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Precursor sticking coefficient determination from indented deposits fabricated by electron beam induced deposition

  • Alexander Kuprava and
  • Michael Huth

Beilstein J. Nanotechnol. 2025, 16, 35–43, doi:10.3762/bjnano.16.4

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  • estimate or initial guess in calculations or even simulations dedicated to FEBID for precursors such as WF6 [9], Me3CpPtMe [10][11][12][13][14][15], HCo3Fe(CO)12, and Nb(NMe2)3(N-t-Bu) [12], as well as tetraethyl orthosilicate (TEOS) [16]. The sticking coefficient has been determined only in the work of
  • pumping speed, and gas injection system (GIS) geometry using the GIS nozzle gas dynamics simulation approach described in [22]. The tilt of the GIS in relation to the substrate surface that defines the angle at which molecules hit the surface was 13° for Cr(C6H6)2 and 50° for Me3CpPtMe. Both GIS needles
  • Arrhenius-type behavior, an activation energy value Ea = 1.13 eV can be derived from the linear fit in Figure 4. The derived value is too big if physisorption is assumed, and it is two times bigger than the adsorption activation energy previously determined for Me3CpPtMe [11][13]. However, this derived
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Published 13 Jan 2025

Bioinspired nanofilament coatings for scale reduction on steel

  • Siad Dahir Ali,
  • Mette Heidemann Rasmussen,
  • Jacopo Catalano,
  • Christian Husum Frederiksen and
  • Tobias Weidner

Beilstein J. Nanotechnol. 2025, 16, 25–34, doi:10.3762/bjnano.16.3

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  • SNFs. These filaments have been developed for coatings on polymers [10][11][12], textiles [12][13][14][15][16][17], aluminium and titanium [11][12], and glass [11][12][13][18][19], to replicate the water-repelling effects observed in nature [13][18][20][21]. Coatings with nano- or micrometer-sized
  • polymerization of a polysiloxane on the material surface [18]. The polysiloxane methyl groups lower the surface energy and render the surface hydrophobic. Clearly, the surface chemistry of steel surfaces is very different from the previously used materials such as glass [11][12][13][18], polymers [10][11][12
  • ], and textiles [11][12][13][14][15][16] as it does not offer the hydroxy moieties used previously for direct surface polymerization. It is therefore important to carefully test the stability and attachment of any SNFs growing on steel surfaces. Mechanical scratching of the coated steel surface will
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Published 09 Jan 2025

A nanocarrier containing carboxylic and histamine groups with dual action: acetylcholine hydrolysis and antidote atropine delivery

  • Elina E. Mansurova,
  • Andrey A. Maslennikov,
  • Anna P. Lyubina,
  • Alexandra D. Voloshina,
  • Irek R. Nizameev,
  • Marsil K. Kadirov,
  • Anzhela A. Mikhailova,
  • Polina V. Mikshina,
  • Albina Y. Ziganshina and
  • Igor S. Antipin

Beilstein J. Nanotechnol. 2025, 16, 11–24, doi:10.3762/bjnano.16.2

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  • calixarenes, have been extensively utilized in the creation of different smart systems [13][14]. Owing to their unique structural features, these macrocycles are employed in catalysis, such as in the breakdown of OPs [15][16][17][18], as carriers for drug delivery [19][20][21][22], and in the creation of
  • concentration range (13–1650 μM) and did not cause hemolysis even at the highest concentration of 825 μM (Table 2 and Supporting Information File 1, Figure S4). Hist-RA at 220 μM led to nearly 100% hemolysis (Supporting Information File 1, Figure S4), while at concentrations of 110 and 55 μM, agglutination was
  • , 10.74 g (77.6 mmol) of K2CO3 and 1.6 g (9.7 mmol) of KI were added. The mixture was stirred at room temperature, and a solution of ethyl bromoacetate (13 g, 77.8 mmol) in 100 mL of acetone was added dropwise. After addition, the mixture was stirred at 80 °C for 24 h, followed by the removal of the
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Published 09 Jan 2025

Orientation-dependent photonic bandgaps in gold-dust weevil scales and their titania bioreplicates

  • Norma Salvadores Farran,
  • Limin Wang,
  • Primoz Pirih and
  • Bodo D. Wilts

