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Search for "chemical synthesis" in Full Text gives 74 result(s) in Beilstein Journal of Nanotechnology.

Fabrication of silver nanoisland films by pulsed laser deposition for surface-enhanced Raman spectroscopy

  • Bogusław Budner,
  • Mariusz Kuźma,
  • Barbara Nasiłowska,
  • Bartosz Bartosewicz,
  • Malwina Liszewska and
  • Bartłomiej J. Jankiewicz

Beilstein J. Nanotechnol. 2019, 10, 882–893, doi:10.3762/bjnano.10.89

Graphical Abstract
  • nanoparticle films [12][13][14]. Metallic NPs of different sizes and shapes are prepared in solution mainly by chemical synthesis using various reducing agents and conditions [13]. However, physical methods such as laser ablation are also often used [15]. Other examples of nanoparticle fabrication using
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Published 16 Apr 2019

Sub-wavelength waveguide properties of 1D and surface-functionalized SnO2 nanostructures of various morphologies

  • Venkataramana Bonu,
  • Binaya Kumar Sahu,
  • Arindam Das,
  • Sankarakumar Amirthapandian,
  • Sandip Dhara and
  • Harish C. Barshilia

Beilstein J. Nanotechnol. 2019, 10, 379–388, doi:10.3762/bjnano.10.37

Graphical Abstract
  • this context, there have been attempts to understand the relevant thermodynamic aspects and to evaluate the impact of parameters like temperature, pressure, and precursor concentration in the growth process [8][20][21]. Apart from different approaches for wet chemical synthesis [22] of SnO2 NSs, the
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Published 07 Feb 2019

Heating ability of magnetic nanoparticles with cubic and combined anisotropy

  • Nikolai A. Usov,
  • Mikhail S. Nesmeyanov,
  • Elizaveta M. Gubanova and
  • Natalia B. Epshtein

Beilstein J. Nanotechnol. 2019, 10, 305–314, doi:10.3762/bjnano.10.29

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  • , different methods of chemical synthesis of iron oxide nanoparticles give particles of various characteristic diameters [3] that are usually far from the optimal theoretical values. Another important issue is the nature of the magnetic anisotropy of individual nanoparticles of the assembly. Are the magnetic
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Published 29 Jan 2019

Wet chemistry route for the decoration of carbon nanotubes with iron oxide nanoparticles for gas sensing

  • Hussam M. Elnabawy,
  • Juan Casanova-Chafer,
  • Badawi Anis,
  • Mostafa Fedawy,
  • Mattia Scardamaglia,
  • Carla Bittencourt,
  • Ahmed S. G. Khalil,
  • Eduard Llobet and
  • Xavier Vilanova

Beilstein J. Nanotechnol. 2019, 10, 105–118, doi:10.3762/bjnano.10.10

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  • Institution for Research and Advanced Studies (ICREA) via the ICREA Academia Award. MS is a FRS Postdoctoral Researcher, CB is Research Associate at the FRS-FNRS. Authors Contributions The chemical synthesis for the CNT decoration was performed by H. M. Elnabawy under the supervision of B. Anis, M. Fedawy
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Published 09 Jan 2019

Threshold voltage decrease in a thermotropic nematic liquid crystal doped with graphene oxide flakes

  • Mateusz Mrukiewicz,
  • Krystian Kowiorski,
  • Paweł Perkowski,
  • Rafał Mazur and
  • Małgorzata Djas

Beilstein J. Nanotechnol. 2019, 10, 71–78, doi:10.3762/bjnano.10.7

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  • Mateusz Mrukiewicz Krystian Kowiorski Pawel Perkowski Rafal Mazur Malgorzata Djas Institute of Applied Physics, Military University of Technology, 00-908 Warsaw, Poland Department of Chemical Synthesis and Flake Graphene, Institute of Electronic Materials Technology, 01-919 Warsaw, Poland 10.3762
  • Chemical Synthesis and Flake Graphene, Institute of Electronic Materials Technology, Warsaw, Poland. Then, the GO flakes in water were transferred by solvent exchange into isopropanol (IPA) and were sonicated to achieve a stable GO-IPA suspension of a known concentration. The structure of the flakes was
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Published 07 Jan 2019

