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Search for "electron microscopy" in Full Text gives 1249 result(s) in Beilstein Journal of Nanotechnology. Showing first 200.

Glycerol photoelectrochemical oxidation reaction at carbon nitrides/BiVO4 materials

  • Charles Garcia da Cunha,
  • Isabelle M. D. Gonzaga,
  • Cristian Hessel,
  • Izadora F. Reis,
  • Ivo F. Teixeira,
  • Lucia H. Mascaro and
  • Elton Sitta

Beilstein J. Nanotechnol. 2026, 17, 806–817, doi:10.3762/bjnano.17.57

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  • acetylacetonate at 500 °C for 2 h. The CN/BiVO4 heterojunctions presented bandgap energy values, Eg, similar to pure BiVO4. X-ray diffraction analysis also revealed that the BiVO4 phase was not altered by the presence of the CN. However, scanning electron microscopy analysis coupled to energy-dispersive X-ray
  • acquired from 10° to 80° at a rate of 2°·min−1 with a step size of 0.02°. Morphological features and elemental composition were determined by field-emission scanning electron microscopy (FEG-SEM; Zeiss Supra35) coupled with energy-dispersive X-ray spectroscopy (EDS), operating at 15 kV. Optical properties
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Published 17 Jun 2026

Restorative potential of laser-synthesized silver nanoparticles with Salvia officinalis for periodontal disease treatment: an in vitro study

  • Jelena Filipović Tričković,
  • Sanja Živković,
  • Bojana Ilić,
  • Miloš Tošić,
  • Jelena Marinković,
  • Ana Valenta Šobot and
  • Miloš Momčilović

Beilstein J. Nanotechnol. 2026, 17, 781–795, doi:10.3762/bjnano.17.55

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  • . AgNPs were synthesized at two laser pulse energies (2 and 6 mJ), in sage extract and deionized water, and characterized by dynamic light scattering, transmission electron microscopy, and inductively coupled plasma optical emission spectroscopy. Synthesis at 6 mJ in sage extract (SageAgNPs6mJ) yielded
  • polystyrene cuvettes (DTS0012, Malvern Panalytical, UK) at ambient temperature (25 ± 0.1 °C). The selected AgNPs that displayed antimicrobial effects were further analyzed by transmission electron microscopy (TEM), to evaluate their size, shape, and dispersity. An FEI Talos F200X microscope, operating at 200
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Published 15 Jun 2026

Substrate-dependent pore formation in molybdenum disulfide monolayers under ion irradiation

  • Yossarian Liebsch,
  • Umair Javed,
  • Lucia Skopinski,
  • Leon Daniel,
  • Franziska Appel,
  • Radia Rahali,
  • Clara Grygiel,
  • Henning Lebius,
  • Carolin Frank,
  • Lars Breuer,
  • Leon Kirsch,
  • Frieder Koch,
  • Jani Kotakoski and
  • Marika Schleberger

Beilstein J. Nanotechnol. 2026, 17, 769–780, doi:10.3762/bjnano.17.54

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  • highly charged ions (HCIs) and swift heavy ions (SHIs) – two types of ions that, despite having vastly different kinetic energies, both interact primarily with the electronic system of the target. Using scanning transmission electron microscopy, we quantify pore radii and pore formation efficiencies for
  • under both HCI and SHI irradiation conclusively demonstrate the central role of substrate and interface-dependent electronic dissipation pathways regarding damage under these types of ion irradiation. Keywords: defects; MoS2; nanopores; SiO2; scanning transmission electron microscopy (STEM
  • , high-resolution scanning transmission electron microscopy (STEM) generally requires freestanding membranes, while atomic-resolution atomic force microscopy (AFM) and scanning tunneling microscopy (STM) demand exceptionally clean surfaces; also, substrate effects can further complicate interpretation
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Published 12 Jun 2026

Tailoring Ag–Pt nanoalloys through solid-state dewetting: structural and optical insights

  • Marcin Łapiński,
  • Piotr Okoczuk,
  • Blaž Grobiša,
  • Ewa Pawlikowska,
  • Amelia Rozwadowska,
  • Wojciech Sadowski and
  • Barbara Kościelska

