Synthesis of biowaste-derived carbon-dot-mediated silver nanoparticles and the evaluation of electrochemical properties for supercapacitor electrodes

• Navya Kumari Tenkayala,
• Chandan Kumar Maity,
• Md Moniruzzaman and
• Subramani Devaraju

Beilstein J. Nanotechnol. 2025, 16, 933–943, doi:10.3762/bjnano.16.71

• energy demand. Therefore, a notable research focus has been given to advancements in renewable energy storage systems. Secondary batteries and supercapacitors are promising alternatives for energy storage applications [1][2]. Through the electrostatic polarization of electrolyte solutions, supercapacitor

• color changing from brown to dark brownish black confirmed the synthesis of PG-CDs-AgNP within 2 h. After 2 h of reaction, the sample was collected for UV–vis studies. The UV–vis spectra were also implemented at 12 and 24 h, respectively. The growth and the formation of PG-CDs-AgNP were recorded by

• absorption bands of PG-CDs-AgNPs was acquired at various time intervals to study the production and growth of nanoparticles over time. The gradual growth of PG-CDs-AgNPs has been checked and depicted in Figure 1b. The SPR peak was noticed within 2 h of reaction with PG-CDs, with a visible change in color of

Structural and magnetic properties of microwave-synthesized reduced graphene oxide/VO₂/Fe₂O₃ nanocomposite

• Sumanta Sahoo,
• Ankur Sood and
• Sung Soo Han

Beilstein J. Nanotechnol. 2025, 16, 921–932, doi:10.3762/bjnano.16.70

• . Keywords: Fe2O3; magnetism; microwave irradiation; reduced graphene oxide; VO2; Introduction Graphene-based materials have been significantly explored in various fields of materials science due to their unique physical and chemical characteristics [1][2][3][4]. The special arrangement of carbon materials

• be ascribed to significant exfoliation of the graphite oxide to form the rGO. Figure 2 schematically summarizes the effects of MW irradiation on the mixed powder of graphite oxide and metal oxide precursors. The short-life MW irradiation was also successful in converting V2O5 to VO2. This type of

• element (derived from rGO). The data thus obtained was in coherence with the reported results from XRD and EDX analysis. Additionally, the high-resolution XPS spectrum of V 2p designates two major peaks at 516.5 and 523.3 eV, which can be ascribed to the V 2p3/2 and V 2p1/2, respectively (Figure 7b) [40

Focused ion beam-induced platinum deposition with a low-temperature cesium ion source

• Thomas Henning Loeber,
• Bert Laegel,
• Meltem Sezen,
• Feray Bakan Misirlioglu,
• Edgar J. D. Vredenbregt and
• Yang Li

Beilstein J. Nanotechnol. 2025, 16, 910–920, doi:10.3762/bjnano.16.69

• magnetic or superconductive structures can be created [1][2][3][4]. Also, specific mechanical structures on atomic force microscopy (AFM) cantilevers can be made [5][6]. In the literature, four mechanisms are used to explain the complex process of focused ion beam-induced deposition (FIBID) [5][7]; the

• time, and refresh time, precursor material and substrate have an influence on the effective deposition rate. Gallium (Ga+) and helium (He+) are the most often utilized ion species for FIBID [1][2][5]. Besides these standard FIB systems, new kinds of laser-cooled ion sources have been developed in the

• , ion currents from 16 to 285 pA were used, so the current densities were between 0.9 and 14.2 pA·μm−2. The overall deposition time was kept constant at 2:30 min, and the ion dose was changed from 128 to 2138 pC·μm−2. The ions were accelerated with voltages of 2, 5, 8, and 16 kV, while the measured ion

Characterization of ion track-etched conical nanopores in thermal and PECVD SiO₂ using small angle X-ray scattering

• Shankar Dutt,
• Rudradeep Chakraborty,
• Christian Notthoff,
• Pablo Mota-Santiago,
• Christina Trautmann and
• Patrick Kluth

Beilstein J. Nanotechnol. 2025, 16, 899–909, doi:10.3762/bjnano.16.68

• differences between the nanopores in thermal and PECVD SiO2. The track-to-bulk etching rate ratio is significantly different for the two materials, producing nanopores with cone angles that differ by almost a factor of two. Furthermore, thermal SiO2 exhibits an exceptionally narrow size distribution of only 2