Size-selected Fe3O4–Au hybrid nanoparticles for improved magnetism-based theranostics

  • Maria V. Efremova,
  • Yulia A. Nalench,
  • Eirini Myrovali,
  • Anastasiia S. Garanina,
  • Ivan S. Grebennikov,
  • Polina K. Gifer,
  • Maxim A. Abakumov,
  • Marina Spasova,
  • Makis Angelakeris,
  • Alexander G. Savchenko,
  • Michael Farle,
  • Natalia L. Klyachko,
  • Alexander G. Majouga and
  • Ulf Wiedwald

Beilstein J. Nanotechnol. 2018, 9, 2684–2699, doi:10.3762/bjnano.9.251

Graphical Abstract
  • diameters of 6–44 nm (Fe3O4) and 3–11 nm (Au) were prepared by high temperature, wet chemical synthesis. High-quality Fe3O4 nanocrystals with bulk-like magnetic behavior were obtained as confirmed by the presence of the Verwey transition. The 25 nm diameter Fe3O4–Au hybrid nanomaterial sample (in aqueous
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Published 16 Oct 2018

Enhanced antineoplastic/therapeutic efficacy using 5-fluorouracil-loaded calcium phosphate nanoparticles

  • Shanid Mohiyuddin,
  • Saba Naqvi and
  • Gopinath Packirisamy

Beilstein J. Nanotechnol. 2018, 9, 2499–2515, doi:10.3762/bjnano.9.233

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  • , while aqueous-dissolved 5-FU comprises a dispersed phase. The calculated drug loading efficiency of 5-FU in CaP nanoparticles was 64%, which represents an improved drug encapsulation efficiency. The final yield of the chemical synthesis was found to be 10 mg/100 mL. UV–visible spectroscopic studies The
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Published 20 Sep 2018

Synthesis of rare-earth metal and rare-earth metal-fluoride nanoparticles in ionic liquids and propylene carbonate

  • Marvin Siebels,
  • Lukas Mai,
  • Laura Schmolke,
  • Kai Schütte,
  • Juri Barthel,
  • Junpei Yue,
  • Jörg Thomas,
  • Bernd M. Smarsly,
  • Anjana Devi,
  • Roland A. Fischer and
  • Christoph Janiak

Beilstein J. Nanotechnol. 2018, 9, 1881–1894, doi:10.3762/bjnano.9.180

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  • diameters of (1.5 ± 0.5) to (5 ± 1) nm. The characterization was completed by energy-dispersive X-ray spectroscopy (EDX). Keywords: ionic liquids; metal amidinates; rare-earth metal-fluoride nanoparticles; rare-earth metal nanoparticles; soft wet-chemical synthesis; Introduction Rare-earth (RE) elements
  • -methylimidazolium bis(trifluoromethylsulfonyl)imide ([BMIm][NTf2]) or propylene carbonate (PC) as reaction media RE-NPs were produced. This is an unusual and quite interesting result that we wish to highlight at this point. There exist only few reports on the wet-chemical synthesis of nanoparticles of rare-earth
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Published 28 Jun 2018

Cr(VI) remediation from aqueous environment through modified-TiO2-mediated photocatalytic reduction

  • Rashmi Acharya,
  • Brundabana Naik and
  • Kulamani Parida

Beilstein J. Nanotechnol. 2018, 9, 1448–1470, doi:10.3762/bjnano.9.137

Graphical Abstract
  • transformation for the fine chemical synthesis [39][40][41][42] and (v) photodegradation of pollutants [43][44][45][46][47][48][49]. Semiconductor-based photocatalysis proceeds through following three steps: (1) absorption of light; (2) separation and transport of charge carriers; and (3) redox reactions on the
  • chemical synthesis Photocatalytic, selective, organic transformations are currently preferred over the conventional processes for synthesis of fine chemicals basically due to two reasons. The first one is to restrict the use of environmentally detrimental chemical reagents such as heavy metal catalysts
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Review
Published 16 May 2018

Review on nanoparticles and nanostructured materials: history, sources, toxicity and regulations