Beilstein J. Nanotechnol. 2026, 17, 748–759, doi:10.3762/bjnano.17.52

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  • under an argon atmosphere. The process induced the transformation of continuous bilayers into isolated nanoislands through solid-state dewetting. Scanning electron microscopy and transmission electron microscopy analyses revealed the formation of well-defined, nearly spherical nanoislands with a
  • a region with a lower film thickness at grain boundaries, which is well visible on the linear AFM profile in Figure 1 [45][46][47]. Figure 2a presents an exemplary scanning electron microscopy (SEM) image of nanostructures formed as a result of annealing of a silver–platinum bilayer with a thickness
  • homogeneous Ag–Pt nanoalloys, high-resolution transmission electron microscopy (HR-TEM) observations were performed. Representative cross-section TEM images of two samples with various compositions are shown in Figure 8. Images for both nanostructures exhibit uniform morphology, which strongly indicates alloy
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Published 10 Jun 2026

Oxidative atmosphere-driven formation of single-phase spinel CuRh2O4 nanofibers for alkaline water oxidation

  • Namhee Kim,
  • Sumin Ko,
  • Sohyeon Choi,
  • Seoyoon Jang,
  • Myung Hwa Kim and
  • Dasol Jin

Beilstein J. Nanotechnol. 2026, 17, 737–743, doi:10.3762/bjnano.17.50

Graphical Abstract
  • 609.6 cm−1 (A1g), which are consistent with the spinel CuRh2O4 lattice [17][18], supporting the XRD-based phase assignment (vide supra). As shown in Figure 4b, high-resolution transmission electron microscopy (HRTEM) analysis of the electrospun CuRh2O4 nanofibers reveals clear lattice fringes with an
  • electron microscopy (SEM) was employed to investigate the surface morphology and structural uniformity of the electrospun nanofibers after post-annealing. In the as-spun state prior to annealing, the fibers containing PVP exhibit smooth surfaces with an average diameter of approximately 300 nm (Supporting
  • characterization Morphology and elemental composition of the synthesized nanomaterials were examined using field-emission scanning electron microscopy (FE-SEM; JEOL JSM-6700F) and high-resolution transmission electron microscopy (HRTEM; JEOL JEM-2100F). Surface chemical states and crystallographic structures were
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Published 27 May 2026

Environmental applications of silver nanoparticles: state-of-the-art review and emerging trends

  • Soni Prajapati,
  • Akash Kumar and
  • Ranjana Singh

Beilstein J. Nanotechnol. 2026, 17, 697–736, doi:10.3762/bjnano.17.49

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  • needed before engineering AgNPs for particular applications. AgNPs are characterised using optical spectroscopy, electron microscopy, X-ray diffraction, and dynamic light scattering (DLS) to measure plasmonic absorbance, size, shape, structure, and stability [49]. Optical spectroscopy is a rapid and
  • , which calculated the AgNP concentration as particles per millilitre [53]. Microscopic techniques, such as transmission electron microscopy, provide high-resolution images of individual nanoparticles, confirming morphology, size distribution, and elemental composition when coupled with energy-dispersive
  • X-ray analysis [49]. TEM analysis is performed on copper grids with varying mesh sizes and coatings, with carbon/formvar-coated copper grids commonly preferred. Scanning electron microscopy (SEM) provides information on the silver nanoparticles’ surface properties and the aggregation state of dried
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Published 26 May 2026

Molecular engineering of individual dye-based nanoparticle photostability for ultrabright two-photon fluorescence

  • Eleonore Kurek,
  • Sasha Cooper,
  • Alexandre Clausolles,
  • Karen Perronet,
  • Jonathan Daniel,
  • Mireille Blanchard-Desce and
  • François Marquier

Beilstein J. Nanotechnol. 2026, 17, 688–696, doi:10.3762/bjnano.17.48

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  • ) Transmission electron microscopy (TEM) and size distribution of dFONs(1), data reused from [20]. (d) TEM and size distribution of dFONs(2). (e) Normalized absorption spectra of dFONs(1) (green) and dFONs(2) (red). (f) Normalized emission spectra of dFONs(1) (green) and dFONs(2) (red). (g) Two-photon absorption
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Published 22 May 2026

Decontamination from water pollutants and pathogens by electrospun nanofibers doped with heavy-atom-free borafluorene-BODIPY photosensitizers