• attracted significant attention in the past decade because of their broad applicability in a variety of areas including biosensing, micro/ultrafiltration, desalination, ion and molecular separation, dialysis, battery technologies, blue energy generation, and nanofluidics [1][2][3][4][5][6][7][8][9][10][11

• uncertainties in dimensional measurements and makes it challenging to obtain robust structural information about the nanopores. Figure 2 shows a representative 2D scattering pattern obtained from conical nanopores in thermal SiO2. This image represents the simultaneous measurement of approximately 107 parallel

Heat-induced transformation of nickel-coated polycrystalline diamond film studied in situ by XPS and NEXAFS

• Olga V. Sedelnikova,
• Yuliya V. Fedoseeva,
• Dmitriy V. Gorodetskiy,
• Yuri N. Palyanov,
• Elena V. Shlyakhova,
• Eugene A. Maksimovskiy,
• Anna A. Makarova,
• Lyubov G. Bulusheva and
• Aleksandr V. Okotrub

Beilstein J. Nanotechnol. 2025, 16, 887–898, doi:10.3762/bjnano.16.67

• producing hybrid materials which combine these two forms of carbon [1][2][3]. In particular, such graphene-on-diamond heterostructures have been shown to be attractive for power electronics [4][5], microelectronic devices [6][7], and detectors [7][8]. At room temperature and atmospheric pressure, carbon in

• spectra were measured upon excitation by photons with energies of 830 and 330 eV to probe different surface depths of the samples after annealing (Figure 2). In these cases, the inelastic mean free path for electrons emitted from the C 1s level in diamond is about 1.0 nm (probing depth of 3 nm) for 830 eV

• to sp2-hybridized carbon atoms. The relative area of this sp2-peak is 3% in the spectrum measured at 830 eV, and becomes significantly larger (16%) as the photon excitation energy decreases to 330 eV. The rather small amount of sp2 carbon in the 2 nm thick surface layer indicates that the temperature

Ar⁺ implantation-induced tailoring of RF-sputtered ZnO films: structural, morphological, and optical properties

• Manu Bura,
• Divya Gupta,
• Arun Kumar and
• Sanjeev Aggarwal

Beilstein J. Nanotechnol. 2025, 16, 872–886, doi:10.3762/bjnano.16.66

• Manu Bura Divya Gupta Arun Kumar Sanjeev Aggarwal Department of Physics, Kurukshetra University, Kurukshetra, 136119, India 10.3762/bjnano.16.66 Abstract Radio frequency-sputtered zinc oxide films are implanted with 30 keV Ar+ ions at various fluences ranging from 1 × 1015 to 2 × 1016 ions·cm−2

• promising material for device fabrication in different fields, namely, spintronics, nanoelectronics, and photonics [1][2]. It possesses a wide bandgap of 3.37 eV [3] and has a large exciton binding energy of about 60 meV [4], which assures the stability of ZnO film-based devices such as liquid crystal

• 2.5 × 1015 ions·cm−2. Gupta et al. [14] have investigated the activation of the A1 (LO) mode and the production of a broad band at the lower Raman shift side in ZnO films implanted with 300 keV argon and 1.2 MeV xenon ions with varying fluence from 1 × 1014 to 3 × 1015 ions·cm−2. Gautam et al. [15

Insights into the electronic and atomic structures of cerium oxide-based ultrathin films and nanostructures using high-brilliance light sources

• Paola Luches and
• Federico Boscherini

Beilstein J. Nanotechnol. 2025, 16, 860–871, doi:10.3762/bjnano.16.65

• ; Introduction Transition metal oxides in the form of thin films or nanostructures find extensive use in sustainable energy technologies [1][2]. They serve as active materials or supports for catalysts for various chemical reactions, essential to energy conversion, sensing, and environmental remediation [3][4

• spectrum shows only minor modifications after annealing, while if the Ce3+-related resonant energy is used (125 eV), a marked Ce 4f peak appears around 2 eV binding energy after the annealing. This demonstrates the significantly higher sensitivity to Ce3+ that can be achieved by exploiting resonant

• its sensitivity, the method, when combined with other techniques, has provided quantitative information on the number of electrons transferred per particle to the support (Figure 2), enabling the optimization of the size of the supported active Pt catalyst [27]. This is a crucial factor in minimizing

Synchrotron X-ray photoelectron spectroscopy study of sodium adsorption on vertically arranged MoS₂ layers coated with pyrolytic carbon