  • Jaison Jeevanandam,
  • Ahmed Barhoum,
  • Yen S. Chan,
  • Alain Dufresne and
  • Michael K. Danquah

Beilstein J. Nanotechnol. 2018, 9, 1050–1074, doi:10.3762/bjnano.9.98

Graphical Abstract
  • useful in a nanomedicine application as they were found to reduce potential cellular toxicity [152]. However, the major drawbacks of these NPs are that they require more time for synthesis, are difficult to filter, and produce a low yield of NPs, as compared to chemical synthesis [153]. Novel nano
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Published 03 Apr 2018

The rational design of a Au(I) precursor for focused electron beam induced deposition

  • Ali Marashdeh,
  • Thiadrik Tiesma,
  • Niels J. C. van Velzen,
  • Sjoerd Harder,
  • Remco W. A. Havenith,
  • Jeff T. M. De Hosson and
  • Willem F. van Dorp

Beilstein J. Nanotechnol. 2017, 8, 2753–2765, doi:10.3762/bjnano.8.274

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  • , University of Ghent, B-9000 Ghent, Belgium Uniresearch B.V., 2628 XG Delft, Netherlands 10.3762/bjnano.8.274 Abstract Au(I) complexes are studied as precursors for focused electron beam induced processing (FEBIP). FEBIP is an advanced direct-write technique for nanometer-scale chemical synthesis. The
  • ; Introduction Electron microscopes, typically used for imaging and analysis, can be turned into a platform for nanoscale chemical synthesis using electron beam induced chemistry. The electron beam can act as a pen or an eraser on any solid sample, using a technique called focused electron beam induced
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Published 20 Dec 2017

Synthesis of metal-fluoride nanoparticles supported on thermally reduced graphite oxide

  • Alexa Schmitz,
  • Kai Schütte,
  • Vesko Ilievski,
  • Juri Barthel,
  • Laura Burk,
  • Rolf Mülhaupt,
  • Junpei Yue,
  • Bernd Smarsly and
  • Christoph Janiak

Beilstein J. Nanotechnol. 2017, 8, 2474–2483, doi:10.3762/bjnano.8.247

Graphical Abstract
  • constant, ILs are an ideal media for microwave reactions and for the stabilization of M-NPs [34][35][36][37]. Soft wet-chemical synthesis in organic solvents from metal-organic complexes is an essential method to obtain metal or metal alloy nanoparticles [38][39][40][41][42][43][44][45][46][47][48][49][50
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Published 22 Nov 2017

Calcium fluoride based multifunctional nanoparticles for multimodal imaging

  • Marion Straßer,
  • Joachim H. X. Schrauth,
  • Sofia Dembski,
  • Daniel Haddad,
  • Bernd Ahrens,
  • Stefan Schweizer,
  • Bastian Christ,
  • Alevtina Cubukova,
  • Marco Metzger,
  • Heike Walles,
  • Peter M. Jakob and
  • Gerhard Sextl

Beilstein J. Nanotechnol. 2017, 8, 1484–1493, doi:10.3762/bjnano.8.148

Graphical Abstract
  • on synthesis and characterization of multifunctional NPs based on CaF2. These NPs are produced by wet-chemical synthesis and doped with multiple ions leading to paramagnetism and fluorescence, making them suitable for T1-weighted MRI and PL microscopy. The characterization of the resulting NPs is
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Published 18 Jul 2017

Charge transport in organic nanocrystal diodes based on rolled-up robust nanomembrane contacts

  • Vineeth Kumar Bandari,
  • Lakshmi Varadharajan,
  • Longqian Xu,
  • Abdur Rehman Jalil,
  • Mirunalini Devarajulu,
  • Pablo F. Siles,
  • Feng Zhu and
  • Oliver G. Schmidt

Beilstein J. Nanotechnol. 2017, 8, 1277–1282, doi:10.3762/bjnano.8.129

Graphical Abstract
  • optoelectronics and spintronics [4][5][6]. Organic nanocrystals have drawn much attention in the community because high quality material can be efficiently generated by controlling the nanoscale physical growth and/or chemical synthesis process [7][8][9][10]. The deposition of organic conjugated molecules is
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Published 19 Jun 2017