  • Angelika Zaszczyńska,
  • Paulina H. Marek-Urban,
  • Karolina Wrochna,
  • Agnieszka E. Kuklewska,
  • Kacper Kręgielewski,
  • Marta Grodzik,
  • Dawid R. Natkowski,
  • Jolanta Mierzejewska,
  • Ewa Iwanek,
  • Agata Blacha-Grzechnik,
  • Paweł Sajkiewicz and
  • Krzysztof Durka

Beilstein J. Nanotechnol. 2026, 17, 668–682, doi:10.3762/bjnano.17.46

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  • 30 µm, Rotilabo®, Roth Selection, Germany), which was attached to the collector. After the electrospinning process, all mats were placed under a fume hood for 48 h to evaporate solvents in the fibers. Morphology analysis The morphological properties of samples were examined through scanning electron
  • microscopy (SEM) using a JSM-6010PLUS/LV InTouchScope™ system from JEOL (Tokyo, Japan), operating at an accelerating voltage of 11 kV. Prior to imaging, each nonwoven sample underwent a double-coating process with a thin gold layer (2–3 nm). Microstructural analysis was subsequently performed utilizing
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Published 20 May 2026

afspm: A framework for manufacturer-agnostic automation in scanning probe microscopy

  • Nicholas J. Sullivan,
  • Julio J. Valdés,
  • Kirk H. Bevan and
  • Peter Grutter

Beilstein J. Nanotechnol. 2026, 17, 653–667, doi:10.3762/bjnano.17.45

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  • instruments’ communication interfaces, and may benefit from similar frameworks. We particularly highlight optical and electron microscopy as these instruments share common experimental workflows (e.g., searching a wider region to determine where to image) and may benefit from direct repurposing of automation
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Published 18 May 2026

Two-step laser synthesis of Ag@TiO2 nanomaterials for the photocatalytic degradation of rhodamine B

  • Marija Kovačević,
  • Miloš Tošić,
  • Rafaela Radičić,
  • Vladimir Rajić,
  • Nikša Krstulović,
  • Miloš Momčilović and
  • Sanja Živković

Beilstein J. Nanotechnol. 2026, 17, 622–634, doi:10.3762/bjnano.17.43

Graphical Abstract
  • characterization was performed using scanning electron microscopy (SEM) and transmission electron microscopy (TEM) with energy-dispersive spectroscopy (EDS), aiming to establish a clear correlation between synthesis parameters, nanostructure features, and photocatalytic activity. In our previous studies [6][7][21
  • microstructural examination utilizing transmission electron microscopy. Investigations were conducted using scanning transmission electron microscopy, high-angle annular dark-field with energy-dispersive spectroscopy, and conventional and high-resolution transmission electron microscopy. A drop of the suspended
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Published 11 May 2026

Recent progress in enhancing built-in electric fields of perovskite solar cells via junction engineering

  • Tong Xiao and
  • Ke Xu

Beilstein J. Nanotechnol. 2026, 17, 602–621, doi:10.3762/bjnano.17.42

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Published 07 May 2026

Upcycling agroindustrial waste into graphene oxide supports for gold nanoparticles: toward sustainable nanomaterials

  • Juan Marcos Castro-Tapia,
  • Selene Acosta,
  • Hiram Joazet Ojeda-Galván,
  • Elsie Evelyn Araujo-Palomo,
  • Edgar Giovanni Villabona-Leal and
  • Mildred Quintana

Beilstein J. Nanotechnol. 2026, 17, 489–504, doi:10.3762/bjnano.17.32

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  • = 1486.6 eV). The pass energy was set to 10 eV for high-resolution scans and to 40 eV for survey spectra. All binding energies were referenced to the C=C peak at 284.4 eV. Transmission electron microscopy (TEM) was carried using a JEOL JEM-2100 microscope operating at an accelerating voltage of 200 kV. TEM
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Published 01 Apr 2026

Defects and defect-mediated engineering of two-dimensional materials: challenges and open questions