Beilstein J. Nanotechnol. 2025, 16, 1–10, doi:10.3762/bjnano.16.1

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  • copolymers [10][11], lithography, or laser etching [12][13], but it can be routinely found in animal integuments. Biomimetic approaches using templates from natural structures offers a possible alternative. The scales of many beetles and weevils contain diamond photonic crystals [14][15][16] that may serve
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Published 02 Jan 2025

Mechanistic insights into endosomal escape by sodium oleate-modified liposomes

  • Ebrahim Sadaqa,
  • Satrialdi,
  • Fransiska Kurniawan and
  • Diky Mudhakir

Beilstein J. Nanotechnol. 2024, 15, 1667–1685, doi:10.3762/bjnano.15.131

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  • evidenced by a shift in zeta potential to a slightly positive value of 1.07 ± 1.80 mV. This shift may be attributed to the protonation of amino acids such as glutamic and aspartic acid in the peptide sequence, which, under acidic conditions, likely contributes to an increase in positive charge [13
  • purchased from Avanti Polar Lipids (Alabaster, AL, USA). Cholesterol (CAS No. 57-88-5, ≥99% purity), 4-(2-hydroxyethyl)-1-piperazineethanesulfonic acid (HEPES, CAS No. 7365-45-9, ≥99.5% purity), resazurin (CAS No. 62758-13-8, ≥98% purity), and sodium oleate (CAS No. 143-19-1, ≥97% purity) were obtained from
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Published 30 Dec 2024

Attempts to preserve and visualize protein corona on the surface of biological nanoparticles in blood serum using photomodification

  • Julia E. Poletaeva,
  • Anastasiya V. Tupitsyna,
  • Alina E. Grigor’eva,
  • Ilya S. Dovydenko and
  • Elena I. Ryabchikova

Beilstein J. Nanotechnol. 2024, 15, 1654–1666, doi:10.3762/bjnano.15.130

Graphical Abstract
  • system, and the role of the corona in the pathogenesis of chronic diseases are being studied [5][10][11][12][13]. A number of works are devoted to the study of protein corona formation on EVs previously isolated from biological fluids [14][15]. The existence of a “natural” protein corona on EVs in the
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Published 30 Dec 2024

Fabrication of hafnium-based nanoparticles and nanostructures using picosecond laser ablation

  • Abhishek Das,
  • Mangababu Akkanaboina,
  • Jagannath Rathod,
  • R. Sai Prasad Goud,
  • Kanaka Ravi Kumar,
  • Raghu C. Reddy,
  • Ratheesh Ravendran,
  • Katia Vutova,
  • S. V. S. Nageswara Rao and
  • Venugopal Rao Soma

Beilstein J. Nanotechnol. 2024, 15, 1639–1653, doi:10.3762/bjnano.15.129

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  • size and morphology [1]. Recently, interest has risen regarding synthesis and study of Hf-based NPs. Depending on the morphology, chemical composition, and quantum confinement effects, NPs can exhibit novel properties, making them applicable for large-spectrum usage [12][13]. Thus, synthesizing the
  • ± 18 nm, that of HfNSs-T ranged from 50 to 200 nm, with an average feature size of 121 ± 37 nm, and that of HfNSs-A ranged from 50 to 150 nm with an average feature size of 102 ± 24 nm. Figure 13 shows the relationship between the refractive index (η) of the liquid used during ablation and the
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Published 18 Dec 2024

Heterogeneous reactions in a HFCVD reactor: simulation using a 2D model

  • Xochitl Aleyda Morán Martínez,
  • José Alberto Luna López,
  • Zaira Jocelyn Hernández Simón,
  • Gabriel Omar Mendoza Conde,
  • José Álvaro David Hernández de Luz and
  • Godofredo García Salgado

Beilstein J. Nanotechnol. 2024, 15, 1627–1638, doi:10.3762/bjnano.15.128

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  • . Different tools such as ab initio density functional theory [13][14], kinetic Monte Carlo simulations [15][16], and reactive molecular dynamics simulations [17][18] have been used to understand the chemical reactions underlying the growth of the films [19]. Modeling the reaction mechanism in both two
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Published 17 Dec 2024