• Alexander V. Okotrub,
• Anastasiya D. Fedorenko,
• Anna A. Makarova,
• Veronica S. Sulyaeva,
• Yuliya V. Fedoseeva and
• Lyubov G. Bulusheva

Beilstein J. Nanotechnol. 2025, 16, 847–859, doi:10.3762/bjnano.16.64

• capacity and cycle life of SIBs. Molybdenum disulfide (MoS2) has a layered structure and a high theoretical capacity of 669 mAh·g−1, so it is considered as a promising anode material for SIBs [1][2]. The large sodium ion can diffuse with a low energy barrier between the S−Mo−S layers due to the interlayer

• about 2 and 7 atom % after coating the film with PyC. Figure 4 compares the S/Mo, Na/Mo, and Na/C ratios in the samples determined from the XPS survey spectra measured at excitation photon energies of 470 and 830 eV. The former energy provides a probing depth of about 1 nm and therefore allows for the

• and PyC-MoS2 films is shown in Figure 5. The low-energy peak at 226.1–226.3 eV corresponds to the S 2s line. The Mo 3d spectra of the initial MoS2 and PyC-MoS2 consist of an intense spin–orbit doublet with the binding energy of the Mo 3d5/2 component of 228.9 eV (Figure 5a,b). This energy corresponds

Facile one-step radio frequency magnetron sputtering of Ni/NiO on stainless steel for an efficient electrode for hydrogen evolution reaction

• Ha Huu Do,
• Khac Binh Nguyen,
• Phuong N. Nguyen and
• Hoai Phuong Pham

Beilstein J. Nanotechnol. 2025, 16, 837–846, doi:10.3762/bjnano.16.63

• efficiency. The evaluation of catalytic activities revealed that the optimal sample of Ni/NiO/SS-10 displayed a higher HER performance than bare SS. To produce H2 at a current density of 10 mA·cm−2, this electrode required a low overpotential of 184 mV and demonstrated remarkable durability over 12 h of

• increasing consumption of fossil fuels, causing CO2 emissions and resulting in climate change [1]. Hydropower can be harnessed to provide sustainable energy for future generations because there are no harmful emissions with only water vapor as a byproduct [2][3][4]. Also, hydropower offers better energy

• and O peaks. The chemical state of Ni is further analyzed by the Ni 2p3/2 peaks. As depicted in Figure 5b, the Ni 2p3/2 spectrum can be deconvoluted into four peaks. The peaks at 852.8, 853.7, and 855.8 eV correspond to Ni0, Ni2+, and Ni3+, respectively. Another broad peak at nearly 861 eV is

Synthesis and magnetic transitions of rare-earth-free Fe–Mn–Ni–Si-based compositionally complex alloys at bulk and nanoscale

• Shabbir Tahir,
• Tatiana Smoliarova,
• Carlos Doñate-Buendía,
• Michael Farle,
• Natalia Shkodich and
• Bilal Gökce

Beilstein J. Nanotechnol. 2025, 16, 823–836, doi:10.3762/bjnano.16.62

• field, exhibit an adiabatic temperature change, enabling energy-efficient and environmentally friendly refrigeration [2]. These solid-state cooling systems are being developed as alternatives to conventional gas-based refrigeration and are especially advantageous for applications requiring tailored

• Ni55.2Mn18.6Ga26.2, a giant magnetocaloric response with a ΔS of −20.4 J·kg−1·K−1 at 317 K in a 5 T field can be achieved compared to Ni57.2Mn15.9Ga27.0 where a ΔS of just −2 J·kg−1·K−1 at 310 K was witnessed. Within the myriad of material systems exhibiting magnetic transitions, compositionally complex alloys (CCAs

• transition near 200 K with an isothermal entropy change of −23 J·kg−1·K−1 at 2 T, respectively. Bulk CCAs are explored thanks to the metallurgy approaches that allow for material composition control and alloying. However, it is desirable to achieve controlled methodologies to downsize CCAs to the nanoscale

Supramolecular hydration structure of graphene-based hydrogels: density functional theory, green chemistry and interface application

• Hon Nhien Le,
• Duy Khanh Nguyen,
• Minh Triet Dang,
• Huyen Trinh Nguyen,
• Thi Bang Tam Dao,
• Trung Do Nguyen,
• Chi Nhan Ha Thuc and
• Van Hieu Le