  • Arkady V. Krasheninnikov,
  • Matthias Batzill,
  • Anouar-Akacha Delenda,
  • Marija Drndić,
  • Chris Ewels,
  • Katharina J. Franke,
  • Mahdi Ghorbani-Asl,
  • Alexander Holleitner,
  • Ado Jorio,
  • Ute Kaiser,
  • Daria Kieczka,
  • Hannu-Pekka Komsa,
  • Jani Kotakoski,
  • Manuel Längle,
  • David Lamprecht,
  • Yun Liu,
  • Steven G. Louie,
  • Janina Maultzsch,
  • Thomas Michely,
  • Katherine Milton,
  • Anna Niggas,
  • Hanako Okuno,
  • Joshua A. Robinson,
  • Marika Schleberger,
  • Bruno Schuler,
  • Alexander Shluger,
  • Kazu Suenaga,
  • Kristian S. Thygesen,
  • Richard A. Wilhelm,
  • E. Harriet Åhlgren and
  • Carla Bittencourt

Beilstein J. Nanotechnol. 2026, 17, 454–488, doi:10.3762/bjnano.17.31

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  • created by impacts of energetic particles [18][19][20][21] by foreign atoms. Lots of insights into the structure and properties of defective 2D materials have been obtained using transmission electron microscopy (TEM), including conventional TEM and scanning TEM (STEM). These techniques, along with
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Published 31 Mar 2026

Eco-efficient materials for agricultural crops based on a mineral rich in MOR- and HEU-type zeolites

  • Esperanza Yamile de la Nuez-Pantoja,
  • Inocente Rodríguez-Iznaga,
  • Gerardo Rodríguez-Fuentes,
  • Vitalii Petranovskii,
  • Ariel Martínez García,
  • José Juan Calvino Gámez and
  • Daniel Goma Jiménez

Beilstein J. Nanotechnol. 2026, 17, 381–395, doi:10.3762/bjnano.17.26

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  • urea arranged on the surface so that it covers the material and interacts with the zeolitic frameworks, was evidenced by Fourier-transform IR spectroscopy, adsorption measurements, scanning electron microscopy, scanning transmission electron microscopy, and other methods, as well as through culture
  • microscopy (SEM), scanning transmission electron microscopy (STEM), N2 physisorption, and other research methods. Results and Discussion Characterization of DAP-modified zeolite CLIM The chemical compositions of natural zeolite (CLIM) from the San Andrés deposit and its modified forms (CLIMf) with ammonium
  • consequence of the ion exchange processes (Equation 1) occurring during treatment of CLIM with DAP solution, which is in agreement with the data reported in [16][21][42]. Scanning electron microscopy and scanning transmission electron microscopy Microphotography (Figure 5) of natural zeolite (CLIM) revealed
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Published 26 Feb 2026

Interconnection morphology effects on the radio frequency response of carbon nanotube sponges

  • Manuela Scarselli,
  • Javad Rezvani,
  • Zeno Zuccari,
  • Mattia Scagliotti and
  • Simone Tocci

Beilstein J. Nanotechnol. 2026, 17, 343–351, doi:10.3762/bjnano.17.23

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  • . In particular, we observed that the response of S11 = −22.6 dB around 4.8 GHz from the CNS antenna improved after a mild treatment with ethanol, reaching S11 = −32.6 dB measured after 10 min of waiting. This observed effect is studied in detail with scanning electron microscopy and Raman spectroscopy
  • findings point to a different interpretation related to the morphological effect of ethanol on the CNT mesh [27][29]. A scanning electron microscopy (SEM) study provided insights into the microstructure of the CNT film (Supporting Information File 1, Figure S1) and the sponges (Figure 3). The study
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Published 17 Feb 2026

Beam shaping techniques for pulsed laser ablation in liquids: Unlocking tunable control of nanoparticle synthesis in liquids

  • Sergio Molina-Prados,
  • Nadezhda M. Bulgakova,
  • Alexander V. Bulgakov,
  • Jesus Lancis,
  • Gladys Mínguez Vega and
  • Carlos Doñate-Buendia

Beilstein J. Nanotechnol. 2026, 17, 309–342, doi:10.3762/bjnano.17.22

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Published 16 Feb 2026

Durable antimicrobial activity of fabrics functionalized with zeolite ion-exchanged nanomaterials against Staphylococcus aureus and Escherichia coli

  • Perla Sánchez-López,
  • Kendra Ramirez Acosta,
  • Sergio Fuentes Moyado,
  • Ruben Dario Cadena-Nava and
  • Elena Smolentseva

