Ultrathin water layers on mannosylated gold nanoparticles

• Maiara A. Iriarte Alonso,
• Jorge H. Melillo,
• Silvina Cerveny,
• Yujin Tong and
• Alexander M. Bittner

Beilstein J. Nanotechnol. 2025, 16, 2183–2198, doi:10.3762/bjnano.16.151

• vibrational bands are superimposed on a very broad signal from bulk gold, quasi-constant after normalization (like FTIR). In contrast to FTIR, the bands stem only from vibrations at interfaces, that is, from the NP surface in contact with air. Additionally, highly symmetric vibrations are forbidden (with very

• hydrophilic and hydrophobic surfaces We assessed with SEM and AFM the aggregation tendency of the particles after adsorption. To this end, we determined water contact angles. The hydrophilic APDMES silicon gave 66 ± 3º. In contrast, on the hydrophobic octadecyltrichlorosilane (OTS) silicon, it was 92 ± 2º

• dominant driver of particle motion, and strong particle–substrate interactions may lead to particle attachment before they are transported to the contact line, thereby preventing the formation of a “coffee ring” [34]. Detailed height measurements of adsorbed particles in water vapor AFM under variable RH

Calibration of piezo actuators and systems by dynamic interferometry

• Knarik Khachatryan and
• Michael Reichling

Beilstein J. Nanotechnol. 2025, 16, 2086–2091, doi:10.3762/bjnano.16.143

• Knarik Khachatryan Michael Reichling Institut für Physik, Universität Osnabrück, Barbarastr. 7, 49076 Osnabrück, Germany 10.3762/bjnano.16.143 Abstract To achieve precise measurements of small displacements in non-contact atomic force microscopy, it is crucial to control the position of moving

• oscillation amplitude calibration under conditions of various amounts of tube piezo contraction and extension. The merits and limits of accuracy for such type of calibration are discussed. Keywords: cantilever excitation; fiber interferometer; NC-AFM; piezo calibration; non-contact atomic force microscopy

• ; Introduction Interferometric displacement detection stands as a cornerstone in high-precision techniques employed in cantilever-based atomic force microscopy (AFM), since its early days [1][2][3][4][5][6]. This method of cantilever displacement detection is specifically well suited for non-contact atomic force

Multifrequency AFM integrating PeakForce tapping and higher eigenmodes for heterogeneous surface characterization

• Yanping Wei,
• Jiafeng Shen,
• Yirong Yao,
• Xuke Li,
• Ming Li and
• Peiling Ke

Beilstein J. Nanotechnol. 2025, 16, 2077–2085, doi:10.3762/bjnano.16.142

• factor (Q) cantilever dynamics amplify noise and demand meticulous parameter tuning [18]. To overcome these limitations, PeakForce tapping mode (PFT) was developed. It employs vertical probe oscillations at subresonant frequencies (0.5–8 kHz) to establish quasi-static tip–sample contact [18][19]. Unlike

• stiffness (k) matching, a critical requirement for accurate contact mechanics models [20]. The stiffness k should be neither too large (to ensure a sufficient deflection signal for accurate force measurement) nor too small (to achieve adequate sample indentation). For heterogeneous samples with modulus

• the measurement points can be calculated using the contact mechanics models [18][22]. (ii) Concurrently, the piezoelectric actuator PD-II excites the probe at its higher eigenmode, inducing a minor vibration with an amplitude generally beneath 1 nm. This high-eigenmode oscillation amplitude remains

Molecular and mechanical insights into gecko seta adhesion: multiscale simulations combining molecular dynamics and the finite element method

• Yash Jain,
• Saeed Norouzi,
• Tobias Materzok,
• Stanislav N. Gorb and
• Florian Müller-Plathe

Beilstein J. Nanotechnol. 2025, 16, 2055–2076, doi:10.3762/bjnano.16.141

• . The model reproduces key aspects of spatula behavior during adhesion and detachment, showing that spatula–substrate contact evolves through a combination of bending, sliding, and peeling, depending on the spatula’s initial orientation. Our results further demonstrate that lateral sliding can delay

• model multiple spatulae in parallel, all connected to a larger setal shaft. Forces and displacements are exchanged at each iteration, ensuring that spatula-level phenomena (e.g., van der Waals contact, slight sliding at the substrate, and spatula bending) feed back into the global deformation. The

