Sustainable fabrication of 2D-based devices through reuse of substrates with microfabricated electrodes

• Ying Zhang,
• Yigit Sozen,
• Esteban Zamora-Amo,
• Thomas Pucher,
• Nuria Jiménez-Arévalo,
• Zdenek Sofer,
• Yong Xie and
• Andres Castellanos-Gomez

Beilstein J. Nanotechnol. 2026, 17, 818–827, doi:10.3762/bjnano.17.58

• ), enabling the removal of 2D materials without damaging the electrodes. Electrical measurements, Raman analysis, and Kelvin probe force microscopy measurements collectively confirm the feasibility of repeatedly reusing the same pre-patterned chip, showing that the cleaned regions exhibit no detectable Raman

• adhesive residues were removed from the patterned region, leaving a pristine SiO2/Si surface (Figure 1d). The insets in Figure 1c and Figure 1d provide high-magnification optical microscopy images. Before cleaning, the interconnected network of MoS2 flakes is visible, whereas after treatment, the surface

• surface in three states, namely, pristine electrode, electrode after roll-to-roll mechanically exfoliated MoS2 transfer, and electrode after NMP cleaning. Figure 4a–c shows optical microscopy images of the corresponding regions, with the dashed outlines indicating the areas selected for Raman mapping. For

Glycerol photoelectrochemical oxidation reaction at carbon nitrides/BiVO₄ materials

• Charles Garcia da Cunha,
• Isabelle M. D. Gonzaga,
• Cristian Hessel,
• Izadora F. Reis,
• Ivo F. Teixeira,
• Lucia H. Mascaro and
• Elton Sitta

Beilstein J. Nanotechnol. 2026, 17, 806–817, doi:10.3762/bjnano.17.57

• acetylacetonate at 500 °C for 2 h. The CN/BiVO4 heterojunctions presented bandgap energy values, Eg, similar to pure BiVO4. X-ray diffraction analysis also revealed that the BiVO4 phase was not altered by the presence of the CN. However, scanning electron microscopy analysis coupled to energy-dispersive X-ray

• acquired from 10° to 80° at a rate of 2°·min−1 with a step size of 0.02°. Morphological features and elemental composition were determined by field-emission scanning electron microscopy (FEG-SEM; Zeiss Supra35) coupled with energy-dispersive X-ray spectroscopy (EDS), operating at 15 kV. Optical properties

Restorative potential of laser-synthesized silver nanoparticles with Salvia officinalis for periodontal disease treatment: an in vitro study

• Jelena Filipović Tričković,
• Sanja Živković,
• Bojana Ilić,
• Miloš Tošić,
• Jelena Marinković,
• Ana Valenta Šobot and
• Miloš Momčilović

Beilstein J. Nanotechnol. 2026, 17, 781–795, doi:10.3762/bjnano.17.55

• . AgNPs were synthesized at two laser pulse energies (2 and 6 mJ), in sage extract and deionized water, and characterized by dynamic light scattering, transmission electron microscopy, and inductively coupled plasma optical emission spectroscopy. Synthesis at 6 mJ in sage extract (SageAgNPs6mJ) yielded

• polystyrene cuvettes (DTS0012, Malvern Panalytical, UK) at ambient temperature (25 ± 0.1 °C). The selected AgNPs that displayed antimicrobial effects were further analyzed by transmission electron microscopy (TEM), to evaluate their size, shape, and dispersity. An FEI Talos F200X microscope, operating at 200

Substrate-dependent pore formation in molybdenum disulfide monolayers under ion irradiation

• Yossarian Liebsch,
• Umair Javed,
• Lucia Skopinski,
• Leon Daniel,
• Franziska Appel,
• Radia Rahali,
• Clara Grygiel,
• Henning Lebius,
• Carolin Frank,
• Lars Breuer,
• Leon Kirsch,
• Frieder Koch,
• Jani Kotakoski and
• Marika Schleberger