Enhanced catalytic activity without the use of an external light source using microwave-synthesized CuO nanopetals

  • Govinda Lakhotiya,
  • Sonal Bajaj,
  • Arpan Kumar Nayak,
  • Debabrata Pradhan,
  • Pradip Tekade and
  • Abhimanyu Rana

Beilstein J. Nanotechnol. 2017, 8, 1167–1173, doi:10.3762/bjnano.8.118

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  • , University of Twente, 7500 AE, Enschede, Netherlands 10.3762/bjnano.8.118 Abstract We report enhanced catalytic activity of CuO nanopetals synthesized by microwave-assisted wet chemical synthesis. The catalytic reaction of CuO nanopetals and H2O2 was studied with the application of external light source and
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Published 30 May 2017

Optical response of heterogeneous polymer layers containing silver nanostructures

  • Miriam Carlberg,
  • Florent Pourcin,
  • Olivier Margeat,
  • Judikaël Le Rouzo,
  • Gérard Berginc,
  • Rose-Marie Sauvage,
  • Jörg Ackermann and
  • Ludovic Escoubas

Beilstein J. Nanotechnol. 2017, 8, 1065–1072, doi:10.3762/bjnano.8.108

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  • properties. Thin film layers with inclusions of differently shaped nanoparticles, such as nanospheres and nanoprisms, and of different sizes, are optically characterized. The nanoparticles are produced by a simple chemical synthesis at room temperature in water. The plasmonic resonance peaks of the different
  • visible wavelength range [15]. Progress in the chemistry of NP synthesis allowed us to choose a chemical process adapted to our study that produces NPs of different shapes and sizes. Among different NP production methods, chemical synthesis is easy to implement and produces NPs at low cost. Standard
  • physical vapor deposition methods require high energy sources, such as lasers [16], whereas chemical synthesis produces, among other shapes, nanospheres and nanoprisms of different sizes in water at room temperature. Taking advantage of the size and shape versatility of this chemical synthesis, we aim to
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Published 16 May 2017

Synthesis of graphene–transition metal oxide hybrid nanoparticles and their application in various fields

  • Arpita Jana,
  • Elke Scheer and
  • Sebastian Polarz

Beilstein J. Nanotechnol. 2017, 8, 688–714, doi:10.3762/bjnano.8.74

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Published 24 Mar 2017

Performance of colloidal CdS sensitized solar cells with ZnO nanorods/nanoparticles

  • Anurag Roy,
  • Partha Pratim Das,
  • Mukta Tathavadekar,
  • Sumita Das and
  • Parukuttyamma Sujatha Devi

Beilstein J. Nanotechnol. 2017, 8, 210–221, doi:10.3762/bjnano.8.23

Graphical Abstract
  • colloidal CdS nanoparticles (NPs) by a sono-chemical synthesis using BSA as a biotemplate [24][25][26]. BSA can construct surface functionalized colloidal CdS QDs with modified optical properties as compared to its bulk form. This can further be employed to render stable dispersion of CdS NPs without
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Published 23 Jan 2017

Functionalized platinum nanoparticles with surface charge trigged by pH: synthesis, characterization and stability studies

  • Giovanna Testa,
  • Laura Fontana,
  • Iole Venditti and
  • Ilaria Fratoddi

Beilstein J. Nanotechnol. 2016, 7, 1822–1828, doi:10.3762/bjnano.7.175

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  • stabilizer to protect the platinum nanoparticles [18]. However, an efficient separation of the colloid from solution could be difficult to reach [19]. Among the synthetic approaches, wet chemical synthesis offers the opportunity to introduce a selected functionalization onto the NP surface and generally give
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Published 24 Nov 2016

Role of RGO support and irradiation source on the photocatalytic activity of CdS–ZnO semiconductor nanostructures

  • Suneel Kumar,
  • Rahul Sharma,
  • Vipul Sharma,
  • Gurunarayanan Harith,
  • Vaidyanathan Sivakumar and
  • Venkata Krishnan

