Enhancing the therapeutical potential of metalloantibiotics using nano-based delivery systems

• Alejandro Llamedo,
• Marina Cano,
• Raquel G. Soengas and
• Francisco J. García-Alonso

Beilstein J. Nanotechnol. 2025, 16, 1350–1366, doi:10.3762/bjnano.16.98

• higher light absorption, and greater photoemission output, resulting in enhanced bactericidal activity against S. aureus (Figure 7). The Ir-complex liposomes interact efficiently with 450 nm LED light, leading to ROS generation and subsequent bacterial inactivation at the site of an infected chronic skin

Ferroptosis induction by engineered liposomes for enhanced tumor therapy

• Alireza Ghasempour,
• Mohammad Amin Tokallou,
• Mohammad Reza Naderi Allaf,
• Mohsen Moradi,
• Hamideh Dehghan,
• Mahsa Sedighi,
• Mohammad-Ali Shahbazi and
• Fahimeh Lavi Arab

Beilstein J. Nanotechnol. 2025, 16, 1325–1349, doi:10.3762/bjnano.16.97

• transferrin receptor 1 (TFR1) during receptor-bound endocytosis. In addition to this pathway, iron absorption can also occur with the help of actin filaments, one of the components of the cytoskeleton, via the receptor (TFRC) [36]. The iron required by the cell, in the form of ferrous iron (Fe+2), is produced

• domains and thus provide suitable drug delivery targets to enhance absorption in particular areas [144]. Therefore, engineered liposomes have been developed to deliver targeted ferroptosis agents to tumor cells to improve tumor therapy, which is discussed here. For example, Celastrol (Cel) can inhibit the

Deep-learning recognition and tracking of individual nanotubes in low-contrast microscopy videos

• Vladimir Pimonov,
• Said Tahir and
• Vincent Jourdain

Beilstein J. Nanotechnol. 2025, 16, 1316–1324, doi:10.3762/bjnano.16.96

• selectivity, particularly kinetic selectivity. To address this, we developed a method based on in situ homodyne polarization microscopy (HPM), which is highly sensitive and can detect changes in optical absorption caused by a single carbon nanotube. The technique allows for imaging tens to hundreds of

• adds useful information to the video. Additionally, differential videos capture other processes causing local changes in optical absorption. For instance, if the nanotube structure (also called helicity or chirality) changes during growth, this manifests as a second segment moving synchronously with

• the first one: The new chirality appears either as a bright segment if it has lower optical absorption, or as a dark segment otherwise. If the nanotube switches from growth to shrinkage, it appears as a single bright segment moving backward, corresponding to lower optical absorption [20]. We developed

Wavelength-dependent correlation of LIPSS periodicity and laser penetration depth in stainless steel

• Nitin Chaudhary,
• Chavan Akash Naik,
• Shilpa Mangalassery,
• Jai Prakash Gautam and
• Sri Ram Gopal Naraharisetty

Beilstein J. Nanotechnol. 2025, 16, 1302–1315, doi:10.3762/bjnano.16.95

• modulation of the net localized energy distribution on the surface, and this field absorption is manifested as LIPSS on the surface. This process depends on several experimental factors, namely, incident wavelength, polarization, material dielectric, dielectric, fluence of the laser, pulse width, repetition

• absorption in the metal and scattering in other directions, which depend on the properties of the metal [43]. The penetration depth of SPPs into the metal measures how far the electric field of the SPP decays exponentially inside the metal. Ash and colleagues reported the impact of wavelength and beam width

• geometry. It can also depend on the optical properties of the material, such as the refractive index, absorption coefficient, reflectivity, and laser parameters, such as the wavelength, pulse duration, fluence, incidence angle, and polarization [64]. Generally, penetration depth increases with increasing

Enhancing the photoelectrochemical performance of BiOI-derived BiVO₄ films by controlled-intensity current electrodeposition

• Huu Phuc Dang,
• Khanh Quang Nguyen,
• Nguyen Thi Mai Tho and
• Tran Le

Beilstein J. Nanotechnol. 2025, 16, 1289–1301, doi:10.3762/bjnano.16.94

• limited by material challenges, including insufficient light absorption, high electron–hole recombination rates, and poor stability under operating conditions [5][6]. Among various semiconductor materials, bismuth vanadate (BiVO4) has attracted considerable interest due to its strong visible light