Beilstein J. Nanotechnol. 2026, 17, 769–780, doi:10.3762/bjnano.17.54

• highly charged ions (HCIs) and swift heavy ions (SHIs) – two types of ions that, despite having vastly different kinetic energies, both interact primarily with the electronic system of the target. Using scanning transmission electron microscopy, we quantify pore radii and pore formation efficiencies for

• under both HCI and SHI irradiation conclusively demonstrate the central role of substrate and interface-dependent electronic dissipation pathways regarding damage under these types of ion irradiation. Keywords: defects; MoS2; nanopores; SiO2; scanning transmission electron microscopy (STEM

• , high-resolution scanning transmission electron microscopy (STEM) generally requires freestanding membranes, while atomic-resolution atomic force microscopy (AFM) and scanning tunneling microscopy (STM) demand exceptionally clean surfaces; also, substrate effects can further complicate interpretation

Tailoring Ag–Pt nanoalloys through solid-state dewetting: structural and optical insights

• Marcin Łapiński,
• Piotr Okoczuk,
• Blaž Grobiša,
• Ewa Pawlikowska,
• Amelia Rozwadowska,
• Wojciech Sadowski and
• Barbara Kościelska

Beilstein J. Nanotechnol. 2026, 17, 748–759, doi:10.3762/bjnano.17.52

• under an argon atmosphere. The process induced the transformation of continuous bilayers into isolated nanoislands through solid-state dewetting. Scanning electron microscopy and transmission electron microscopy analyses revealed the formation of well-defined, nearly spherical nanoislands with a

• plasmonic properties. Results and Discussion As-deposited thin Ag–Pt bilayers exhibit a granular morphology, as evidenced by atomic force microscopy (AFM) measurements shown in Figure 1. This granular character leads to instability of the layers at higher temperatures, causing cracking of the continuous

• a region with a lower film thickness at grain boundaries, which is well visible on the linear AFM profile in Figure 1 [45][46][47]. Figure 2a presents an exemplary scanning electron microscopy (SEM) image of nanostructures formed as a result of annealing of a silver–platinum bilayer with a thickness

Oxidative atmosphere-driven formation of single-phase spinel CuRh₂O₄ nanofibers for alkaline water oxidation

• Namhee Kim,
• Sumin Ko,
• Sohyeon Choi,
• Seoyoon Jang,
• Myung Hwa Kim and
• Dasol Jin

Beilstein J. Nanotechnol. 2026, 17, 737–743, doi:10.3762/bjnano.17.50

• 609.6 cm−1 (A1g), which are consistent with the spinel CuRh2O4 lattice [17][18], supporting the XRD-based phase assignment (vide supra). As shown in Figure 4b, high-resolution transmission electron microscopy (HRTEM) analysis of the electrospun CuRh2O4 nanofibers reveals clear lattice fringes with an

• electron microscopy (SEM) was employed to investigate the surface morphology and structural uniformity of the electrospun nanofibers after post-annealing. In the as-spun state prior to annealing, the fibers containing PVP exhibit smooth surfaces with an average diameter of approximately 300 nm (Supporting

• characterization Morphology and elemental composition of the synthesized nanomaterials were examined using field-emission scanning electron microscopy (FE-SEM; JEOL JSM-6700F) and high-resolution transmission electron microscopy (HRTEM; JEOL JEM-2100F). Surface chemical states and crystallographic structures were

Environmental applications of silver nanoparticles: state-of-the-art review and emerging trends

• Soni Prajapati,
• Akash Kumar and
• Ranjana Singh

Beilstein J. Nanotechnol. 2026, 17, 697–736, doi:10.3762/bjnano.17.49

• needed before engineering AgNPs for particular applications. AgNPs are characterised using optical spectroscopy, electron microscopy, X-ray diffraction, and dynamic light scattering (DLS) to measure plasmonic absorbance, size, shape, structure, and stability [49]. Optical spectroscopy is a rapid and

