Continuous flow synthesis of azobenzenes via Baeyer–Mills reaction

Jan H. Griwatz, Anne Kunz and Hermann A. Wegner
Beilstein J. Org. Chem. 2022, 18, 781–787. https://doi.org/10.3762/bjoc.18.78

Supporting Information

Supporting Information File 1: General information, experimental data of all isolated products, 1H and 13C NMR spectra, and structures of unsuccessful substrates.
Format: PDF Size: 3.3 MB Download

Cite the Following Article

Continuous flow synthesis of azobenzenes via Baeyer–Mills reaction
Jan H. Griwatz, Anne Kunz and Hermann A. Wegner
Beilstein J. Org. Chem. 2022, 18, 781–787. https://doi.org/10.3762/bjoc.18.78

How to Cite

Griwatz, J. H.; Kunz, A.; Wegner, H. A. Beilstein J. Org. Chem. 2022, 18, 781–787. doi:10.3762/bjoc.18.78

Download Citation

Citation data can be downloaded as file using the "Download" button or used for copy/paste from the text window below.
Citation data in RIS format can be imported by all major citation management software, including EndNote, ProCite, RefWorks, and Zotero.

Presentation Graphic

Picture with graphical abstract, title and authors for social media postings and presentations.
Format: PNG Size: 11.0 MB Download

Citations to This Article

Up to 20 of the most recent references are displayed here.

Scholarly Works

  • Griwatz, J. H.; Campi, C. E.; Kunz, A.; Wegner, H. A. In-situ Oxidation and Coupling of Anilines towards Unsymmetric Azobenzenes Using Flow Chemistry. ChemSusChem 2024, e202301714. doi:10.1002/cssc.202301714
  • Eschenbacher, R.; Hemauer, F.; Franz, E.; Leng, A.; Schwaab, V.; Waleska‐Wellnhofer, N. J.; Freiberger, E. M.; Fromm, L.; Xu, T.; Görling, A.; Hirsch, A.; Steinrück, H.; Papp, C.; Brummel, O.; Libuda, J. Au‐Catalyzed Energy Release in a Molecular Solar Thermal (MOST) System: A Combined Liquid‐Phase and Surface Science Study. ChemPhotoChem 2023, 8. doi:10.1002/cptc.202300155
  • Patel, A. R.; Patel, G.; Srivastava, A.; Banerjee, S. A Review on Traditional and Modern Methods for the Synthesis of Aromatic Azo Compounds. Current Organic Chemistry 2023, 27, 1611–1628. doi:10.2174/0113852728245448231011103950
  • Duan, Z.; Dong, S.; Li, J. Organozincs for versatile synthesis of non-symmetric azoarenes. Organic & biomolecular chemistry 2023, 21, 5506–5510. doi:10.1039/d3ob00800b
  • Breugst, M.; Andexer, J. N.; Beil, S. B.; Breinbauer, R.; Dumele, O.; Ernst, M.; Gellrich, U.; Germer, P.; Giese, M.; Gulder, T. A. M.; Huy, P.; Hüttel, W.; Kath‐Schorr, S.; Körber, K.; Kordes, M.; Kuttruff, C.; Lindel, T.; Meier, R.; Myllek, S.; Schaschke, N.; Pfrengle, F.; Pietruszka, J.; Sebode, H.; Senge, M. O.; Storch, G.; Straub, B. F.; Teichert, J.; Waldvogel, S. R.; Werner, T.; Winter, C. Trendbericht Organische Chemie 2023. Nachrichten aus der Chemie 2023, 71, 40–66. doi:10.1002/nadc.20234135542
  • Franz, E.; Krappmann, D.; Fromm, L.; Luchs, T.; Görling, A.; Hirsch, A.; Brummel, O.; Libuda, J. Electrocatalytic Energy Release of Norbornadiene-Based Molecular Solar Thermal Systems: Tuning the Electrochemical Stability by Molecular Design. ChemSusChem 2022, 15, e202201483. doi:10.1002/cssc.202201483
  • Finck, L.; Oestreich, M. Synthesis of Non-Symmetric Azoarenes by Palladium-Catalyzed Cross-Coupling of Silicon-Masked Diazenyl Anions and (Hetero)Aryl Halides. Angewandte Chemie (International ed. in English) 2022, 61, e202210907. doi:10.1002/anie.202210907
  • Finck, L.; Oestreich, M. Synthese von unsymmetrischen Azobenzolen durch palladiumkatalysierte Kreuzkupplung von siliciummaskierten Diazenylanionen und (Hetero)arylhalogeniden. Angewandte Chemie 2022, 134. doi:10.1002/ange.202210907
Other Beilstein-Institut Open Science Activities