnol. 2024, 15, 1627–1638, doi:10.3762/bjnano.15.128

• 700 K, the supersaturation is high and the nucleation is homogeneous in the process, leading to the precipitation of solid particles on the substrate and powder formation [23]. SiOx powders are obtained in the HFCVD reactor when the distance between the filaments and the source is less than 6 mm

Facile synthesis of size-tunable L-carnosine-capped silver nanoparticles and their role in metal ion sensing and catalytic degradation of p-nitrophenol

• Akash Kumar,
• Ridhima Chadha,
• Abhishek Das,
• Nandita Maiti and
• Rayavarapu Raja Gopal

Beilstein J. Nanotechnol. 2024, 15, 1576–1592, doi:10.3762/bjnano.15.124

• ), 1 mL AgNO3 (0.01 M), and 2 mL NaBH4 (0.001 M). The term “ʟ-car-AgNPs” is used throughout the article to refer to the synthesized silver nanoparticles collectively. Furthermore, nanopowders of the samples were prepared using 1 M NaCl solution via the precipitation method, and the obtained precipitate

• , respectively. The insets of Figure 4d and Figure 4e indicate 2.13 and 3.2 wt % of silver in ʟ-car-AgNP1 and ʟ-car-AgNP2, respectively. However, apart from silver, high fractions of sodium and chlorine were observed. This is probably due to the preparation of the nanopowders using the precipitation method with

Green synthesis of silver nanoparticles derived from algae and their larvicidal properties to control Aedes aegypti

• Matheus Alves Siqueira de Assunção,
• Douglas Dourado,
• Daiane Rodrigues dos Santos,
• Gabriel Bezerra Faierstein,
• Mara Elga Medeiros Braga,
• Severino Alves Junior,
• Rosângela Maria Rodrigues Barbosa,
• Herminio José Cipriano de Sousa and
• Fábio Rocha Formiga

Beilstein J. Nanotechnol. 2024, 15, 1566–1575, doi:10.3762/bjnano.15.123

• processes that involve reducing the size of bulk silver materials to the atomic size of the AgNPs [25]. Bottom-up AgNPs are synthesized via precursor salt reactions that lead to the formation of AgNPs [26] including condensation, precipitation, and pyrolysis [27]. AgNPs can be synthesized using physical

Interaction of graphene oxide with tannic acid: computational modeling and toxicity mitigation in C. elegans

• Romana Petry,
• James M. de Almeida,
• Francine Côa,
• Felipe Crasto de Lima,
• Diego Stéfani T. Martinez and
• Adalberto Fazzio

Beilstein J. Nanotechnol. 2024, 15, 1297–1311, doi:10.3762/bjnano.15.105

• directly affects delivered dose, internalization, and biodistribution in organisms. In the EPA medium, GO exhibited aggregation and precipitation at concentrations of 5.0 and 10 mg·L−1, respectively, a phenomenon attributable to the screening effect of salt ions diminishing the repulsive forces between GO

• sheets. TA did not improve the stability of these samples. After the 24 h, only the suspensions of 1 mg·L−1 of GO did not exhibit visual precipitation (Supporting Information File 1, Figure S1a). The results of dynamic light scattering (DLS) measurements presented in Table S1 (Supporting Information File

•  1) confirm the aggregation and the subsequent precipitation of GO in the EPA medium; it is noticeable that hydrodynamic diameters rapidly increase in this medium. Although higher TA concentrations slow down aggregation and lead to smaller hydrodynamic diameters after 3 h, after 24 h the samples were

Mn-doped ZnO nanopowders prepared by sol–gel and microwave-assisted sol–gel methods and their photocatalytic properties

• Cristina Maria Vlăduț,
• Crina Anastasescu,
• Silviu Preda,
• Oana Catalina Mocioiu,
• Simona Petrescu,
• Jeanina Pandele-Cusu,
• Dana Culita,
• Veronica Bratan,
• Ioan Balint and
• Maria Zaharescu

Beilstein J. Nanotechnol. 2024, 15, 1283–1296, doi:10.3762/bjnano.15.104

• of amorphous oxide nanopowders, the precipitation of nanocrystalline metal oxides, and the drying and thermal treatment of oxide films [23]. However, there has been comparatively less focus on studying chemical reactions in sol–gel solutions under microwave irradiation [24][25][26][27]. Numerous

A low-kiloelectronvolt focused ion beam strategy for processing low-thermal-conductance materials with nanoampere currents

• Annalena Wolff,
• Nico Klingner,
• William Thompson,
• Yinghong Zhou,
• Jinying Lin and
• Yin Xiao

Beilstein J. Nanotechnol. 2024, 15, 1197–1207, doi:10.3762/bjnano.15.97

• was purified by NaCl precipitation at acidic and then neutral pH. Collagen sponges were prepared using purified type-I collagen, glutaraldehyde fixation, and freeze drying, also as previously described [17]. Stopping and range of ions in matter (SRIM) simulations of 5 keV gallium ions in skin The