Beilstein J. Nanotechnol. 2025, 16, 806–822, doi:10.3762/bjnano.16.61

• deoxyribonucleic acid (DNA) [1]. Water molecules and their hydrogen bonding network function as lubricants for biomolecular dynamics. Recent scientific works have analyzed the important role of hydration shells on DNA, proteins, and phospholipid membranes [2][3][4]. The first hydration shell (about 3.5 Å) at the

• exothermic heat increased the reactor temperature to above 90 °C). After 2 h of agitation, the reaction was mixed with 150 mL of a 5% H2O2 solution and kept stirring for one day. After washing to neutral pH, the material was dried and ground to produce a GrO powder (moisture ≈20%). Next, the GrO powder was

• synthesis and brush coating experiments. Synthesis of graphene oxide–nanosilica–zinc hydroxide hydrogel The suspension of 0.625 g GrO and 250 mL of water was agitated and then sonicated for 1 h. The suspension was decanted to collect about 250 mL of GO dispersion. An amount of 4.4 g of Zn(CH3COO)2·2H2O was

Morphology and properties of pyrite nanoparticles obtained by pulsed laser ablation in liquid and thin films for photodetection

• Akshana Parameswaran Sreekala,
• Bindu Krishnan,
• Rene Fabian Cienfuegos Pelaes,
• David Avellaneda Avellaneda,
• Josué Amílcar Aguilar-Martínez and
• Sadasivan Shaji

Beilstein J. Nanotechnol. 2025, 16, 785–805, doi:10.3762/bjnano.16.60

• a narrow bandgap (0.95 eV), high light absorption coefficient (≈105 cm−1), excellent properties in photoelectric conversion, and has enormous potential as an efficient photodetector system and in lithium batteries [1][2]. The prevalent forms of FeS2 are cubic-system pyrite and the orthorhombic

• repetition frequency of 100 Hz, and energy of 90 mJ/pulse was used. In each solvent, laser ablation was carried out for 10 minutes with the aid of a focusing lens (focal length of 50 cm) kept at a 25 cm distance from the target. The laser fluence calculated at this point was 0.23 J·cm−2. Images of the pyrite

• parallel to one another and immersed in 12.5 mL FeS2 nanocolloid (FIPA) kept at room temperature during EPD. A potential difference of 400 V (constant voltage, with current of approximately 2 mA) was applied after optimization of EPD conditions. The deposition was carried out for 1 h. The positive

Changes of structural, magnetic and spectroscopic properties of microencapsulated iron sucrose nanoparticles in saline

• Sabina Lewińska,
• Pavlo Aleshkevych,
• Roman Minikayev,
• Anna Bajorek,
• Mateusz Dulski,
• Krystian Prusik,
• Tomasz Wojciechowski and
• Anna Ślawska-Waniewska

Beilstein J. Nanotechnol. 2025, 16, 762–784, doi:10.3762/bjnano.16.59

• that stabilized the entire nanoparticle [2][3][4]. Such a variety of the iron delivery drugs in the pharmaceutical market results from the continuous improvement of their properties, such as absorption of iron in the human body, time of iron release after administration to the patient, and shape and

• separated from each other and not magnetically interacting. There are many others literature examples of studies of chemical and physical properties on iron deficiency drugs and their usage in agents [2][7][8][11][12][13][14][15]. However, in this work the whole attention is focused on the iron deficiency

• core–shell nanoparticle form, where the shell consists of sucrose, while the core is iron(III) oxide mineral. The average diameter of iron sucrose nanoparticles included in Venofer® was estimated as ≈7 nm, whose core diameter is 3 nm [2][7][8][13]. The elemental analysis for a single iron sucrose

Thickness dependent oxidation in CrCl₃: a scanning X-ray photoemission and Kelvin probe microscopies study

• Shafaq Kazim,
• Rahul Parmar,
• Maryam Azizinia,
• Matteo Amati,
• Muhammad Rauf,
• Andrea Di Cicco,
• Seyed Javid Rezvani,
• Dario Mastrippolito,
• Luca Ottaviano,
• Tomasz Klimczuk,
• Luca Gregoratti and
• Roberto Gunnella

Beilstein J. Nanotechnol. 2025, 16, 749–761, doi:10.3762/bjnano.16.58

• of CrCl3 [2], which can be easily exfoliated and exhibits a slower degradation rate compared to CrI3 or CrBr3[3]. To fully exploit the potential of any material, a detailed understanding of its electronic and structural changes arising from intrinsic and extrinsic defects is crucial [4]. Despite this