Biomimetic nanocarriers: integrating natural functions for advanced therapeutic applications

  • Hugo Felix Perini,
  • Beatriz Sodré Matos,
  • Carlo José Freire de Oliveira and
  • Marcos Vinicius da Silva

Beilstein J. Nanotechnol. 2024, 15, 1619–1626, doi:10.3762/bjnano.15.127

Graphical Abstract
  • such as: loss of stability, low efficiency in crossing biological barriers, inadequate efficacy in reaching target active molecules, and poor biodistribution [13][14]. Nanocarriers are employed to transport raw materials, which can be vesicles or solid nanoparticles [15]. Despite the significant
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Published 16 Dec 2024

Natural nanofibers embedded in the seed mucilage envelope: composite hydrogels with specific adhesive and frictional properties

  • Agnieszka Kreitschitz and
  • Stanislav N. Gorb

Beilstein J. Nanotechnol. 2024, 15, 1603–1618, doi:10.3762/bjnano.15.126

Graphical Abstract
  • the diaspore) [6][13]. Mucilage is often composed of three types of polysaccharides, which are typical components found in the plant cell wall. It exhibits modified secondary cell wall, where pectins are the dominating component, while hemicelluloses and cellulose fibrils constitute the lesser part of
  • its composition [14][15][16]. The nanoscale level of the spatial organisation of mucilage observed with scanning electron microscopy (SEM) reveals the complexity of the mucilage with special features, such as 3D organisation of polysaccharides in a net-like structure [7][13]. In the last years, the
  • hydration [8][22][38]. Mucilage, which is produced by the mucilaginous cells of diaspores in a form of densely packed layers, has the ability of loosening its structure after hydration into an easily accessible 3D fibrillar network [7][13][14][39] (Figure 3 and Figure 4 below). One of the key components of
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Published 13 Dec 2024

Liver-targeting iron oxide nanoparticles and their complexes with plant extracts for biocompatibility

  • Shushanik A. Kazaryan,
  • Seda A. Oganian,
  • Gayane S. Vardanyan,
  • Anatolie S. Sidorenko and
  • Ashkhen A. Hovhannisyan

Beilstein J. Nanotechnol. 2024, 15, 1593–1602, doi:10.3762/bjnano.15.125

Graphical Abstract
  • in most biological and chemical reactions involved in the production of medical materials [10][11][12][13]. Magnetic nanoparticles (MNPs), such as iron oxides, not only exhibit superparamagnetism and high magnetic susceptibility, they also possess unique physical properties, biocompatibility
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Published 11 Dec 2024

Facile synthesis of size-tunable L-carnosine-capped silver nanoparticles and their role in metal ion sensing and catalytic degradation of p-nitrophenol

  • Akash Kumar,
  • Ridhima Chadha,
  • Abhishek Das,
  • Nandita Maiti and
  • Rayavarapu Raja Gopal

Beilstein J. Nanotechnol. 2024, 15, 1576–1592, doi:10.3762/bjnano.15.124

Graphical Abstract
  • through surface chemistry and other parameters such as size and shape [13]. Kästner and Thünemann described the catalytic degradation of P-NP using silver nanoparticles with the activity depending on the capping agents [14]. To design a dual-functional system for environmental applications, a potential
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Published 06 Dec 2024

Green synthesis of silver nanoparticles derived from algae and their larvicidal properties to control Aedes aegypti

  • Matheus Alves Siqueira de Assunção,
  • Douglas Dourado,
  • Daiane Rodrigues dos Santos,
  • Gabriel Bezerra Faierstein,
  • Mara Elga Medeiros Braga,
  • Severino Alves Junior,
  • Rosângela Maria Rodrigues Barbosa,
  • Herminio José Cipriano de Sousa and
  • Fábio Rocha Formiga

Beilstein J. Nanotechnol. 2024, 15, 1566–1575, doi:10.3762/bjnano.15.123

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  • characteristics such as greater absorption capacity, greater bioavailability, controlled release of active ingredients, improved solubility of hydrophobic substances in water, and good kinetic stability [12][13][14]. Metallic nanoparticles have been investigated as a promising approach for vector control. The
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Published 04 Dec 2024