• absorption, moderate bandgap (≈2.4 eV), high theoretical photocurrent density (≈7.5 mA·cm−2), and chemical stability in aqueous environments [7][8][9]. Nevertheless, BiVO4 suffers from intrinsic drawbacks such as low charge carrier mobility, limited conductivity, and rapid recombination of photogenerated

• . Characteristics of materials X-ray diffraction (XRD, Bruker D8 Advance) and Raman spectroscopy (LabRAM Odyssey Semiconductor) were used to analyze the crystal structures of photoanodes. UV–vis absorption spectra were obtained using a Cary 60 spectrophotometer. X-ray photoelectron spectroscopy (XPS, VG ESCALAB250

Acrocomia aculeata oil-loaded nanoemulsion: development, anti-inflammatory properties, and cytotoxicity evaluation

• Verónica Bautista-Robles,
• Hady Keita,
• Edgar Julián Paredes Gamero,
• Layna Tayná Brito Leite,
• Jessica de Araújo Isaías Muller,
• Mônica Cristina Toffoli Kadri,
• Ariadna Lafourcade Prada and
• Jesús Rafael Rodríguez Amado

Beilstein J. Nanotechnol. 2025, 16, 1277–1288, doi:10.3762/bjnano.16.93

• counterpart [47]. The superior pharmacological response of the nanoemulsion may be attributed to the nanoscale droplet size, which increases the surface area-to-volume ratio, enhances solubility and stability, and promotes rapid absorption and cellular uptake [56]. The nanometric scale facilitates more

Better together: biomimetic nanomedicines for high performance tumor therapy

• Imran Shair Mohammad,
• Gizem Kursunluoglu,
• Anup Kumar Patel,
• Hafiz Muhammad Ishaq,
• Cansu Umran Tunc,
• Dilek Kanarya,
• Mubashar Rehman,
• Omer Aydin and
• Yin Lifang

Beilstein J. Nanotechnol. 2025, 16, 1246–1276, doi:10.3762/bjnano.16.92

Functional bio-packaging enhanced with nanocellulose from rice straw and cinnamon essential oil Pickering emulsion for fruit preservation

• Tuyen B. Ly,
• Duong D. T. Nguyen,
• Hieu D. Nguyen,
• Yen T. H. Nguyen,
• Bup T. A. Bui,
• Kien A. Le and
• Phung K. Le

Beilstein J. Nanotechnol. 2025, 16, 1234–1245, doi:10.3762/bjnano.16.91

• microbial access [7]. PVA also exhibits superior biocompatibility as evidenced by its high safety threshold (LD50 of 15–20 g·kg−1), low systemic absorption, absence of mutagenic effects, and established medical applications, making it a reliable choice for biopackaging without concerns of harmful

• characteristic peaks confirm the presence of functional groups associated with PE-CEO and polymer interactions. The broad absorption band around 3300 cm−1 corresponds to O–H stretching vibrations, indicating hydrogen bonding between the biopolymer and PE-CEO components [24]. The intensity of the peaks at 1730 cm

• materials (BP, rBP, and rCBP) was observed using a scanning electron microscope (SEM), model Primas E (US). The samples were coated with Pt for 30 s prior to measurement. Bioactive properties UV absorption. Transparency and UV absorption of the films were determined using UV–vis spectroscopy in the

Hydrogels and nanogels: effectiveness in dermal applications

• Jéssica da Cruz Ludwig,
• Diana Fortkamp Grigoletto,
• Daniele Fernanda Renzi,
• Wolf-Rainer Abraham,
• Daniel de Paula and
• Najeh Maissar Khalil

Beilstein J. Nanotechnol. 2025, 16, 1216–1233, doi:10.3762/bjnano.16.90

• stability, absorption, and biodistribution impairments. Among the DDSs, we can highlight hydrogels and nanogels, which are easy to obtain, show good biocompatibility, and have several applications in the design of drug carriers for dermal and ocular administration. In this review, we introduce a brief

• [20][21], drug monitoring in biological fluids [22], CO2 absorption from the atmosphere [23], dye removal from industrial effluents [24], cavity-prevention in oral products [25], insect repellent coating for textiles [26], lead detection in water reservoirs [27], production of vaccines [28], and

• angiogenic factor associated with the tumor, called thymidine phosphorylase (dTfdPase), thus minimizing the exposure of healthy tissues to 5-FU [216]. Biodegradable polymers are widely used in nanotechnology to develop different systems due to their advantages, such as greater absorption [218][219] and high

Investigation of the solubility of protoporphyrin IX in aqueous and hydroalcoholic solvent systems

