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Beilstein J. Org. Chem. 2024, 20, 155–161, doi:10.3762/bjoc.20.14
Graphical Abstract
Scheme 1: Methods for the C5-selective bromination of 8-aminoquinoline amides.
Scheme 2: Substrate scope of the 8-aminoquinoline amides. Reaction conditions: 1 (0.2 mmol), 2a (0.8 mmol), C...
Scheme 3: Substrate scope of the bromoalkanes. Reaction conditions: 1a (0.2 mmol), 2 (0.8 mmol), Cu(OAc)2·H2O...
Scheme 4: Further substrate scope investigations and gram-scale application.
Scheme 5: Control experiments and proposed mechanism.
Beilstein J. Org. Chem. 2019, 15, 703–709, doi:10.3762/bjoc.15.65
Scheme 1: Representative strategies for the synthesis of N-substituted 2-aminobenzothiopyranones.
Scheme 2: The synthesis of sulfide 1, sulfoxide 2, and sulfone 3.
Scheme 3: Scope of the synthesis of versatile 2-aminobenzothiopyranones. All reactions were performed with 1....
Scheme 4: The gram-scale synthesis of 2-aminobenzothiopyranones 4a and 4d.