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Beilstein J. Org. Chem. 2022, 18, 95–101, doi:10.3762/bjoc.18.10
Structure of AZT and representative related bicyclic nucleosides.
Retrosynthetic routes for the synthesis of (5′R)-3′-azido-3′-deoxy-2′-O,5′-C-bridged-β-ᴅ-homoarabin...
Synthesis of 3′-azido-3′-deoxy-β-ᴅ-allofuranosylthymine (14a) and -uracil (14b).
Biocatalytic acetylation of the primary hydroxy group of nucleosides 14a,b.
Synthesis of (5'R)-3′-azido-3′-deoxy-2′-O,5′-C-bridged-β-ᴅ-homoarabinofuranosyl nucleosides 9a,b.
Chemical synthesis of nucleosides 9a,b starting from diacetone ᴅ-glucofuranose.
Structure elucidation of (5′R)-3′-azido-3′-deoxy-2′-O,5′-C-bridged-β-ᴅ-homoarabinofuranosylthymine (...
a) Plausible mechanism for the synthesis of (5′R)-3′-azido-3′-deoxy-2′-O,5′-C-bridged-β-ᴅ-homoarabi...
Beilstein J. Org. Chem. 2021, 17, 1727–1732, doi:10.3762/bjoc.17.121
Photocatalyzed aerobic oxidation of aromatic alcohols.
Substrate scope. Reaction conditions as given in Table 1 (entry 1). Yields are isolated yields, average of...
Selective oxidation of 3-bromobenzyl alcohol in the presence of 3-phenylpropanol. Compound 1af was ...
Mechanistic studies. (A): UV–vis spectra of the CeIV(OBn)Cln complex in CH3CN under blue light irra...