Ultrablack color in velvet ant cuticle

  • Vinicius Marques Lopez,
  • Wencke Krings,
  • Juliana Reis Machado,
  • Stanislav Gorb and
  • Rhainer Guillermo-Ferreira

Beilstein J. Nanotechnol. 2024, 15, 1554–1565, doi:10.3762/bjnano.15.122

Graphical Abstract
  • pigmentation originates from the interaction of light with arrays of microlenses on the cuticle or overlapping brush-like scales positioned just above a densely pigmented absorbing layer. Similar phenomena can be observed in butterflies [11][12], birds [13], and snakes [14][15]. This intricately structured
  • light [10][13]. The ultrablack surfaces found in certain organisms present a remarkable adaptation shaped by selective pressures in their respective environments. For example, combining conspicuous visual cues with ultrablack colors may provide heightened internal visual contrast, thus highlighting
  • sexually selected colors in peacock spiders [10][13] (Figure 1A) and birds-of-paradise (Figure 1B). Likewise, ultrablack colors may offer thermoregulatory and disruptive advantages to vipers (Figure 1C) and assist butterflies in predator evasion (Figure 1D) [9][15]. Therefore, the parallel between
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Published 02 Dec 2024

The round-robin approach applied to nanoinformatics: consensus prediction of nanomaterials zeta potential

  • Dimitra-Danai Varsou,
  • Arkaprava Banerjee,
  • Joyita Roy,
  • Kunal Roy,
  • Giannis Savvas,
  • Haralambos Sarimveis,
  • Ewelina Wyrzykowska,
  • Mateusz Balicki,
  • Tomasz Puzyn,
  • Georgia Melagraki,
  • Iseult Lynch and
  • Antreas Afantitis

Beilstein J. Nanotechnol. 2024, 15, 1536–1553, doi:10.3762/bjnano.15.121

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  • NMs and accelerate regulatory decision-making procedures [2][5][13]. An IATA scheme for the prediction of the short-term regional lung-deposited dose of inhaled inorganic NMs in humans following acute exposure and the longer-term NM biodistribution after inhalation, has already been presented [14
  • ][62] (Equation 12). These values quantify the distance of each query sample from the centroid of the training set [61], taking into account the descriptor values employed in model development. The AD boundaries are determined by a predetermined threshold leverage value h* (Equation 13). A test
  • The area of reliable predictions for this model was defined using the leverage method. The leverage threshold was calculated based on the training NMs subset and set to 0.226 (Equation 13). The test NM samples had values within the range of 0.031 to 0.191, indicating that their predictions were
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Published 29 Nov 2024

Electrochemical nanostructured CuBTC/FeBTC MOF composite sensor for enrofloxacin detection

  • Thi Kim Ngan Nguyen,
  • Tien Dat Doan,
  • Huy Hieu Luu,
  • Hoang Anh Nguyen,
  • Thi Thu Ha Vu,
  • Quang Hai Tran,
  • Ha Tran Nguyen,
  • Thanh Binh Dang,
  • Thi Hai Yen Pham and
  • Mai Ha Hoang

Beilstein J. Nanotechnol. 2024, 15, 1522–1535, doi:10.3762/bjnano.15.120

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  • significantly enhanced the electrochemical response of ENR, increasing the signal by more than ten times compared to the unmodified electrode. Under optimal analytical conditions, the sensor exhibited three dynamic ranges for ENR detection, that is, 0.005 to 0.100 µM, 0.1 to 1.0 µM, and 1 to 13 µM, with
  • requirements regarding instruments, chemicals, time consumption, and preparation of the samples. Electrochemical methods to detect ENR have attracted great attention because of benefits including high accuracy, simplicity, and environmental friendliness [11][12][13][14]. Electrochemical methods exhibited high
  • from 1 to 13 µM at an accumulation time of 0 s. The linear relationship obtained is represented by the regression equation Ip (µA) = 1.225 × CENR (µM) + 0.557 (R2 = 0.9992). The consistently high correlation coefficients indicate the robust performance of the developed sensor. From the calibration
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Published 28 Nov 2024

Integrating high-performance computing, machine learning, data management workflows, and infrastructures for multiscale simulations and nanomaterials technologies

