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3 article(s) from Li, Lin

Recent advances in amidyl radical-mediated photocatalytic direct intermolecular hydrogen atom transfer

Hao-Sen Wang,
Lin Li,
Xin Chen,
Jian-Li Wu,
Kai Sun,
Xiao-Lan Chen,
Ling-Bo Qu and
Bing Yu

Beilstein J. Org. Chem. 2025, 21, 1306–1323, doi:10.3762/bjoc.21.100

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Graphical Abstract

Figure 1: (a) BDE of C–H. (b) Direct functionalization of C–H catalyzed by transition-metal. (c) Direct funct...

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Figure 2: (a) Amidyl radical-enabled hydrogen atom transfer. (b) Substituent effects to amidyl radical proper...

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Figure 3: Representative photocatalysts discussed in this review.

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Scheme 1: Alkylation of C(sp³)–H catalyzed by amidyl radical under visible light.

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Scheme 2: Direct heteroarylation of C(sp³)–H catalyzed by amidyl radical under visible light.

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Scheme 3: Alkylation of C(sp³)–H catalyzed by amidyl radical and metal-free photocatalyst under visible light....

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Scheme 4: Alkylation of C(sp³)–H, Si–H, and Ge–H catalyzed by amidyl radical under visible light.

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Scheme 5: Direct heteroarylation of C(sp³)–H catalyzed by synergistic promotion of amidyl radical and photoca...

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Scheme 6: Direct B–H functionalization of icosahedral carboranes catalyzed by amidyl radical under visible li...

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Scheme 7: Nucleophilic amination of C(sp³)–H enabled by amidyl radical under visible light.

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Scheme 8: Direct heteroarylation of C(sp³)–H and C(sp³)–H without the presence of strong bases, acids, or oxi...

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Scheme 9: Xanthylation of C(sp³)–H addressed by amidyl radical under visible light.

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Scheme 10: Xanthylation of C(sp³)–H in polyolefins addressed by amidyl radical under visible light.

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Scheme 11: Site-selective C(sp³)–H bromination implemented by amidyl radical under visible light.

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Scheme 12: Site-selective chlorination of C(sp³)–H in natural products implemented by amidyl radical under vis...

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Scheme 13: Alkylation of C(sp³)–H catalyzed by amidyl radical photocatalyst under visible light.

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Review

Published 27 Jun 2025

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Palladium-catalyzed three-component radical-polar crossover carboamination of 1,3-dienes or allenes with diazo esters and amines

Geng-Xin Liu,
Xiao-Ting Jie,
Ge-Jun Niu,
Li-Sheng Yang,
Xing-Lin Li,
Jian Luo and
Wen-Hao Hu

Beilstein J. Org. Chem. 2024, 20, 661–671, doi:10.3762/bjoc.20.59

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Scheme 1: Background (a and b) and proposed carboamination MCR with diazo esters (c). a) Selected bioactive γ...

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Scheme 2: Substrate scope of diazo compounds, 1,3-dienes and amines. ^aReactions (1/2/3/Pd(OAc)₂/Xantphos = 0....

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Scheme 3: Substrate scope of diazo compounds, allenes and amines. ^aReactions (1/5/3/Pd(OAc)₂/Xantphos = 0.3.0...

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Scheme 4: Mechanistic experiments. a) Radical trapping experiments with TEMPO. b) Exclusion of possible inter...

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Scheme 5: Proposed mechanisms for the carboamination of 1,3-dienes or allenes with diazo esters and amines.

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Scheme 6: Scale-up reactions and synthetic transformations. Reaction conditions: a) LiAlH₄, THF, 0 °C; b) MeM...

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Published 27 Mar 2024

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Four bioactive new steroids from the soft coral Lobophytum pauciflorum collected in South China Sea

Di Zhang,
Zhe Wang,
Xiao Han,
Xiao-Lei Li,
Zhong-Yu Lu,
Bei-Bei Dou,
Wen-Ze Zhang,
Xu-Li Tang,
Ping-Lin Li and
Guo-Qiang Li

Beilstein J. Org. Chem. 2022, 18, 374–380, doi:10.3762/bjoc.18.42

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Figure 1: Structures of compounds 1–7.

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Figure 2: ¹H,¹H-COSY and selected key HMBC correlations of 1–4.

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Figure 3: Selected NOESY correlations of compounds 1–4.

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Figure 4: X-ray crystallographic analysis of compounds 1–3.

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Figure 5: Effects of compound 1 on the anti-inflammation of zebrafish internodes. ## Indicates that the CuSO₄...

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Published 08 Apr 2022

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