• , which calculated the AgNP concentration as particles per millilitre [53]. Microscopic techniques, such as transmission electron microscopy, provide high-resolution images of individual nanoparticles, confirming morphology, size distribution, and elemental composition when coupled with energy-dispersive

• X-ray analysis [49]. TEM analysis is performed on copper grids with varying mesh sizes and coatings, with carbon/formvar-coated copper grids commonly preferred. Scanning electron microscopy (SEM) provides information on the silver nanoparticles’ surface properties and the aggregation state of dried

Molecular engineering of individual dye-based nanoparticle photostability for ultrabright two-photon fluorescence

• Eleonore Kurek,
• Sasha Cooper,
• Alexandre Clausolles,
• Karen Perronet,
• Jonathan Daniel,
• Mireille Blanchard-Desce and
• François Marquier

Beilstein J. Nanotechnol. 2026, 17, 688–696, doi:10.3762/bjnano.17.48

• nonlinear fluorescence microscopy and bioimaging applications. Keywords: bottom-up design; organic nanoparticles; two-photon fluorescence; two-photon microscopy; Introduction Dye-based fluorescent organic nanoparticles (dFONs) are a class of self-stabilized bioimaging probes composed solely of aggregated

• photobleaching behavior of individual dFONs. This was pioneered by our team, by tracking the fluorescence intensity of single dFONs over time during one-photon-excited wide-field video-microscopy SPT experiments. The resulting exponential decay plots revealed characteristic photobleaching times ranging roughly

• . Such insights are essential for optimizing fluorophore-based nanoparticles in nonlinear microscopy and other bioimaging applications where brightness and stability must be carefully balanced. Experimental Nanoparticle preparation The synthesis and characterization of the dyes are described in details

Decontamination from water pollutants and pathogens by electrospun nanofibers doped with heavy-atom-free borafluorene-BODIPY photosensitizers

• Angelika Zaszczyńska,
• Paulina H. Marek-Urban,
• Karolina Wrochna,
• Agnieszka E. Kuklewska,
• Kacper Kręgielewski,
• Marta Grodzik,
• Dawid R. Natkowski,
• Jolanta Mierzejewska,
• Ewa Iwanek,
• Agata Blacha-Grzechnik,
• Paweł Sajkiewicz and
• Krzysztof Durka

Beilstein J. Nanotechnol. 2026, 17, 668–682, doi:10.3762/bjnano.17.46

• microscopy (SEM) using a JSM-6010PLUS/LV InTouchScope™ system from JEOL (Tokyo, Japan), operating at an accelerating voltage of 11 kV. Prior to imaging, each nonwoven sample underwent a double-coating process with a thin gold layer (2–3 nm). Microstructural analysis was subsequently performed utilizing

afspm: A framework for manufacturer-agnostic automation in scanning probe microscopy

• Nicholas J. Sullivan,
• Julio J. Valdés,
• Kirk H. Bevan and
• Peter Grutter

Beilstein J. Nanotechnol. 2026, 17, 653–667, doi:10.3762/bjnano.17.45

• Centre, Ottawa ON K4A 0S2, Canada 10.3762/bjnano.17.45 Abstract Scanning probe microscopy (SPM) is a valuable technique by which one can investigate the physical characteristics of the surfaces of materials. However, its throughput is hampered by the time-consuming nature of running an experiment and

• interfaces types. An automated experiment was run to ensure overall running beyond integration testing. Keywords: atomic force microscopy; automation; manufacturer-agnostic; scanning probe microscopy; software framework; Introduction In scanning probe microscopy (SPM), an atomically sharp tip is scanned

• directly from the computer hard drive, which simplifies the translator logic as it does not need to monitor data live (which is accessible for only some controllers). The exposed level of control assumes the user has pre-configured their “operating mode” (e.g., amplitude-modulated atomic force microscopy

Two-step laser synthesis of Ag@TiO₂ nanomaterials for the photocatalytic degradation of rhodamine B

