Evaluating metal-organic precursors for focused ion beam-induced deposition through solid-layer decomposition analysis

• Benedykt R. Jany,
• Katarzyna Madajska,
• Aleksandra Butrymowicz-Kubiak,
• Franciszek Krok and
• Iwona B. Szymańska

Beilstein J. Nanotechnol. 2025, 16, 1942–1951, doi:10.3762/bjnano.16.135

• or ion beam-induced deposition (FEBID/FIBID) allows for the precise fabrication of two- and three-dimensional nanostructures with well-defined shapes and dimensions ranging from 5 to 10 nm [1][5][6][7][8][9][10]. This high spatial resolution is achieved by precisely controlling the position and

• the fabrication or modification of cantilevers in AFM and scanning optical near-field microscopy, and as plasmonic materials [15][16][17][18][19]. FEBID/FIBID techniques combine the advantages of direct-write lithographic processes, for example, high spatial resolution, site-specificity, no need for

Parylene-coated platinum nanowire electrodes for biomolecular sensing applications

• Chao Liu,
• Peker Milas,
• Michael G. Spencer and
• Birol Ozturk

Beilstein J. Nanotechnol. 2025, 16, 1392–1400, doi:10.3762/bjnano.16.101

• advantage makes them suitable for biosensing applications with high spatial resolution involving single cells. The morphology and functionality of the electrodes were characterized through elemental analysis and copper deposition, demonstrating their capability for effective surface modification. Results

Automated collection and categorisation of STM images and STS spectra with and without machine learning

• Dylan Stewart Barker and
• Adam Sweetman

Beilstein J. Nanotechnol. 2025, 16, 1367–1379, doi:10.3762/bjnano.16.99

• Dylan Stewart Barker Adam Sweetman School of Physics and Astronomy, University of Leeds, Leeds LS2 9JT, United Kingdom 10.3762/bjnano.16.99 Abstract Atomic resolution scanning probe microscopy, and in particular scanning tunnelling microscopy (STM) allows for high-spatial-resolution imaging and

• properties of surfaces and molecules with atomic precision. This opens up the ability to map the local density of states (LDOS) of a sample with high spatial resolution [1][2][3]. Peaks within a map of the LDOS correspond to increases in conductance at specific bias values, revealing the energy levels of key

• misshaped tips cause averaging of contributions over larger areas, reducing the spatial resolution and potentially blending the electronic features between different sites. However, even for tips with high spatial resolution, different tip structures and probe terminations are known to influence these

Nanostructured materials characterized by scanning photoelectron spectromicroscopy

• Matteo Amati,
• Alexey S. Shkvarin,
• Alexander I. Merentsov,
• Alexander N. Titov,
• María Taeño,
• David Maestre,
• Sarah R. McKibbin,
• Zygmunt Milosz,
• Ana Cremades,
• Rainer Timm and
• Luca Gregoratti

Beilstein J. Nanotechnol. 2025, 16, 700–710, doi:10.3762/bjnano.16.54

• high spatial resolution. We correlate that to the chemical surface composition, distinguishing between surface and bulk effects on the path towards improved surface properties of nanowire solar cells with further enhanced efficiency. Furthermore, they demonstrate the large suitability of SPEM for

Nanoscale capacitance spectroscopy based on multifrequency electrostatic force microscopy

• Pascal N. Rohrbeck,
• Lukas D. Cavar,
• Franjo Weber,
• Peter G. Reichel,
• Mara Niebling and
• Stefan A. L. Weber

Beilstein J. Nanotechnol. 2025, 16, 637–651, doi:10.3762/bjnano.16.49

• method for nanoscale capacitance characterization at arbitrary frequencies above the second cantilever resonance. Besides a high spatial resolution, the key advantage of the multifrequency approach of MFH-EFM is that it measures the second-order capacitance gradient at almost arbitrary frequencies

Bolometric IR photoresponse based on a 3D micro-nano integrated CNT architecture

• Yasameen Al-Mafrachi,
• Sandeep Yadav,
• Sascha Preu,
• Jörg J. Schneider and
• Oktay Yilmazoglu