• [2][11][8][10], focusing on thin layered flakes and the role of the layer thicknesses obtained by spectro- and scanning microscopy with a lateral resolution of a few tens of nanometers. The interaction with the supporting substrate is a crucial factor [3][12] regarding the properties of the flakes

• known that 270 nm SiO2/Si substrates provide the highest optical contrast (O.C.) value for a single layer or few layers of CrCl3 [2][11]. Because of the insulating behavior of 270 nm SiO2 and to avoid surface charging, we utilized Si(001) wafers with a 1 nm layer of SiO2 and ITO films (190 nm) on glass

Serum heat inactivation diminishes ApoE-mediated uptake of D-Lin-MC3-DMA lipid nanoparticles

• Demian van Straten,
• Luuk van de Schepop,
• Rowan Frunt,
• Pieter Vader and
• Raymond M. Schiffelers

Beilstein J. Nanotechnol. 2025, 16, 740–748, doi:10.3762/bjnano.16.57

• proteins, forms on its surface. This so-called protein corona significantly affects the physicochemical properties of the nanoparticle, such as size, charge and stability [2][3][4][5]. In turn, the composition of the protein corona is influenced by the physicochemical properties of the pristine

• MDA-MB-231 (ATCC) were cultured in DMEM medium with 10% FCS (Gibco) and 1% penicillin-streptomycin (PS) (Fisher Scientific). The human dermal microvascular endothelial cell line HMEC-1 (ATCC) was cultured in MCDB-131 medium supplemented with 10% FCS (Gibco), 2 mM l-glutamine (Gibco), 10 ng/mL rhEGF

• molar ratio of 50:38.5:10:1.5 and a final lipid concentration of 10 mM. siRNA was diluted in an acetate buffer (25 mM, pH 4.0) to a final concentration of 3.3 µM for MC3 LNPs and 12.33 µM for C12 LNPs. For fluorescent LNPs, siRNA and siRNA-AF647 were mixed 2:1 v/v. For MC3 LNPs the Nanoassemblr was set

Synthesis of a multicomponent cellulose-based adsorbent for tetracycline removal from aquaculture water

• Uyen Bao Tran,
• Ngoc Thanh Vo-Tran,
• Khai The Truong,
• Dat Anh Nguyen,
• Quang Nhat Tran,
• Huu-Quang Nguyen,
• Jaebeom Lee and
• Hai Son Truong-Lam

Beilstein J. Nanotechnol. 2025, 16, 728–739, doi:10.3762/bjnano.16.56

• crucial role in the global economy, particularly for coastal nations, including Vietnam. However, its multibillion dollar contributions are accompanied by the growing problem of excess antibiotic usage, notably tetracyclines (TCs), a widely used class of antibiotics in recent years [1][2][3][4]. Recent

• will be applied in the synthesis of an adsorbent for TC removal from water. Material characterization FE-SEM and FTIR results Figure 2 presents comparative field-emission SEM (FE-SEM) images and FTIR spectra of commercial CMC and PGC. Notably, the FE-SEM analysis of PGC (Figure 2d–f) reveals

• follows the monolayer adsorption mechanism described by the Langmuir model, the degree of fit was evaluated using the equilibrium coefficient RL. Notably, the RL values, calculated in Table 2 and presented in Figure 5c, range from 0.167 to 0.334, indicating that TC adsorption onto PGC is favorable and

Efficiency of single-pulse laser fragmentation of organic nutraceutical dispersions in a circular jet flow-through reactor

• Tina Friedenauer,
• Maximilian Spellauge,
• Alexander Sommereyns,
• Verena Labenski,
• Tuba Esatbeyoglu,
• Christoph Rehbock,
• Heinz P. Huber and
• Stephan Barcikowski

Beilstein J. Nanotechnol. 2025, 16, 711–727, doi:10.3762/bjnano.16.55

• concentrations. In all experiments, chemical degradation was minimal (<2%), and increased mass concentration of curcumin enabled ultralow by-product formation of 0.01%. The process selectivity against degradation was defined by the application-relevant descriptor of mole degradation per produced submicrometer

• few decades, as this relatively new fabrication method can be used to produce stable, additive-free colloids of different material classes under high-purity conditions, which are suitable for a wide range of technical applications [1][2][3][4][5]. Pulsed laser ablation (LAL), laser fragmentation (LFL

• iron phthalocyanines (FePc), but also some purely organic dyes such as naphthalocyanides [25], perylenes [26], perylene diimides [27][28], fullerenes [29][30], and quinacridones [2][31] have been successfully downsized to the nanoscale using nanosecond- and femtosecond-LFL with wavelengths in the UV