• , and hydrophobic substrate at a loading rate of 1.88 × 1012 pN/s. We also examined adhesion forces and quantified spatula–substrate contacts, while comparing with qualitative and quantitative experimental results where available. We synchronously simulated 16 spatula–substrate contact sites via

Stereodiscrimination of guests in chiral organosilica aerogels studied by ESR spectroscopy

• Sebastian Polarz,
• Yasar Krysiak,
• Martin Wessig and
• Florian Kuhlmann

Beilstein J. Nanotechnol. 2025, 16, 2034–2054, doi:10.3762/bjnano.16.140

• of (+)- and (−)-3CP, and, as a result, the selectivity factor remains small (Figure 8c). One also sees that the fraction of the species interacting with the surfaces is small (<10%). Because ethanol predominantly interacts with 3CP, the contact of the spin probe with the chiral groups on the surface

Beyond the shell: exploring polymer–lipid interfaces in core–shell nanofibers to carry hyaluronic acid and β-caryophyllene

• Aline Tavares da Silva Barreto,
• Francisco Alexandrino-Júnior,
• Bráulio Soares Arcanjo,
• Paulo Henrique de Souza Picciani and
• Kattya Gyselle de Holanda e Silva

Beilstein J. Nanotechnol. 2025, 16, 2015–2033, doi:10.3762/bjnano.16.139

• surface distribution may compromise encapsulation efficiency and alter release kinetics [76]. Surface hydrophilicity The hydrophilicity of the membranes was evaluated through contact angle measurements. Figure 10 shows photographs of a water droplet in contact with the surface of the samples: (a

• ) monolithic PLA, (b) HA/PLA, and (c) HA+NE2/PLA. All samples exhibited a hydrophobic surface, with contact angles ranging between 90° and 150°, attributed to the PLA surface. This result corroborates other characterizations demonstrating that the shell effectively coats the hydrophilic core. As expected, the

• monolithic PLA nanofiber sample showed a contact angle of 117.1° ± 11.3°. For core–shell samples, contact angles of 126.9° ± 9.8° and 129.8° ± 1.3° were observed for the samples without NE (HA/PLA) and with NE (HA+NE2/PLA), respectively. The maintenance of surface hydrophobicity with the formation of the

Mechanical property measurements enabled by short-term Fourier-transform of atomic force microscopy thermal deflection analysis

• Thomas Mathias,
• Roland Bennewitz and
• Philip Egberts

Beilstein J. Nanotechnol. 2025, 16, 1952–1962, doi:10.3762/bjnano.16.136

• Contact resonance atomic force microscopy (CR-AFM) has been used in many studies to characterize variations in the elastic and viscoelastic constants of materials along a heterogeneous surface. In almost all experimental work, the quantitative modulus of the surface is calculated in reference to a known

• dynamic mechanics models relating the contact stiffness of the tip/cantilever pressing into a surface with the oscillation frequency of the cantilever and show that they did not accurately model the experiment. Several material combinations of tip and sample were examined; tip size and cantilever

• model, improved matching the cantilever/sample stiffness to obtain a larger variation in contact stiffness with frequency, or investigating the use of higher-order modes that may achieve this improved match. Keywords: atomic force microscopy; contact resonance; highly oriented pyrolytic graphite (HOPG

Quantum circuits with SINIS structures

• Mikhail Tarasov,
• Mikhail Fominskii,
• Aleksandra Gunbina,
• Artem Krasilnikov,
• Maria Mansfeld,
• Dmitrii Kukushkin,
• Andrei Maruhno,
• Valeria Ievleva,
• Mikhail Strelkov,
• Daniil Zhogov,
• Konstantin Arutyunov,
• Vyacheslav Vdovin,
• Vladislav Stolyarov and
• Valerian Edelman

Beilstein J. Nanotechnol. 2025, 16, 1931–1941, doi:10.3762/bjnano.16.134

• contact. When tunneling from a normal metal into a superconductor, due to the presence of an energy gap (Δ), only electrons whose energy exceeds Δ can tunnel into the superconductor. Without applying an external voltage or in the case when eV < Δ (T = 0), tunneling does not occur. Accordingly, a tunnel

Targeting the vector of arboviruses Aedes aegypti with nanoemulsions based on essential oils: a review with focus on larvicidal and repellent properties