Beilstein J. Nanotechnol. 2024, 15, 1030–1040, doi:10.3762/bjnano.15.84

• integration techniques make it important for real-time broadband imaging systems. Keywords: 3D micro-nano architecture; blackbody absorption; CNT microbolometer; high responsivity; high spatial resolution; Introduction Non-cryogenic infrared (IR) microbolometers represent a cutting-edge technology with

AFM-IR investigation of thin PECVD SiO_x films on a polypropylene substrate in the surface-sensitive mode

• Hendrik Müller,
• Hartmut Stadler,
• Teresa de los Arcos,
• Adrian Keller and
• Guido Grundmeier

Beilstein J. Nanotechnol. 2024, 15, 603–611, doi:10.3762/bjnano.15.51

• Photothermal AFM-IR nanospectroscopy is a technique that combines the chemical information from infrared (IR) spectroscopy with the high spatial resolution of atomic force microscopy (AFM). For this, the sample is illuminated with a tunable IR laser [1]. When a suitable IR wavelength is chosen, resonant

Stiffness calibration of qPlus sensors at low temperature through thermal noise measurements

• Laurent Nony,
• Sylvain Clair,
• Daniel Uehli,
• Aitziber Herrero,
• Jean-Marc Themlin,
• Andrea Campos,
• Franck Para,
• Alessandro Pioda and
• Christian Loppacher

Beilstein J. Nanotechnol. 2024, 15, 580–602, doi:10.3762/bjnano.15.50

• possible to quantify the interatomic interaction forces that develop between the tip and the surface acquired in spectroscopic data cube modes [7][8] with both high sensitivity and high spatial resolution. Recently, the force sensitivity has been pushed forward, and forces as low as 100 fN have been

Graphene removal by water-assisted focused electron-beam-induced etching – unveiling the dose and dwell time impact on the etch profile and topographical changes in SiO₂ substrates

• Aleksandra Szkudlarek,
• Jan M. Michalik,
• Inés Serrano-Esparza,
• Zdeněk Nováček,
• Veronika Novotná,
• Piotr Ozga,
• Czesław Kapusta and
• José María De Teresa

Beilstein J. Nanotechnol. 2024, 15, 190–198, doi:10.3762/bjnano.15.18

• , the data reveal phenomena emerging from electron-induced interactions of adsorbed water molecules with SiO2, which have not been reported up to now. We observe that at low electron doses, the method provides a high spatial resolution and induces a low amount of defects in nonexposed areas of graphene

TEM sample preparation of lithographically patterned permalloy nanostructures on silicon nitride membranes

• Joshua Williams,
• Michael I. Faley,
• Joseph Vimal Vas,
• Peng-Han Lu and
• Rafal E. Dunin-Borkowski

Beilstein J. Nanotechnol. 2024, 15, 1–12, doi:10.3762/bjnano.15.1

• –iron alloy (80 atom % Ni and 20 atom % Fe) that has a small coercive field (Hc) [17] and low magnetostriction (λs) [18], as well as high permeability and high saturation magnetization (Ms) [19]. TEM offers high spatial resolution for magnetic imaging. TEM-based magnetic imaging techniques such as

Dual-heterodyne Kelvin probe force microscopy

• Benjamin Grévin,
• Fatima Husainy,
• Dmitry Aldakov and
• Cyril Aumaître

Beilstein J. Nanotechnol. 2023, 14, 1068–1084, doi:10.3762/bjnano.14.88

• dynamics (i.e., decay time-constant). In turn, this experiment confirms that DHe-KPFM allows an ac-demodulated imaging of the SPV (to within the K1 scalar constant) with a very high spatial resolution (a lateral resolution of a few nanometres has been achieved according to image cross-sections, not shown

• lower density of non-percolating PC71BM clusters (delaying the SPV decay less). Imaging weak surface photovoltage signals: CsPbBr3 nanosheets on HOPG We have just seen that images of SPV magnitude and dynamics can be obtained with high spatial resolution. In this final section, we will show that DHe

Industrial perspectives for personalized microneedles

• Remmi Danae Baker-Sediako,
• Benjamin Richter,
• Matthias Blaicher,
• Michael Thiel and
• Martin Hermatschweiler

