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1 article(s) from Ladlow, Mark

Continuous flow based catch and release protocol for the synthesis of α-ketoesters

Alessandro Palmieri,
Steven V. Ley,
Anastasios Polyzos,
Mark Ladlow and
Ian R. Baxendale

Full Research Paper
Published 20 May 2009

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1. Graphical Abstract
2. Figure 1: The Uniqsis FlowSyn™ continuous flow reactor comprising of a column holder and heating unit (A) and...
  
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3. Scheme 1: General procedure for the flow synthesis of α-ketoester products 4a–j.
  
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4. Scheme 2: General procedure for the batch synthesis of nitroolefinic esters 1a–j.
  
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5. Scheme 3: General procedure for the flow synthesis of nitroolefinic esters 1a,c.
  
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6. Figure 2: α-Ketoesters prepared and isolated yields.
  
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Graphical Abstract

Beilstein J. Org. Chem. 2009, 5, No. 23, doi:10.3762/bjoc.5.23

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