Beilstein J. Nanotechnol. 2026, 17, 262–274, doi:10.3762/bjnano.17.18

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  • atom % are evaluated regarding their antimicrobial activity against Staphylococcus aureus (Gram-positive) and Escherichia coli (Gram-negative), as well as regarding their physicochemical and mechanical properties. Scanning electron microscopy confirms the uniform distribution and successful
  • ). Scanning electron microscopy confirmed the effective incorporation and uniform distribution of the nanomaterials on the fabric surface, facilitated by a 10% w/w acrylic resin binder. Among the tested materials, silver-based fabrics displayed the highest antibacterial efficacy, followed by copper and zinc
  • , transmission electron microscopy (TEM) images were obtained using a JEOL JEM-2200FS (200 kV), and elemental analysis was performed using EDS. The crystalline structure of the modified fabrics was determined by X-ray diffraction (XRD) in a Panalytical AERIS diffractometer using Cu Kα (λ = 1.54184 Å). The
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Published 06 Feb 2026

Multilayered hyperbolic Au/TiO2 nanostructures for enhancing the nonlinear response around the epsilon-near-zero point

  • Fernando Arturo Araiza-Sixtos,
  • Mauricio Gomez-Robles,
  • Rafael Salas-Montiel and
  • Raúl Rangel-Rojo

Beilstein J. Nanotechnol. 2026, 17, 251–261, doi:10.3762/bjnano.17.17

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  • actually was not at 800 nm, but rather at 600 nm. We tried to find the reason of this shift with our available resources. Transmission electron microscopy showed that there was no significant change in the geometry, which could have resulted in the ENZ shift. We could not study the composition of the
  • oscillator as a starting material for Au, and with TiO2 with Cody–Lorentz oscillators as starting material for TiO2. Scanning electron microscopy (Hitachi SU8030) was used to obtain the cross-sectional image (below in Figure 4a), with the sample oriented to expose the ENZ material edge to the electron beam
  • the deposited layers. In Table 1, we can see that we have widths for every stack that are different from the ones proposed for the simulated ENZ points. This change in thickness was also seen in scanning electron microscopy (SEM). In Figure 4a we present a SEM image of the ML800 structure; we see that
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Published 05 Feb 2026

Comparative study on 3D morphologies of delignified, single tracheids and fibers of five wood species

  • Helen Gorges,
  • Felicitas von Usslar,
  • Cordt Zollfrank,
  • Silja Flenner,
  • Imke Greving,
  • Martin Müller,
  • Clemens F. Schaber,
  • Chuchu Li and
  • Stanislav N. Gorb

Beilstein J. Nanotechnol. 2026, 17, 239–250, doi:10.3762/bjnano.17.16

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  • . Scanning electron microscopy was used to compare the morphology between untreated and delignified fibers and tracheids. X-ray tomography enabled us to reconstruct high-resolution 3D models of delignified single tracheids or fibers, providing information on the pit arrangements. Moreover, delignification
  • largely absent from scientific literature. Although previous studies have examined wood anatomy using various imaging techniques, such as X-ray micro-computed tomography in addition to scanning and transmission electron microscopy [22][23][24][25][26][27], high-resolution 3D reconstructions of single
  • species in this study by observation of the structural differences after delignification. Using X-ray tomography, we were able to build 3D models of single fibers and tracheids. Additionally, we imaged untreated and delignified samples using scanning electron microscopy for measuring fiber and tracheid
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Published 04 Feb 2026

Gold nanoparticle-decorated reduced graphene oxide as a highly effective catalyst for the selective α,β-dehydrogenation of N-alkyl-4-piperidones

  • Brenda Flore Kenyim,
  • Mihir Tzalis,
  • Marilyn Kaul,
  • Robert Oestreich,
  • Aysenur Limon,
  • Chancellin Pecheu Nkepdep and
  • Christoph Janiak

Beilstein J. Nanotechnol. 2026, 17, 218–238, doi:10.3762/bjnano.17.15

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  • , scanning electron microscopy (SEM) and nitrogen gas sorption surface area analysis using the Brunauer–Emmett–Teller (BET) theory were employed to evaluate the surface structure, porosity, and overall texture of the materials. The SEM image in Figure 2a reveals the typical structure of AC, characterized by
  • scattering (DLS) measurements was 12 nm (Figure 4b). Transmission electron microscopy (TEM) analysis showed spherical and well-dispersed nanoparticles and their particle size distribution (Figure 4c), based on the measurements of approximately 200 nanoparticles, yielded an average diameter of 12 nm with a
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Published 30 Jan 2026