Beilstein J. Nanotechnol. 2023, 14, 857–864, doi:10.3762/bjnano.14.70

• dimensions with high spatial resolution, which lends itself to continuous rather than discrete printing [59][61]. A key result of 2PP grayscale printing is that the technique is, on average, five to ten times faster than the common 2PP layer-by-layer approach [52]. Thiel et al. successfully applied 2GL® to

Cross-sectional Kelvin probe force microscopy on III–V epitaxial multilayer stacks: challenges and perspectives

• Mattia da Lisca,
• José Alvarez,
• James P. Connolly,
• Nicolas Vaissiere,
• Karim Mekhazni,
• Jean Decobert and
• Jean-Paul Kleider

Beilstein J. Nanotechnol. 2023, 14, 725–737, doi:10.3762/bjnano.14.59

• the overall VOC. Nevertheless, these considerations need further investigations and further support from modelling. Conclusion In this contribution, it is shown that KPFM under ambient conditions is a valuable tool to investigate III–V multilayer stacks with high spatial resolution of down to 20 nm

The steep road to nonviral nanomedicines: Frequent challenges and culprits in designing nanoparticles for gene therapy

• Yao Yao,
• Yeongun Ko,
• Grant Grasman,
• Jeffery E. Raymond and
• Joerg Lahann

Beilstein J. Nanotechnol. 2023, 14, 351–361, doi:10.3762/bjnano.14.30

• throughput and high spatial resolution (in parallel) should be considered as best practice for the purposes of accuracy, statistical relevance, and comparisons between studies. An in-depth mechanistic understanding of NP uptake will be required to improve the design of NP-based delivery platforms. The sole

High–low Kelvin probe force spectroscopy for measuring the interface state density

• Ryo Izumi,
• Masato Miyazaki,
• Yan Jun Li and
• Yasuhiro Sugawara

Beilstein J. Nanotechnol. 2023, 14, 175–189, doi:10.3762/bjnano.14.18

• of the effects of semiconductor interface states with high spatial resolution using high and low AC bias frequencies compared with the cutoff frequency of the carrier transfer between the interface and bulk states. Information on the energy spectrum of the interface state density is important for

• known as a method that can measure the contact potential difference (CPD) between a tip and a sample with high spatial resolution [4][5]. KPFM is based on the detection of the electrostatic force between a tip and a sample using atomic force microscopy (AFM) [6][7][8]. CPD and topographic measurements

Characterisation of a micrometer-scale active plasmonic element by means of complementary computational and experimental methods

• Ciarán Barron,
• Giulia Di Fazio,
• Samuel Kenny,
• Silas O’Toole,
• Robin O’Reilly and
• Dominic Zerulla

Beilstein J. Nanotechnol. 2023, 14, 110–122, doi:10.3762/bjnano.14.12

• method therefore investigates the thermal response of this active plasmonic element at a high spatial resolution. Knowledge of the distribution leads to predictions on how the near field will be locally affected, which is key for understanding the behaviour of the active plasmonic element. The heating

Studies of probe tip materials by atomic force microscopy: a review

• Ke Xu and
• Yuzhe Liu

Beilstein J. Nanotechnol. 2022, 13, 1256–1267, doi:10.3762/bjnano.13.104

• structure [37][38]. Due to these unique properties, CNT-AFM probes offer a longer lifetime, high spatial resolution, and unprecedented sensitivity than their conventional silicon counterparts. Carbon nanotubes are generally prepared by assembled and grown methods. Assembled carbon nanotube probe Nishijima

A cantilever-based, ultrahigh-vacuum, low-temperature scanning probe instrument for multidimensional scanning force microscopy

• Hao Liu,
• Zuned Ahmed,
• Sasa Vranjkovic,
• Manfred Parschau,
• Andrada-Oana Mandru and
• Hans J. Hug

Beilstein J. Nanotechnol. 2022, 13, 1120–1140, doi:10.3762/bjnano.13.95

• not limited by detector noise at room temperature. Such an extremely high force derivative sensitivity is key for MFM experiments with high spatial resolution (and also to minimize the influence of the tip stray field on the sample by employing low magnetic moment tips). In addition, such a

Theranostic potential of self-luminescent branched polyethyleneimine-coated superparamagnetic iron oxide nanoparticles