• Michelly de Sá Matsuoka,
• Giovanna Carla Cadini Ruiz,
• Marcos Luciano Bruschi and
• Jéssica Bassi da Silva

Beilstein J. Nanotechnol. 2025, 16, 1209–1215, doi:10.3762/bjnano.16.89

• its bioavailability and light absorption capacity will be increased [5]. To overcome this problem, the development of drug delivery systems, such as poloxamer-based ones, has played an important role on the delivery of dyes for PDT [8][9][10]. Poloxamers are triblock copolymers with thermosensitive

Chitosan nanocomposite containing rotenoids: an alternative bioinsecticidal approach for the management of Aedes aegypti

• Maria A. A. Bertonceli,
• Vitor D. C. Cristo,
• Ivo J. Vieira,
• Francisco J. A. Lemos,
• Arnoldo R. Façanha,
• Raimundo Braz-Filho,
• Gustavo V. T. Batista,
• Luis G. M. Basso,
• Sérgio H. Seabra,
• Thalya S. R. Nogueira,
• Felipe F. Moreira,
• Arícia L. E. M. Assis,
• Antônia E. A. Oliveira and
• Kátia V. S. Fernandes

Beilstein J. Nanotechnol. 2025, 16, 1197–1208, doi:10.3762/bjnano.16.88

• between the rotenoids and the nanocomposite matrix was obtained through Fourier-transform infrared (FTIR) spectroscopy. Figure 3A shows the FTIR spectra of CS/TPP-β-CD, CS/TPP-β-CD loaded with rotenoids (CS/TPP-β-CD-rot), and pure rotenoids. All three spectra display a broad absorption band in the 3600

• region, while glycosidic linkages and methoxyl groups contribute bands in the 1300–1000 cm−1 range [25][26]. Figure 3B presents a spectral subtraction analysis between CS/TPP-β-CD and CS/TPP-β-CD-rot, clearly revealing absorption features from the encapsulated rotenoids in the functionalized

• rotenoids, empty nanoparticles (CS/TPP-β-CD), and rotenoid-loaded nanoparticles (CS/TPP-β-CD-rot). B) Comparison between the spectrum of in natura rotenoids and the differential spectrum obtained by subtracting the CS/TPP-β-CD spectrum from that of CS/TPP-β-CD-rot, highlighting the characteristic absorption

Electronic and optical properties of chloropicrin adsorbed ZnS nanotubes: first principle analysis

• Prakash Yadav,
• Boddepalli SanthiBhushan and
• Anurag Srivastava

Beilstein J. Nanotechnol. 2025, 16, 1184–1196, doi:10.3762/bjnano.16.87

• , optical absorption, and optical conductivity of the ZnS NT-CP system. Our findings reveal that the interaction between CP and ZnS NT induces notable changes in the electronic and optical properties of the nanotube, including a substantial bandgap reduction of up to ≈40% for the specific orientation A. The

• adsorption energy ranges from −0.389 to −0.657 eV, indicating weak physisorption. The Mulliken charge transfer varies between 0.06e and 0.109e, confirming effective but nondestructive interaction. A favorable recovery time of ≈3.533 μs at room temperature, along with a significant red shift in the absorption

• highly toxic chemical warfare agent, remains an area with untapped potential. Addressing this gap, the present work constructs an armchair ZnS NT to investigate its adsorption configurations, charge transfer, band structure, density of states, optical absorption, and optical conductivity using a density

Towards a quantitative theory for transmission X-ray microscopy

• James G. McNally,
• Christoph Pratsch,
• Stephan Werner,
• Stefan Rehbein,
• Andrew Gibbs,
• Jihao Wang,
• Thomas Lunkenbein,
• Peter Guttmann and
• Gerd Schneider

Beilstein J. Nanotechnol. 2025, 16, 1113–1128, doi:10.3762/bjnano.16.82

• that this model produces good qualitative agreement with our 3D measurements of 60 nm gold nanospheres, but only if both β and δ for the complex refractive index n = 1 – δ + iβ of gold are included in the model. This shows that both absorption and phase properties of the specimen influence the acquired

• TXM image. The qualitative agreement improves if we incorporate a small tilt into the condenser illumination relative to the optical axis, implying a small misalignment in the microscope. Finally, in quantitative comparisons, we show that the model predicts the nanosphere’s expected absorption as

• determined by Beer’s law, whereas the microscope underestimates this absorption by 10–20%. This surprising observation highlights the need for future work to identify the microscope feature(s) that lead to this quantitative discrepancy. Keywords: 3D imaging; mathematical model; Mie theory; nanoparticle