• Laryssa Ferreira do Nascimento Silva,
• Douglas Dourado,
• Thayse Silva Medeiros,
• Mariana Alice Gonzaga Gabú,
• Maria Cecilia Queiroga dos Santos,
• Daiane Rodrigues dos Santos,
• Mylena Lemos dos Santos,
• Gabriel Bezerra Faierstein,
• Rosângela Maria Rodrigues Barbosa and
• Fabio Rocha Formiga

Beilstein J. Nanotechnol. 2025, 16, 1894–1913, doi:10.3762/bjnano.16.132

• as a mosquito, feeds on the blood of an infected host [1]. Thus, the virus undergoes a replication process in the midgut of the mosquito, being disseminated to different organs, mainly the salivary glands. Upon contact with a new host, the virus is inoculated through the bite of the vector

• female mosquitoes. These eggs are capable of surviving for a prolonged period in the absence of water and can withstand extreme environmental conditions, thereby persisting in aridand/or cold environments [20][48]. Upon contact with water, the eggs hatch, resulting in the hatching of larvae corresponding

• outbreaks in the Americas, being linked to severe complications such as congenital zika syndrome and Guillain–Barré syndrome [56]. In addition to mosquito transmission, ZIKV can spread through sexual contact [57], blood transfusions [58], and from mother to child [59]. Given the persistence and severity of

Low-temperature AFM with a microwave cavity optomechanical transducer

• Ermes Scarano,
• Elisabet K. Arvidsson,
• August K. Roos,
• Erik Holmgren,
• Riccardo Borgani,
• Mats O. Tholén and
• David B. Haviland

Beilstein J. Nanotechnol. 2025, 16, 1873–1882, doi:10.3762/bjnano.16.130

• stiffness values of the order of 100 N/m to avoid the tip jumping to contact and sticking to the surface [21]. Such a stiffness would necessitate seven orders of magnitude improvement in detector noise to achieve an equivalent force sensitivity. Reduction of detection noise is therefore critical for

Self-assembly and adhesive properties of Pollicipes pollicipes barnacle cement protein cp19k: influence of pH and ionic strength

• Shrutika Sawant,
• Anne Marie Power and
• J. Gerard Wall

Beilstein J. Nanotechnol. 2025, 16, 1863–1872, doi:10.3762/bjnano.16.129

• fibrillar aggregates formed under gland-like conditions, though structurally robust, may offer less surface contact, resulting in the granular Coomassie staining. The curled fibres formed in low pH and low salt concentration conditions were also tested for surface adhesion, resulting in no homogenous or

Current status of using adsorbent nanomaterials for removing microplastics from water supply systems: a mini review

• Nguyen Thi Nhan and
• Tran Le Luu

Beilstein J. Nanotechnol. 2025, 16, 1837–1850, doi:10.3762/bjnano.16.127

• and lakes) often contain higher levels of MPs because of direct contact with the environment, with concentrations ranging from 1473 to 3605 particles·L−1. After undergoing various treatment stages, these values decrease significantly, and MPs are still detected in treated water, with concentrations

Electrical, photocatalytic, and sensory properties of graphene oxide and polyimide implanted with low- and medium-energy silver ions

• Josef Novák,
• Eva Štěpanovská,
• Petr Malinský,
• Vlastimil Mazánek,
• Jan Luxa,
• Ulrich Kentsch and
• Zdeněk Sofer

Beilstein J. Nanotechnol. 2025, 16, 1794–1811, doi:10.3762/bjnano.16.123

• Keithley 6317B electrometer. To quantify the sheet resistivity, two gold contacts, each with a thickness of 50 nm and a length of 10 mm, were deposited onto the surfaces of GO and PI thin films. The placement of these contacts adhered to a prescribed contact distance of 1 mm, ensuring a consistent and

Exploring the potential of polymers: advancements in oral nanocarrier technology

• Rousilândia de Araujo Silva,
• Igor Eduardo Silva Arruda,
• Luise Lopes Chaves,
• Mônica Felts de La Roca Soares and
• Jose Lamartine Soares Sobrinho

Beilstein J. Nanotechnol. 2025, 16, 1751–1793, doi:10.3762/bjnano.16.122

• , drug release from the polymer matrix can proceed through various mechanisms after in vivo administration. In this context, water is absorbed by the polymer, leading to pore formation, which results in the creation of degradation products that dissolve in the release medium. Increased contact with water

Ambient pressure XPS at MAX IV

• Mattia Scardamaglia,
• Ulrike Küst,
• Alexander Klyushin,
• Rosemary Jones,
• Jan Knudsen,
• Robert Temperton,
• Andrey Shavorskiy and
• Esko Kokkonen