• Marija Kovačević,
• Miloš Tošić,
• Rafaela Radičić,
• Vladimir Rajić,
• Nikša Krstulović,
• Miloš Momčilović and
• Sanja Živković

Beilstein J. Nanotechnol. 2026, 17, 622–634, doi:10.3762/bjnano.17.43

• characterization was performed using scanning electron microscopy (SEM) and transmission electron microscopy (TEM) with energy-dispersive spectroscopy (EDS), aiming to establish a clear correlation between synthesis parameters, nanostructure features, and photocatalytic activity. In our previous studies [6][7][21

• microstructural examination utilizing transmission electron microscopy. Investigations were conducted using scanning transmission electron microscopy, high-angle annular dark-field with energy-dispersive spectroscopy, and conventional and high-resolution transmission electron microscopy. A drop of the suspended

Recent progress in enhancing built-in electric fields of perovskite solar cells via junction engineering

• Tong Xiao and
• Ke Xu

Beilstein J. Nanotechnol. 2026, 17, 602–621, doi:10.3762/bjnano.17.42

• constructing an n–p homojunction. Accordingly, UPS and Kelvin probe force microscopy (KPFM) measurements showed that the surface work function increased by about 0.5 eV and the potential difference increased by about 0.26 V. Mott–Schottky analysis further revealed an increase in Vbi of roughly 0.1 V

Probing tribological evolution in atomically thin MoS₂ at different scales

• Xingzhong Zeng and
• Miao Zhang

Beilstein J. Nanotechnol. 2026, 17, 586–597, doi:10.3762/bjnano.17.40

• nanoscale to sub-nanoscale, providing critical insights for designing low-friction coatings and high-performance micro/nanoelectromechanical systems (MEMS/NEMS). Keywords: atomic force microscopy; MoS2; strengthening effect; sub-nanoscale stick–slip motion; Introduction Nanoscale friction is a pivotal

• –slip events driven by in-plane tip apex motion and modulated by contact geometry via molecular dynamics (MD) simulations and frictional force microscopy (FFM) [11][12]. Despite these theoretical and simulation insights, experimental observation and quantification of sub-nanoscale stick–slip motion in

Impacts of annealing on structural and photophysical properties of zinc phthalocyanine adsorbed on graphene

• Gautier Creutzer,
• Quentin Fernez,
• Nataliya Kalashnyk,
• Zohreh Safarzadeh,
• Lydia Sosa Vargas,
• Céline Fiorini-Debuisschert,
• Nicolas Fabre and
• Fabrice Charra

Beilstein J. Nanotechnol. 2026, 17, 576–585, doi:10.3762/bjnano.17.39

• -tunneling-microscopy and optical microspectroscopy of a 2D phase change experienced by a self-assembled zinc phthalocyanine (ZnPc) monolayer adsorbed on graphene. To probe the intrinsic properties of individual ZnPc molecules, they are spatially confined within the pores of a self-assembled 2D matrix. This

• formation towards 3D self-assembly. Keywords: graphene; optical spectroscopy; organic semiconductors; phthalocyanine; scanning tunneling microscopy; self-assembly; Introduction Combining the properties of graphene and molecular semiconductors in a given material organized at the molecular scale appears as

• compared with results of scanning tunneling microscopy (STM) and scanning tunneling spectroscopy (STS) [29]. Similarly to their thicker 3D counterparts, 2D metal-free Pc [30] or metalated Pc [31] assemblies adsorbed on various substrates have shown important phase changes induced by thermal treatments. In

Upcycling agroindustrial waste into graphene oxide supports for gold nanoparticles: toward sustainable nanomaterials

• Juan Marcos Castro-Tapia,
• Selene Acosta,
• Hiram Joazet Ojeda-Galván,
• Elsie Evelyn Araujo-Palomo,
• Edgar Giovanni Villabona-Leal and
• Mildred Quintana