Influence of ion beam current on the structural, optical, and mechanical properties of TiO₂ coatings: ion beam-assisted vs conventional electron beam evaporation

• Agata Obstarczyk and
• Urszula Wawrzaszek

Beilstein J. Nanotechnol. 2025, 16, 1097–1112, doi:10.3762/bjnano.16.81

• energy of the thin film coatings strongly depends on the conditions and deposition methods. To complete analysis of the bandgap structure, the Urbach energy was evaluated based on the logarithmic plot of the absorption coefficient vs photon energy (Figure 5d–f). The slope of the linear dependence of ln α

• thin film coatings (Figure 4) and was proven in Figure 6a. The low value of the imaginary part of the refractive index, also known as extinction coefficient (Figure 6b), ranging from 2.12·10−3 to 4.64·10−3, indicates low light absorption in the studied thin films [58]. According to [6], TiO2 films

• in an increase in the refractive index. In addition, the low values of the extinction coefficient (from 2.12·10−3 to 4.64·10−3) indicated minimal light absorption in the tested films. The results of the nanoindentation studies showed that the hardness of thin films deposited by the conventional EBE

Fabrication of metal complex phthalocyanine and porphyrin nanoparticle aqueous colloids by pulsed laser fragmentation in liquid and their potential application to a photosensitizer for photodynamic therapy

• Taisei Himeda,
• Risako Kunitomi,
• Ryosuke Nabeya,
• Tamotsu Zako and
• Tsuyoshi Asahi

Beilstein J. Nanotechnol. 2025, 16, 1088–1096, doi:10.3762/bjnano.16.80

• fragmentation in liquids; reactive oxygen species generation; Introduction Porphyrins and phthalocyanines (Pcs), exhibiting intense absorption in the visible to near-infrared (NIR) regions, are well studied as photosensitizers in photodynamic therapy (PDT) [1]. Especially, Pcs absorb strongly light in the

• cuvette (1 × 1 × 4 cm3) and irradiated with nanosecond laser pulses (532 nm wavelength, 6 ns full-width at half-maximum, 10 Hz repetition rate, fluence = 140 mJ·cm−2 per pulse) under stirring with a magnetic stirrer. The nanoparticle generation was examined by measuring the absorption spectrum with a USB

• spectrometer, and the sample was irradiated with laser pulses until the absorption spectrum stopped changing. The sample was muddy blue, and most of the AlClPc precipitated to the bottom of the cuvette before laser irradiation. After irradiation with nanosecond laser pulses for 40 min (Figure 2a), the sample

Single-layer graphene oxide film grown on α-Al₂O₃(0001) for use as an adsorbent

• Shiro Entani,
• Mitsunori Honda,
• Masaru Takizawa and
• Makoto Kohda

Beilstein J. Nanotechnol. 2025, 16, 1082–1087, doi:10.3762/bjnano.16.79

• deposition; electronic state analysis; graphene oxide; X-ray absorption fine structure; Introduction Graphene oxide (GO) is oxidized graphene and its surface and periphery are partially modified by epoxy, hydroxy, and carboxy functional groups [1][2]. GO can be thinned to a monolayer of one carbon atom and

• findings reported in [22]. At the same time, the significant changes arose after the oxidization of SLG in the C 1s core XPS and C K-edge near-edge X-ray absorption fine structure (NEXAFS) spectra. Figure 3a shows C 1s XPS spectra of SLG and SLGO. In SLG, an intense peak is observed at 283.4 eV. The C 1s

Piezoelectricity of hexagonal boron nitrides improves bone tissue generation as tested on osteoblasts

• Sevin Adiguzel,
• Nilay Cicek,
• Zehra Cobandede,
• Feray B. Misirlioglu,
• Hulya Yilmaz and
• Mustafa Culha

Beilstein J. Nanotechnol. 2025, 16, 1068–1081, doi:10.3762/bjnano.16.78

• the B–N vibrational mode (E2g) as consistent with the literature [44][45]. Due to its highly transparent properties, hBN can transmit 99% of light in the 250–900 nm region. The UV–vis absorption peak at 203 nm is shown in Supporting Information File 1, Figure S3 (e), corresponding to its optical