  • Fabio Le Piane,
  • Mario Vozza,
  • Matteo Baldoni and
  • Francesco Mercuri

Beilstein J. Nanotechnol. 2024, 15, 1498–1521, doi:10.3762/bjnano.15.119

Graphical Abstract
  • unprecedented resolutions [11][12][13]. This aids in the understanding of fundamental properties and the identification of structure–property relationships. The integration of digital technologies with experimental techniques also enables real-time monitoring and control of materials synthesis processes
  • , GPUs are nowadays considered the most efficient technological platform for performing AI and data-intensive tasks [13][25]. This has enabled the development of complex models that can process vast amounts of materials data. Another consumer-driven technology that has boosted the digitalization of
  • relatively low throughput of multiscale modelling approaches in current scenarios. In recent years, however, we have begun to witness the success of AI and ML for materials development [7][13]. This is particularly evident, for example, in the application of AI-related methods for the prediction of structure
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Published 27 Nov 2024

Polymer lipid hybrid nanoparticles for phytochemical delivery: challenges, progress, and future prospects

  • Iqra Rahat,
  • Pooja Yadav,
  • Aditi Singhal,
  • Mohammad Fareed,
  • Jaganathan Raja Purushothaman,
  • Mohammed Aslam,
  • Raju Balaji,
  • Sonali Patil-Shinde and
  • Md. Rizwanullah

Beilstein J. Nanotechnol. 2024, 15, 1473–1497, doi:10.3762/bjnano.15.118

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  • matrix, which can vary in its configuration depending on the specific requirements of the delivery system [12][13]. The lipid components, often phospholipids, cholesterol, and surfactants are integral for solubilizing lipophilic drugs. The polymer component, which can include materials such as
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Published 22 Nov 2024

Effect of radiation-induced vacancy saturation on the first-order phase transformation in nanoparticles: insights from a model

  • Aram Shirinyan and
  • Yuriy Bilogorodskyy

Beilstein J. Nanotechnol. 2024, 15, 1453–1472, doi:10.3762/bjnano.15.117

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  • . For example, a two-phase TiCr alloy undergoes phase transformation when irradiated with Kr+ ions with an energy of 1 MeV [13]. In another study, a bcc→fcc phase transition was observed in an α-FeNi alloy due to radiation of self-ions at 673 K and a dose of approximately 1.2 dpa [14]. Furthermore
  • concentration and grain size is about 1.4, but not 2 as used in Shen’s model [3]. An experimental study on ZrO2 with grain sizes ranging from 10 to 300 nm showed that the number of defects per volume (defect clusters per cubic nanometer) can be fitted by an expression like Equation 13 with a fitted exponent of
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Published 21 Nov 2024

Strain-induced bandgap engineering in 2D ψ-graphene materials: a first-principles study

  • Kamal Kumar,
  • Nora H. de Leeuw,
  • Jost Adam and
  • Abhishek Kumar Mishra

Beilstein J. Nanotechnol. 2024, 15, 1440–1452, doi:10.3762/bjnano.15.116

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  • transition of graphene from a semimetal to an insulator after full hydrogenation [9]. After the discovery of graphene, other novel 2D materials, such as goldene [10], stanene [11], plumbene [12], antimonene [13], and arsenene [14], have been predicted and experimentally synthesized. Few of these materials
  • negative strain in the lattice plane, ψ-graphene maintains its conductive nature until −13%; at −14%, a bandgap of ≈0.2 eV emerges between the valence and conduction bands as shown in Figure 2. Beyond −14% negative strain, a proportional increment in the bandgap is observed, reaching its maximum value of
  • without experiencing much out-plane deformation or buckling. Here, we observe that ψ-graphene retains its flat structure up to −10% with negligible buckling, and only above this strain value buckling was observed in ψ-graphene sheets, as shown in Table 2 for −13% to −17% strain. Hence, within the negative
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Published 20 Nov 2024

Ion-induced surface reactions and deposition from Pt(CO)2Cl2 and Pt(CO)2Br2

  • Mohammed K. Abdel-Rahman,
  • Patrick M. Eckhert,
  • Atul Chaudhary,
  • Johnathon M. Johnson,
  • Jo-Chi Yu,
  • Lisa McElwee-White and
  • D. Howard Fairbrother