Beilstein J. Nanotechnol. 2026, 17, 489–504, doi:10.3762/bjnano.17.32

• = 1486.6 eV). The pass energy was set to 10 eV for high-resolution scans and to 40 eV for survey spectra. All binding energies were referenced to the C=C peak at 284.4 eV. Transmission electron microscopy (TEM) was carried using a JEOL JEM-2100 microscope operating at an accelerating voltage of 200 kV. TEM

Defects and defect-mediated engineering of two-dimensional materials: challenges and open questions

• Arkady V. Krasheninnikov,
• Matthias Batzill,
• Anouar-Akacha Delenda,
• Marija Drndić,
• Chris Ewels,
• Katharina J. Franke,
• Mahdi Ghorbani-Asl,
• Alexander Holleitner,
• Ado Jorio,
• Ute Kaiser,
• Daria Kieczka,
• Hannu-Pekka Komsa,
• Jani Kotakoski,
• Manuel Längle,
• David Lamprecht,
• Yun Liu,
• Steven G. Louie,
• Janina Maultzsch,
• Thomas Michely,
• Katherine Milton,
• Anna Niggas,
• Hanako Okuno,
• Joshua A. Robinson,
• Marika Schleberger,
• Bruno Schuler,
• Alexander Shluger,
• Kazu Suenaga,
• Kristian S. Thygesen,
• Richard A. Wilhelm,
• E. Harriet Åhlgren and
• Carla Bittencourt

Beilstein J. Nanotechnol. 2026, 17, 454–488, doi:10.3762/bjnano.17.31

• created by impacts of energetic particles [18][19][20][21] by foreign atoms. Lots of insights into the structure and properties of defective 2D materials have been obtained using transmission electron microscopy (TEM), including conventional TEM and scanning TEM (STEM). These techniques, along with

• chemical potential with 2D materials determines the defect concentration. Ideally, in situ measurements of defects are employed, but given the challenging atmosphere this may require optical methods, which may not have the required sensitivity to small defect concentrations. Ex situ microscopy measurements

• (scanning tunneling microscopy (STM) and STEM) are slower and may introduce uncertainties due to the required change in the thermodynamic conditions during transfer from the processing chamber to the vacuum in the microscope. Are defect complexes in sub-stoichiometric/impurity-doped 2D materials more

Eco-efficient materials for agricultural crops based on a mineral rich in MOR- and HEU-type zeolites

• Esperanza Yamile de la Nuez-Pantoja,
• Inocente Rodríguez-Iznaga,
• Gerardo Rodríguez-Fuentes,
• Vitalii Petranovskii,
• Ariel Martínez García,
• José Juan Calvino Gámez and
• Daniel Goma Jiménez

Beilstein J. Nanotechnol. 2026, 17, 381–395, doi:10.3762/bjnano.17.26

• urea arranged on the surface so that it covers the material and interacts with the zeolitic frameworks, was evidenced by Fourier-transform IR spectroscopy, adsorption measurements, scanning electron microscopy, scanning transmission electron microscopy, and other methods, as well as through culture

• microscopy (SEM), scanning transmission electron microscopy (STEM), N2 physisorption, and other research methods. Results and Discussion Characterization of DAP-modified zeolite CLIM The chemical compositions of natural zeolite (CLIM) from the San Andrés deposit and its modified forms (CLIMf) with ammonium

• consequence of the ion exchange processes (Equation 1) occurring during treatment of CLIM with DAP solution, which is in agreement with the data reported in [16][21][42]. Scanning electron microscopy and scanning transmission electron microscopy Microphotography (Figure 5) of natural zeolite (CLIM) revealed

Ferroelectric nanodot reservoir for neuromorphic computing

• Anna Razumnaya,
• Yuri Tikhonov,
• Dmitrii Naidenko,
• Léo Boron,
• Valerii Vinokur and
• Igor Lukyanchuk