• Rouhollah Khodadust,
• Ozlem Unal and
• Havva Yagci Acar

Beilstein J. Nanotechnol. 2022, 13, 82–95, doi:10.3762/bjnano.13.6

• growing demand for a combination of different imaging modalities to improve the detection limit and to provide image-guided therapies [41][42]. Both MRI and optical imaging are noninvasive imaging modalities. Magnetic resonance imaging provides high spatial resolution but lacks sensitivity. Optical

A review of defect engineering, ion implantation, and nanofabrication using the helium ion microscope

• Frances I. Allen

Beilstein J. Nanotechnol. 2021, 12, 633–664, doi:10.3762/bjnano.12.52

• , namely site-specific ion-enhanced etching with high spatial resolution. Similarly, site-selective etching of MoS2 has been demonstrated using helium ion irradiation to create defective regions that become activated for oxygen adsorption and subsequent oxidative etching when heated in air [68]. Helium ion

A review on nanostructured silver as a basic ingredient in medicine: physicochemical parameters and characterization

• Gabriel M. Misirli,
• Kishore Sridharan and
• Shirley M. P. Abrantes

Beilstein J. Nanotechnol. 2021, 12, 440–461, doi:10.3762/bjnano.12.36

• complementary way, the size, distribution, shape heterogeneity, morphology, dispersion, and aggregation can be directly evaluated via TEM in which the high spatial resolution facilitates the investigation of the electronic structure and chemical composition [156]. However, the disadvantages other than the

Intracranial recording in patients with aphasia using nanomaterial-based flexible electronics: promises and challenges

• Qingchun Wang and
• Wai Ting Siok

Beilstein J. Nanotechnol. 2021, 12, 330–342, doi:10.3762/bjnano.12.27

• data from patients who suffered from pharmacoresistant focal epilepsies [45]. ECoG offers high spatial resolution. The ECoG grid and strip electrodes can cover a large area of the cortex, and as many as 100–200 electrodes can be used [42]. However, in actual applications, the clinical needs of the

The patterning toolbox FIB-o-mat: Exploiting the full potential of focused helium ions for nanofabrication

• Victor Deinhart,
• Lisa-Marie Kern,
• Jan N. Kirchhof,
• Sabrina Juergensen,
• Joris Sturm,
• Enno Krauss,
• Thorsten Feichtner,
• Sviatoslav Kovalchuk,
• Michael Schneider,
• Dieter Engel,
• Bastian Pfau,
• Bert Hecht,
• Kirill I. Bolotin,
• Stephanie Reich and
• Katja Höflich

Beilstein J. Nanotechnol. 2021, 12, 304–318, doi:10.3762/bjnano.12.25

• , other challenges such as small sputter rates and large interaction volumes persist. Therefore, 2D materials are an ideal platform for ion beam machining with light ions. The lack (or non-relevance) of the interaction volume allows for a high spatial resolution, enabling the fabrication of structural

Numerical analysis of vibration modes of a qPlus sensor with a long tip

• Kebei Chen,
• Zhenghui Liu,
• Yuchen Xie,
• Chunyu Zhang,
• Gengzhao Xu,
• Wentao Song and
• Ke Xu

Beilstein J. Nanotechnol. 2021, 12, 82–92, doi:10.3762/bjnano.12.7

• horizontally and vertically. The vibration characteristics of qPlus sensors with different tip sizes were studied. An optimized tip size was derived from obtained values of tip amplitude, ratio between vertical and lateral amplitude components, output current, and quality factor. For high spatial resolution

• extensively in the fields of physics, chemistry, and materials science to obtain images of high spatial resolution [4][5][6][7][8][9][10][11][12]. Most research under low-temperature and ultrahigh-vacuum (LT-UHV) conditions has been carried out using the first-order eigenmode of the qPlus sensor, which has a

Bio-imaging with the helium-ion microscope: A review

• Matthias Schmidt,
• James M. Byrne and
• Ilari J. Maasilta

Beilstein J. Nanotechnol. 2021, 12, 1–23, doi:10.3762/bjnano.12.1

• -SIMS remains in the development stage with few commercial systems available. However, they are potential game changers for the investigation of biological samples at high spatial resolution in combination with chemical characterisation. A first biological application was presented by Lovric et al. when