Beilstein J. Nanotechnol. 2024, 15, 1427–1439, doi:10.3762/bjnano.15.115

Graphical Abstract
  • , deposition strategies in various applications, such as circuit editing and lithographic mask repair in the semiconductor industry [7][8][9][10][11][12] as well as the growth of functional materials for magnetism [13][14][15][16], superconductivity [17], and sensing [18][19]. Compared to FEBID, FIBID operates
  • with the presence of trace peaks at m/z 13 and m/z 45, corresponding to 13CO, 13C, and 13CO2, respectively. Contributions from the background gases are superimposed (dashed red spectrum). The peaks that appear due to ion irradiation can be easily identified because of the presence of 13C from Pt(13CO
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Published 19 Nov 2024

Lithium niobate on insulator: an emerging nanophotonic crystal for optimized light control

  • Midhun Murali,
  • Amit Banerjee and
  • Tanmoy Basu

Beilstein J. Nanotechnol. 2024, 15, 1415–1426, doi:10.3762/bjnano.15.114

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  • effect (largest electro-optic coefficient r33 = 27 pm/V at 1500 nm) [13], enables dynamic control of the reflection spectrum of DBR through applied electric fields, unlocking functionalities such as wavelength filtering and modulation [9][11][12]. LiNbO3 is transparent across a broad spectrum, spanning
  • from the visible to the infrared (400–5000 nm) [13]. The high degree of flexibility in fabrication created functional photonic nanostructures such as microring, periodically poled lithium niobate, and photonic crystals [14][15]. This versatility makes it suitable for DBRs to be used in various
  • in refractive index which is crucial for the creation of photonic bandgap [13]. In addition, these two materials are highly used in the photonics industry due to their easy availability and low cost. Moreover, both TiO2 and SiO2 can be integrated with various materials. The precise choice of
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Published 14 Nov 2024

Nanotechnological approaches for efficient N2B delivery: from small-molecule drugs to biopharmaceuticals

  • Selin Akpinar Adscheid,
  • Akif E. Türeli,
  • Nazende Günday-Türeli and
  • Marc Schneider

Beilstein J. Nanotechnol. 2024, 15, 1400–1414, doi:10.3762/bjnano.15.113

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  • regulatory cells for the homeostasis of the BBB. The interaction between astrocytes and pericytes plays a vital role in brain vasculogenesis and the maintenance of the BBB [12]. Overall, the high selectivity of the BBB provides optimal conditions for CNS homeostasis [13]. Because of the presence of the BBB
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Published 12 Nov 2024

Various CVD-grown ZnO nanostructures for nanodevices and interdisciplinary applications

  • The-Long Phan,
  • Le Viet Cuong,
  • Vu Dinh Lam and
  • Ngoc Toan Dang

Beilstein J. Nanotechnol. 2024, 15, 1390–1399, doi:10.3762/bjnano.15.112

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  • microcavities [9]. Additionally, it is a transparent semiconductor with significant piezoelectricity [10]. These noble characteristics suggest ZnO to be a potential material in the fabrication of UV/blue/green LEDs, solid-state random lasers, UV-absorption devices, and nanogenerators [9][11][12][13]. Magnetic
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Published 11 Nov 2024

A biomimetic approach towards a universal slippery liquid infused surface coating

  • Ryan A. Faase,
  • Madeleine H. Hummel,
  • AnneMarie V. Hasbrook,
  • Andrew P. Carpenter and
  • Joe E. Baio

Beilstein J. Nanotechnol. 2024, 15, 1376–1389, doi:10.3762/bjnano.15.111

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  • materials, researchers have developed strategies to combat blood clots and bacterial infections in frequently used devices such as tubing, catheters, and grafts [9][10][11][12][13][14][15]. Consideration of the coagulation cascade is a crucial part in engineering new materials that interact with blood and
  • ][13], anodization [3][14], silane chemistry [18], and polymer multilayers [5][15]. While these methods are effective, there is often a requirement for a specific chemical environment, like a plasma processing step or the growth of an oxide layer. In this investigation, we aim to simplify the
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Published 08 Nov 2024
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