Beilstein J. Nanotechnol. 2026, 17, 352–364, doi:10.3762/bjnano.17.24

• interfaces. An alternative configuration is shown in Figure 7b, where atomic force microscopy or piezoresponse force microscopy are used for both input and output operations. Here, the localized tip of the microscope is used to inject or sense charges at specific positions in the ferroelectric array

• and readout realized via atomic or piezoresponse force microscopy. Funding This research was funded by the European Union HORIZON action MSCA-SE-3D-TOPO (project number 101236483). A.R. acknowledges the Slovenian Research Agency support (P1-0125). The work of V.V. was supported by Terra Quantum AG.

Interconnection morphology effects on the radio frequency response of carbon nanotube sponges

• Manuela Scarselli,
• Javad Rezvani,
• Zeno Zuccari,
• Mattia Scagliotti and
• Simone Tocci

Beilstein J. Nanotechnol. 2026, 17, 343–351, doi:10.3762/bjnano.17.23

• . In particular, we observed that the response of S11 = −22.6 dB around 4.8 GHz from the CNS antenna improved after a mild treatment with ethanol, reaching S11 = −32.6 dB measured after 10 min of waiting. This observed effect is studied in detail with scanning electron microscopy and Raman spectroscopy

• findings point to a different interpretation related to the morphological effect of ethanol on the CNT mesh [27][29]. A scanning electron microscopy (SEM) study provided insights into the microstructure of the CNT film (Supporting Information File 1, Figure S1) and the sponges (Figure 3). The study

Beam shaping techniques for pulsed laser ablation in liquids: Unlocking tunable control of nanoparticle synthesis in liquids

• Sergio Molina-Prados,
• Nadezhda M. Bulgakova,
• Alexander V. Bulgakov,
• Jesus Lancis,
• Gladys Mínguez Vega and
• Carlos Doñate-Buendia

Beilstein J. Nanotechnol. 2026, 17, 309–342, doi:10.3762/bjnano.17.22

Calculation of the dynamic stiffness of a cantilever under torsional oscillation

• Keita Nishida,
• Yuuki Yasui and
• Yoshiaki Sugimoto

Beilstein J. Nanotechnol. 2026, 17, 303–308, doi:10.3762/bjnano.17.21

• Keita Nishida Yuuki Yasui Yoshiaki Sugimoto Department of Advanced Materials Science, The University of Tokyo, Chiba 277-8561, Japan 10.3762/bjnano.17.21 Abstract Atomic force microscopy using Si cantilevers provides an effective means for investigating both conservative and dissipative

• : atomic force microscopy; dynamic stiffness; energy dissipation; friction; torsional oscillation mode; Introduction Friction serves as a fundamental mechanism of energy dissipation [1]. While friction typically arises from direct mechanical contact between surfaces, energy dissipation can also occur even

• detailed mechanisms remain not fully understood [5]. Non-contact atomic force microscopy (nc-AFM) is widely employed to investigate non-contact friction through its dissipation channel. Common techniques include pendulum AFM, bimodal AFM, and quartz tuning fork AFM [6][7][8]. Pendulum AFM uses cantilevers

Advancing nanolithography: a comprehensive review of materials for local anodic oxidation with AFM

• Matteo Lorenzoni

Beilstein J. Nanotechnol. 2026, 17, 275–291, doi:10.3762/bjnano.17.19

• technique for nanoscale patterning, leveraging the precision of scanning probe microscopy, relying specifically on atomic force microscopy. This review explores the materials utilized in LAO experiments, including semiconductors, metals, insulators, two-dimensional (2D) materials, and emerging

• oxide growth on a silicon surface during LAO, illustrating the formation of a protruding oxide feature and the corresponding buried oxide volume. Reproduced from [8], M. Lorenzoni and F. Pérez-Murano, “Conductive Atomic Force Microscopy for Nanolithography Based on Local Anodic Oxidation,” in Conductive