• )] and the peak that appeared at 715 cm−1 correspond to [A1(LO), E(LO)] [54]. The UV–vis spectrum presented in Supporting Information File 1, Figure S4 (c) showed an absorption edge increase of BaTiO3 at around 300 nm [55]. Supporting Information File 1, Figure S4 (d) shows that the DLS spectrum provides

Soft materials nanoarchitectonics: liquid crystals, polymers, gels, biomaterials, and others

• Katsuhiko Ariga

Beilstein J. Nanotechnol. 2025, 16, 1025–1067, doi:10.3762/bjnano.16.77

• . Consequently, rod-shaped gold nanoparticles have been the subject of considerable interest with regard to their potential use in optical antennas, sensitive biosensors, and medical applications. This is due to their strong plasmonic absorption in the visible–near infrared region, which is caused by electronic

Multifunctional properties of bio-poly(butylene succinate) reinforced with multiwalled carbon nanotubes

• Volodymyr Krasinskyi,
• Krzysztof Bajer,
• Ludmila Dulebova,
• Nickolas Polychronopoulos,
• Oksana Krasinska and
• Daniel Kaczor

Beilstein J. Nanotechnol. 2025, 16, 1014–1024, doi:10.3762/bjnano.16.76

• and water absorption of PBS; however, it significantly influences surface wettability and tribological properties (Table 3). The dynamic and static coefficients of friction for the PBS/CNT_0.5 nanocomposite are 1.7 and 1.3–1.7 times lower, respectively, than those of the pure PBS. The surface

• water absorption (n) was measured following ISO 62:2008 “Plastics – Determination of Water Absorption”, using film samples of a square shape (50 × 50 mm2) with a thickness of 350 µm. The surface tension or wettability (σ) of the films was measured according to ISO 8296:2003 “Plastics – Film and Sheeting

A calix[4]arene-based supramolecular nanoassembly targeting cancer cells and triggering the release of nitric oxide with green light

• Cristina Parisi,
• Loredana Ferreri,
• Tassia J. Martins,
• Francesca Laneri,
• Samantha Sollima,
• Antonina Azzolina,
• Antonella Cusimano,
• Nicola D’Antona,
• Grazia M. L. Consoli and
• Salvatore Sortino

Beilstein J. Nanotechnol. 2025, 16, 1003–1013, doi:10.3762/bjnano.16.75

• . Compound 2 and its non-nitrosated precursor 2b were characterized by 1D NMR (Figures S8,S9, Supporting Information File 1). Self-assembling and spectroscopic properties of 1 Due to the polycationic structure, compound 1 showed good water solubility as evidenced by its absorption spectrum dominated by the

• in diameter with a polydispersity index (PI) of ca. 0.4 (inset Figure 1A). This means the sample has a moderate range of particle sizes, however suitable for drug delivery applications. Figure 1B shows the fluorescence emission spectra of a water solution of 1. Similar to the absorption, the spectrum

• room temperature for at least 48 h, as evidenced by the unaltered values of the hydrodynamic diameter and the unchanged absorption and emission features over this time window. Cytotoxicity and cell targeting properties of 1 The effects of the nanoassembly of 1 on cell viability were evaluated on

Time-resolved probing of laser-induced nanostructuring processes in liquids

• Maximilian Spellauge,
• David Redka,
• Mianzhen Mo,
• Changyong Song,
• Heinz Paul Huber and
• Anton Plech

Beilstein J. Nanotechnol. 2025, 16, 968–1002, doi:10.3762/bjnano.16.74

• parameters, improving reproducibility, and tailoring material properties for specific applications. Ultrafast optical techniques such as transient absorption spectroscopy (TAS) [84][85][86][87] have been applied to investigate the influence of the liquid environment on the energy relaxation processes of

• to liquid) should lead to restructuring. In a simple model, the laser energy is converted into heat that will be localized in the absorbing part within the laser penetration depth. Absorption is linear as expressed by the (known) absorption cross section. In the model by Takami et al. [46], which is

• macroscopic suspension containing NPs or reflection from a photoexcited NP is determined by absorption as well as scattering, several structural processes may contribute to a change in signal. Metal NPs show SPR linked to coherent excitation of electrons in the conduction band. Its position and width are

Synthesis of biowaste-derived carbon-dot-mediated silver nanoparticles and the evaluation of electrochemical properties for supercapacitor electrodes

• Navya Kumari Tenkayala,
• Chandan Kumar Maity,
• Md Moniruzzaman and
• Subramani Devaraju