Beilstein J. Nanotechnol. 2025, 16, 1677–1694, doi:10.3762/bjnano.16.118

• meniscus must be thin enough to allow photoelectrons to escape, yet thick enough to maintain electrical contact. The meniscus thickness depends on factors such as the wetting properties of the WE, liquid viscosity, surface tension, and pulling speed. This geometry enables true operando studies of solid

Prospects of nanotechnology and natural products for cancer and immunotherapy

• Jan Filipe Andrade Santos,
• Marcela Bernardes Brasileiro,
• Pamela Danielle Cavalcante Barreto,
• Ligiane Aranha Rocha and
• José Adão Carvalho Nascimento Júnior

Beilstein J. Nanotechnol. 2025, 16, 1644–1667, doi:10.3762/bjnano.16.116

• by Li et al. discussed patent CN115671277 [94]. Nanoparticles Nanoparticles are materials with at least one dimension ranging from 1 to 999 nm [95]. This technology possesses a high contact surface, a high concentration of surface-active centers, and low toxicity due to promoting a reduction in the

• glycolysis, reducing angiogenesis, and promoting the degradation of oncogenic proteins [162][163]. The invention proposes the use of carbon dots (CDs) loaded with BER as an API, with a sustained drug release that increases upon contact with the acidic conditions surrounding tumors. Both non-loaded CDs and

Venom-loaded cationic-functionalized poly(lactic acid) nanoparticles for serum production against Tityus serrulatus scorpion

• Philippe de Castro Mesquita,
• Karla Samara Rocha Soares,
• Manoela Torres-Rêgo,
• Emanuell dos Santos-Silva,
• Mariana Farias Alves-Silva,
• Alianda Maira Cornélio,
• Matheus de Freitas Fernandes-Pedrosa and
• Arnóbio Antônio da Silva-Júnior

Beilstein J. Nanotechnol. 2025, 16, 1633–1643, doi:10.3762/bjnano.16.115

• desiccator for 24 h. The images were obtained with a silicon tip, operating in the attractive region of a cantilever in non-contact mode. For the FEGSEM analyzes, a drop of dispersion was placed in a microscope slide with carbon tapes and dried under a desiccator for 24 h [46]. Protein-loading efficiency The

Nanotechnology-based approaches for the removal of microplastics from wastewater: a comprehensive review

• Nayanathara O Sanjeev,
• Manjunath Singanodi Vallabha and
• Rebekah Rubidha Lisha Rabi

Beilstein J. Nanotechnol. 2025, 16, 1607–1632, doi:10.3762/bjnano.16.114

• contact angle decreasing from 84.6° ± 1° to 64.2° ± 1.2°), work of adhesion, wetting energy, porosity, and pore dimensions. Among various loadings, the membrane with 0.5 wt % MIL-100 (Fe) (M0.5) showed the best overall performance. It delivered a pure water flux over ten times higher than M0 and achieved

Bioinspired polypropylene-based functionally graded materials and metamaterials modeling the mistletoe–host interface

• Lina M. Rojas González,
• Naeim Ghavidelnia,
• Christoph Eberl and
• Max D. Mylo

Beilstein J. Nanotechnol. 2025, 16, 1592–1606, doi:10.3762/bjnano.16.113

• tissues of the two species. Moreover, a decrease in cell wall thickness from the interface to the inner parts of the mistletoe was found [30]. The material and geometric structuring of the interface increase the contact area and enable a smooth transition between the different mechanical properties of the

• between PP and PPFG. The subsections were assumed to be bonded to one another through contact conditions. The bottom sides of the structure were considered as fixed (clamped) supports without any displacement and rotation, and the loading was applied as a ramped displacement from 0 to 5 mm at the top edge

Photocatalytic degradation of ofloxacin in water assisted by TiO₂ nanowires on carbon cloth: contributions of H₂O₂ addition and substrate absorbability

• Iram Hussain,
• Lisha Zhang,
• Zhizhen Ye and
• Jin-Ming Wu

Beilstein J. Nanotechnol. 2025, 16, 1567–1579, doi:10.3762/bjnano.16.111

• of as-precipitated nanowires in air at a heating rate of 10 K·min−1 from room temperature to 500 °C. The static water contact angles were measured using a goniometer (OCA 11, DataPhysics Instruments GmbH, Filderstadt, Germany) following the standard sessile drop method. The measurements were