• Atomic Force Microscopy: Applications in Nanomaterials, with permission from John Wiley and Sons. Copyright © 2017 Wiley-VCH GmbH. This content is not subject to CC BY 4.0. (c) AFM images of square oxide patterns fabricated by LAO on SiC before and after wet etching. (d) Height profile of the top left

Durable antimicrobial activity of fabrics functionalized with zeolite ion-exchanged nanomaterials against Staphylococcus aureus and Escherichia coli

• Perla Sánchez-López,
• Kendra Ramirez Acosta,
• Sergio Fuentes Moyado,
• Ruben Dario Cadena-Nava and
• Elena Smolentseva

Beilstein J. Nanotechnol. 2026, 17, 262–274, doi:10.3762/bjnano.17.18

• atom % are evaluated regarding their antimicrobial activity against Staphylococcus aureus (Gram-positive) and Escherichia coli (Gram-negative), as well as regarding their physicochemical and mechanical properties. Scanning electron microscopy confirms the uniform distribution and successful

• ). Scanning electron microscopy confirmed the effective incorporation and uniform distribution of the nanomaterials on the fabric surface, facilitated by a 10% w/w acrylic resin binder. Among the tested materials, silver-based fabrics displayed the highest antibacterial efficacy, followed by copper and zinc

• , transmission electron microscopy (TEM) images were obtained using a JEOL JEM-2200FS (200 kV), and elemental analysis was performed using EDS. The crystalline structure of the modified fabrics was determined by X-ray diffraction (XRD) in a Panalytical AERIS diffractometer using Cu Kα (λ = 1.54184 Å). The

Multilayered hyperbolic Au/TiO₂ nanostructures for enhancing the nonlinear response around the epsilon-near-zero point

• Fernando Arturo Araiza-Sixtos,
• Mauricio Gomez-Robles,
• Rafael Salas-Montiel and
• Raúl Rangel-Rojo

Beilstein J. Nanotechnol. 2026, 17, 251–261, doi:10.3762/bjnano.17.17

• actually was not at 800 nm, but rather at 600 nm. We tried to find the reason of this shift with our available resources. Transmission electron microscopy showed that there was no significant change in the geometry, which could have resulted in the ENZ shift. We could not study the composition of the

• oscillator as a starting material for Au, and with TiO2 with Cody–Lorentz oscillators as starting material for TiO2. Scanning electron microscopy (Hitachi SU8030) was used to obtain the cross-sectional image (below in Figure 4a), with the sample oriented to expose the ENZ material edge to the electron beam

• the deposited layers. In Table 1, we can see that we have widths for every stack that are different from the ones proposed for the simulated ENZ points. This change in thickness was also seen in scanning electron microscopy (SEM). In Figure 4a we present a SEM image of the ML800 structure; we see that

Comparative study on 3D morphologies of delignified, single tracheids and fibers of five wood species

• Helen Gorges,
• Felicitas von Usslar,
• Cordt Zollfrank,
• Silja Flenner,
• Imke Greving,
• Martin Müller,
• Clemens F. Schaber,
• Chuchu Li and
• Stanislav N. Gorb

Beilstein J. Nanotechnol. 2026, 17, 239–250, doi:10.3762/bjnano.17.16

• . Scanning electron microscopy was used to compare the morphology between untreated and delignified fibers and tracheids. X-ray tomography enabled us to reconstruct high-resolution 3D models of delignified single tracheids or fibers, providing information on the pit arrangements. Moreover, delignification

• largely absent from scientific literature. Although previous studies have examined wood anatomy using various imaging techniques, such as X-ray micro-computed tomography in addition to scanning and transmission electron microscopy [22][23][24][25][26][27], high-resolution 3D reconstructions of single

• species in this study by observation of the structural differences after delignification. Using X-ray tomography, we were able to build 3D models of single fibers and tracheids. Additionally, we imaged untreated and delignified samples using scanning electron microscopy for measuring fiber and tracheid