Beilstein J. Nanotechnol. 2025, 16, 933–943, doi:10.3762/bjnano.16.71

• evidenced from the progressive color change of the solution as shown by surface plasmon resonance (SPR). Structural and morphological analysis The optical properties of PG-CDs and PG-CDs-AgNPs were studied using UV–visible spectroscopy and photoluminescence (PL) spectroscopy. An absorption peak at 275 nm

• was visualized in the UV–visible absorption spectrum of the PG-CDs, which is represented in Figure 1a. This peak might be accredited to the π–π* transition of conjugated (Csp²=Csp²) aromatic domain of the PG-CDs [24]. Under the ultraviolet illuminator (365 nm), the brownish/red aqueous solution of the

• absorption bands of PG-CDs-AgNPs was acquired at various time intervals to study the production and growth of nanoparticles over time. The gradual growth of PG-CDs-AgNPs has been checked and depicted in Figure 1b. The SPR peak was noticed within 2 h of reaction with PG-CDs, with a visible change in color of

Heat-induced transformation of nickel-coated polycrystalline diamond film studied in situ by XPS and NEXAFS

• Olga V. Sedelnikova,
• Yuliya V. Fedoseeva,
• Dmitriy V. Gorodetskiy,
• Yuri N. Palyanov,
• Elena V. Shlyakhova,
• Eugene A. Maksimovskiy,
• Anna A. Makarova,
• Lyubov G. Bulusheva and
• Aleksandr V. Okotrub

Beilstein J. Nanotechnol. 2025, 16, 887–898, doi:10.3762/bjnano.16.67

• thin nickel film deposited by thermal evaporation. The graphitization of diamond with and without a nickel coating as a result of high-vacuum annealing at a temperature of about 1100 °C was studied in situ using synchrotron-based X-ray photoelectron spectroscopy (XPS) and near-edge X-ray absorption

• . Keywords: graphitization; near-edge X-ray absorption fine structure spectroscopy; nickel coating; polycrystalline diamond film; single-crystal diamond; X-ray photoelectron spectroscopy; Introduction Diamond and graphite, both composed entirely of carbon atoms, exhibit vastly different properties due to

• requires a detailed study. HRTEM has proven very useful for investigating the graphite–diamond interface [19][24]. However, it provides information about local morphology and ordering of diamond surface and graphite layers. X-ray photoelectron spectroscopy (XPS) and near-edge X-ray absorption fine

Ar⁺ implantation-induced tailoring of RF-sputtered ZnO films: structural, morphological, and optical properties

• Manu Bura,
• Divya Gupta,
• Arun Kumar and
• Sanjeev Aggarwal

Beilstein J. Nanotechnol. 2025, 16, 872–886, doi:10.3762/bjnano.16.66

• fundamental absorption edge. With the increase in argon ion fluence, the diffuse reflectance was found to decrease, which is related to the decrease in the surface RMS roughness also reported in AFM analysis. Thus, implanted ZnO films can be employed as an antireflection coating in optoelectronic devices [38

• ]. The diffuse reflectance of the films can be used to calculate the associated Kubelka–Munk function, which is equivalent to the absorption spectra [39][40]. This paves the way to calculate the optical bandgap of the implanted films. The Kubelka–Munk function F(R) is determined employing diffuse

• reflectance by the following relation [41]: Here R is the diffuse reflectance of the samples; s and α correspond to scattering and absorption coefficients, respectively. The scattering coefficient does not depend on the wavelength. Thus, F(R) becomes proportional to α. It has been observed that with the rise

Insights into the electronic and atomic structures of cerium oxide-based ultrathin films and nanostructures using high-brilliance light sources

• Paola Luches and
• Federico Boscherini

Beilstein J. Nanotechnol. 2025, 16, 860–871, doi:10.3762/bjnano.16.65

• light sources, such as synchrotrons and free-electron lasers, allow researchers to probe the structural, electronic, and dynamic properties of functional materials at an unprecedented level of detail. Techniques like X-ray photoelectron spectroscopy and X-ray absorption spectroscopy, can reveal atomic

• absorption spectroscopy to explain the factors influencing the material’s reducibility, with particular focus on dimensionality effects and on metal–oxide interaction, and the interaction with molecules. The potential of studies conducted under ambient pressure conditions is highlighted, and, finally, the

• perspectives offered by the ultrahigh brilliance and ultrashort free-electron laser pulses for dynamic studies of the processes that take place upon photoexcitation are discussed. Keywords: cerium oxide; free-electron lasers; thin films; X-ray absorption spectroscopy; X-ray photoelectron spectroscopy