Beilstein J. Nanotechnol. 2016, 7, 1684–1697, doi:10.3762/bjnano.7.161

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  • nanostructures. Keywords: catalytic properties; chemical synthesis; nanostructures; semiconductors; transmission electron microscopy (TEM); Introduction In the past decade, there has been an increased interest in the photocatalytic degradation of various kinds of organic pollutants in water and soil [1]. Many
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Published 11 Nov 2016

Novel roles for well-known players: from tobacco mosaic virus pests to enzymatically active assemblies

  • Claudia Koch,
  • Fabian J. Eber,
  • Carlos Azucena,
  • Alexander Förste,
  • Stefan Walheim,
  • Thomas Schimmel,
  • Alexander M. Bittner,
  • Holger Jeske,
  • Hartmut Gliemann,
  • Sabine Eiben,
  • Fania C. Geiger and
  • Christina Wege

Beilstein J. Nanotechnol. 2016, 7, 613–629, doi:10.3762/bjnano.7.54

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  • , spread, or interactions with host cells and tissues, viruses and VLPs have been regarded as a new class of biomaterials with an immense potential for applications as templates, building blocks and “smart” tools in chemical synthesis, medicine and nanotechnology since the turn of the century [1][2][3][4
  • . Virus particles of both spherical and helical shapes are accessible to a wide range of modifications, making them versatile tools e.g. for chemical synthesis, medical imaging or drug delivery applications, and biotemplates of variable shapes to serve as nanocarriers for functional units and building
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Published 25 Apr 2016

Linear and nonlinear optical properties of hybrid metallic–dielectric plasmonic nanoantennas

  • Mario Hentschel,
  • Bernd Metzger,
  • Bastian Knabe,
  • Karsten Buse and
  • Harald Giessen

Beilstein J. Nanotechnol. 2016, 7, 111–120, doi:10.3762/bjnano.7.13

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  • chemical synthesis and subsequent nanostructuring [74]. In order to increase a possible signal from the LiNbO3 particles, which intrinsically break inversion symmetry, we have to align them with respect to the antenna axis. As the particles are ferroelectric and exhibit a spontaneous macroscopic electric
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Published 26 Jan 2016

Peptide-equipped tobacco mosaic virus templates for selective and controllable biomineral deposition

  • Klara Altintoprak,
  • Axel Seidenstücker,
  • Alexander Welle,
  • Sabine Eiben,
  • Petia Atanasova,
  • Nina Stitz,
  • Alfred Plettl,
  • Joachim Bill,
  • Hartmut Gliemann,
  • Holger Jeske,
  • Dirk Rothenstein,
  • Fania Geiger and
  • Christina Wege

Beilstein J. Nanotechnol. 2015, 6, 1399–1412, doi:10.3762/bjnano.6.145

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  • because chemical synthesis or technical approaches applied at mild conditions commonly generate spherical structures [14]. Mineral nanofibers of predetermined size are of major importance for the preparation of functional films and extended 3D materials. Hence, anisotropic scaffolds such as high molecular
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Published 25 Jun 2015

Self-assembly of nanostructures and nanomaterials

  • Isabelle Berbezier and
  • Maurizio De Crescenzi

Beilstein J. Nanotechnol. 2015, 6, 1397–1398, doi:10.3762/bjnano.6.144

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  • construction. Research on self-assembled nanostructures encompasses fundamental issues in chemical synthesis, crystal growth and self-organization of 0D, 1D and 2D nanostructures, nanopatterning, lithographic techniques, nanocharacterization, scaling of materials properties down to molecular dimensions
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Editorial
Published 24 Jun 2015

Synthesis, characterization and in vitro effects of 7 nm alloyed silver–gold nanoparticles

  • Simon Ristig,
  • Svitlana Chernousova,
  • Wolfgang Meyer-Zaika and
  • Matthias Epple

Beilstein J. Nanotechnol. 2015, 6, 1212–1220, doi:10.3762/bjnano.6.124

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  • a versatile and facile wet chemical synthesis that allows size control and ligand exchange without affecting the resulting nanoparticle purity or stability. The in vitro studies were performed using HeLa cells and hMSCs. The cytotoxicity increased with increasing silver content in the nanoalloys
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Published 27 May 2015
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