• capability The contact angle measurements in Supporting Information File 1, Figure S9 reveal distinct differences in surface wettability among the samples. The pristine carbon cloth shows a high contact angle of approximately 138.9°, indicating strong hydrophobicity (Supporting Information File 1, Figure S9b

• ). Remarkably, the CC/NW-450 °C composite exhibits a contact angle of 0° (Supporting Information File 1, Figure S9c), showing complete wettability. This significant enhancement in hydrophilicity is attributed to the high surface roughness and porous hydrophilic nanowire architecture formed on the carbon cloth

Modeling magnetic properties of cobalt nanofilms used as a component of spin hybrid superconductor–ferromagnetic structures

• Aleksey Fedotov,
• Olesya Severyukhina,
• Anastasia Salomatina and
• Anatolie Sidorenko

Beilstein J. Nanotechnol. 2025, 16, 1557–1566, doi:10.3762/bjnano.16.110

• contact from a multilayer nanostructure” (methodology for modeling magnetic properties) and with the financial support of the Russian Science Foundation (project No. 23-72-30004) (research at ultra-low temperatures) and the project No. 020201 of the Moldova State Program “Nanostructures and advanced

Dendrimer-modified carbon nanotubes for the removal and recovery of heavy metal ions from water

• Thao Quynh Ngan Tran,
• Huu Trung Nguyen,
• Subodh Kumar and
• Xuan Thang Cao

Beilstein J. Nanotechnol. 2025, 16, 1522–1532, doi:10.3762/bjnano.16.107

• adsorbents for both Pb2+ and Cd2+ ions. The impact of contact time on the Pb2+ and Cd2+ ion adsorption efficiency was also investigated (Figure 3d). Each adsorbent showed increased adsorption efficiency for both the metal ions in the case of longer contact time ranging from 0 to 240 min. This behavior

• suggests that longer time is favorable for metal ions to be adsorbed onto the surface of dendrimerized CNTs. However, the adsorption efficiency reached a plateau after 120 min, implying an equilibrium between adsorption and desorption processes. Accordingly, 120 min was chosen as the optimal contact time

• of CNTs, CNTs-MA, CNTs-G0, CNTs-G1, CNTs-G2, CNTs-G3, and CNTs-G5; and (d) TGA curves of CNTs, CNTs-G0, CNTs-G1, CNTs-G2, CNTs-G3, and CNTs-G5. SEM images of (a) CNTs, (b) CNTs-G1, (c) CNTs-G3, and (d) CNTs-G5. Effect of (a, b) adsorbents dosage, (c) solution pH, and (d) contact time on the removal

Laser processing in liquids: insights into nanocolloid generation and thin film integration for energy, photonic, and sensing applications

• Akshana Parameswaran Sreekala,
• Pooja Raveendran Nair,
• Jithin Kundalam Kadavath,
• Bindu Krishnan,
• David Avellaneda Avellaneda,
• M. R. Anantharaman and
• Sadasivan Shaji

Beilstein J. Nanotechnol. 2025, 16, 1428–1498, doi:10.3762/bjnano.16.104

Parylene-coated platinum nanowire electrodes for biomolecular sensing applications

• Chao Liu,
• Peker Milas,
• Michael G. Spencer and
• Birol Ozturk

Beilstein J. Nanotechnol. 2025, 16, 1392–1400, doi:10.3762/bjnano.16.101

• was gradually increased to 20–75 µm to prevent contact between the growing nanowire and the counter electrode, which leads to a short circuit and damages the nanowire. Parylene-C coating The parylene-C coating system was a modified version of the setup from Gluschke and colleagues [33]. As shown in

Synthesis and antibacterial properties of nanosilver-modified cellulose triacetate membranes for seawater desalination

• Lei Wang,
• Shizhe Li,
• Kexin Xu,
• Wenjun Li,
• Ying Li and
• Gang Liu

Beilstein J. Nanotechnol. 2025, 16, 1380–1391, doi:10.3762/bjnano.16.100

• , Bacillus thuringiensis, Lysinibacillus xylanilyticus, Lysinibacillus lparviboronicapiens and Burkholderia ambifaria after 24 h of contact of the membrane with the above bacteria. The modified membrane of Ag@PCTA demonstrates significant disinfection and sterilization effects on all tested strains