Time of flight secondary ion mass spectrometry imaging of contaminant species in chemical vapour deposited graphene on copper

  • Barry Brennan,
  • Vlad-Petru Veigang-Radulescu,
  • Philipp Braeuninger-Weimer,
  • Stephan Hofmann and
  • Andrew J. Pollard

Beilstein J. Nanotechnol. 2026, 17, 200–213, doi:10.3762/bjnano.17.13

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  • a Wyko NT1100 White Light Optical Profiling System using a 20× magnification in vertical scanning interferometry (VSI) mode. Scanning electron microscopy (SEM) was carried out with a Carl Zeiss SIGMA VP at an acceleration voltage of 2 kV to ensure sample consistency. Four separate Cu foil samples
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Published 21 Jan 2026

Functional surface engineering for cultural heritage protection: the role of superhydrophobic and superoleophobic coatings – a comprehensive review

  • Giuseppe Cesare Lama,
  • Marino Lavorgna,
  • Letizia Verdolotti,
  • Federica Recupido,
  • Giovanna Giuliana Buonocore and
  • Bharat Bhushan

Beilstein J. Nanotechnol. 2026, 17, 63–96, doi:10.3762/bjnano.17.6

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Published 07 Jan 2026

Subdigital integumentary microstructure in Cyrtodactylus (Squamata: Gekkota): do those lineages with incipiently expressed toepads exclusively exhibit adhesive setae?

  • Philipp Ginal,
  • Yannick Ecker,
  • Timothy Higham,
  • L. Lee Grismer,
  • Benjamin Wipfler,
  • Dennis Rödder,
  • Anthony Russell and
  • Jendrian Riedel

Beilstein J. Nanotechnol. 2026, 17, 38–56, doi:10.3762/bjnano.17.4

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  • variation of digital form within this genus, from species with ancestrally small, round subdigital scales to macroscopically defined incipient toepads (broadened lamella-like subdigital scales). We employed scanning electron microscopy (SEM) and phylogenetic comparative methods to (a) explore the
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Published 06 Jan 2026

Reduced graphene oxide paper electrode for lithium-ion cells – towards optimized thermal reduction

  • Agata Pawłowska,
  • Magdalena Baran,
  • Stefan Marynowicz,
  • Aleksandra Izabela Banasiak,
  • Adrian Racki,
  • Adrian Chlanda,
  • Tymoteusz Ciuk,
  • Marta Wolczko and
  • Andrzej Budziak

Beilstein J. Nanotechnol. 2026, 17, 24–37, doi:10.3762/bjnano.17.3

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  • and thickness were determined with scanning electron microscopy imaging. This paper also reveals electrical and electrochemical properties of the material. The conductivity of the material obtained at 800 °C reached ≈70 S/cm, and the discharge capacity reached ≈160 mAh/g at 100 mA/g current density
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Published 05 Jan 2026

Improving magnetic properties of Mn- and Zn-doped core–shell iron oxide nanoparticles by tuning their size

  • Dounia Louaguef,
  • Ghouti Medjahdi,
  • Sébastien Diliberto,
  • Klaus M. Seemann,
  • Thomas Gries,
  • Joelle Bizeau,
  • Damien Mertz,
  • Eric Gaffet and
  • Halima Alem

Beilstein J. Nanotechnol. 2025, 16, 2285–2295, doi:10.3762/bjnano.16.157

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  • least tenfold). The designed core NPs are composed of a Zn0.4Fe2.6O4 core and a MnFe2O4 shell. Their size and morphology were determined by transmission electron microscopy, Fourier-transform infrared spectroscopy was used to investigate their chemical composition. The iron oxide phase was confirmed by
  • evaluation of the Mössbauer spectra was performed by least-square fitting of lines using the Winnormos (Wissel) program. The error on all Fe Mössbauer spectra was ±0.1 mm·s−1. High-resolution transmission electron microscopy (HRTEM) and scanning transmission electron microscopy (STEM) images were performed
  • focused on precise control of shape and size, critical factors for tuning magnetic behavior. By employing thermal decomposition, Zn0.4Fe2.6O4 NPs were synthesized with a well-defined polyhedral morphology, as confirmed by high-resolution transmission electron microscopy (HRTEM) (Figure 1). This morphology
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Published 15 Dec 2025
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