2 article(s) from Bode, Moira L
- Full Research Paper
- Published 08 Sep 2021
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Graphical Abstract
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Figure 1: Biologically active phenanthridines.
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Figure 2: Synthetic routes to phenanthridines via iminyl radicals.
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Scheme 1: Previous unexpected synthesis of the phenanthridine framework.
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Scheme 2: Synthesis of biaryl benzaldehydes.
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Scheme 3: Synthesis of biaryl oximes.
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Scheme 4: Synthesis of phenanthridines. Reagents and conditions (i) UV irradiation (450 W medium pressure Hg ...
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Figure 3: Two possible mechanistic routes and intermediates in the synthesis of phenanthridines.
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Scheme 5: Synthesis of trisphaeridine. Reagents and conditions (i) cat. Pd(PPh3)4, aq Na2CO3, DME, reflux, Ar...
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- Full Research Paper
- Published 10 Jun 2021
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Figure 1: Structure of pavettamine 1 and its enantiomer 2.
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Scheme 1: Established route for the synthesis of intermediate 4 [1].
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Scheme 2: Alternative route. Reaction conditions: a) TrCl, pyridine, rt, overnight, 100%; b) DMAP, imidazole,...
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Figure 2: Crystal structure of compound 9.
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Scheme 3: Sequence showing the source of compound 9.
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Scheme 4: Stereoselective reduction of intermediate 8 as key step towards intermediate 4. Reaction conditions...
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Figure 3: Single crystal X-ray structure of compound 4.
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Scheme 5: Synthesis of the C5 fragments from intermediate 4. Reaction conditions: a) i) TFAA, collidine, 0 °C...
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Scheme 6: Synthesis of ent-pavettamine as the TFA salt 28. Reaction conditions: a) IBX, DMSO, rt, overnight, ...
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