Nanostructured materials characterized by scanning photoelectron spectromicroscopy

• Matteo Amati,
• Alexey S. Shkvarin,
• Alexander I. Merentsov,
• Alexander N. Titov,
• María Taeño,
• David Maestre,
• Sarah R. McKibbin,
• Zygmunt Milosz,
• Ana Cremades,
• Rainer Timm and
• Luca Gregoratti

Beilstein J. Nanotechnol. 2025, 16, 700–710, doi:10.3762/bjnano.16.54

• the materials formed by similar building blocks, then having similar properties, are called phases from which another possible definition of these heterogeneous materials such as multi-phase materials comes [2][3][4]. Nanostructured materials are the playground for the advancement of some key

• why these structural fragments form a single crystal and not independent phases. An analysis of the binding energy of the core levels of Cr 3p, Ti 3p, Ti 2p, and Cr 2p3/2 (Figure 1d–f) in the different fragments reveals a shift of about 0.5 eV in the binding energy, indicating that the fragments are

• spectra were obtained along the nanowire with a step width of about 130 nm, roughly equaling the size of the X-ray beam, as indicated in Figure 2d. The resulting In 3d5/2 spectra are shown in Figure 2e for the unbiased case, highlighting the p-doped and n-doped nanowire segments with the depletion zone in

High-temperature epitaxial growth of tantalum nitride thin films on MgO: structural evolution and potential for SQUID applications

• Michelle Cedillo Rosillo,
• Oscar Contreras López,
• Jesús Antonio Díaz,
• Agustín Conde Gallardo and
• Harvi A. Castillo Cuero

Beilstein J. Nanotechnol. 2025, 16, 690–699, doi:10.3762/bjnano.16.53

• transition temperature (Tc). Discovered in 1911 by Heike Kamerlingh Onnes [1], superconductors exhibit unique properties, including perfect conductivity and the Meissner effect [2], that is, the expulsion of magnetic fields. These remarkable properties make them highly valuable for diverse applications, such

• electronic devices operating in the gigahertz range. Transition-metal compounds, such as nitrides and carbides (e.g., NbN, TiN, TiC, and TaN), have demonstrated Tc values ranging from 2 to 10.4 K [3][4][5][6]. These compounds constitute a significant class of materials because of their exceptional physical

• frequency of 7.5 Hz, the substrate-to-target distance was 5 cm, and the incident energy density was 4.88 J·cm−2. We studied the stoichiometry and properties of the thin films as a function of gas pressure by introducing N2 to realize RPLD. At this time, the ion pumps were closed and isolated from the PLD

The impact of tris(pentafluorophenyl)borane hole transport layer doping on interfacial charge extraction and recombination

• Konstantinos Bidinakis and
• Stefan A. L. Weber

Beilstein J. Nanotechnol. 2025, 16, 678–689, doi:10.3762/bjnano.16.52

• ; hole transport layer doping; Kelvin probe force microscopy; perovskite solar cells; Introduction Perovskite solar cells (PSCs) are a promising class of photovoltaic material that exhibits high power conversion efficiencies and relies on a low-cost solution-processed fabrication method [1][2][3][4]. At

• -sections by means of argon ion polishing. To get results that closely simulate the operation of working devices, we used a comprehensive static KPFM measurement protocol (See Supporting Information File 1, Section 2) and measured potential profiles across all layers while applying a voltage or under

• smooth cross-section. This is useful for getting stable KPFM images, without electrostatic cross-talk. At every step of this procedure, the current–voltage characteristics were being monitored, as shown in Figure 2. By carefully selecting the parameters of the ion milling, we can ensure that the exposed

Colloidal few layered graphene–tannic acid preserves the biocompatibility of periodontal ligament cells

• Teissir Ben Ammar,
• Naji Kharouf,
• Dominique Vautier,
• Housseinou Ba,
• Nivedita Sudheer,
• Philippe Lavalle and
• Vincent Ball

Beilstein J. Nanotechnol. 2025, 16, 664–677, doi:10.3762/bjnano.16.51

• , 67034 Strasbourg Cedex 2 BP43, France 10.3762/bjnano.16.51 Abstract Dental diseases pose a global health concern. In addition to medication and care, the use of biocompatible and even bioactive dental materials can contribute to global oral health. Among such materials, nanomaterials begin to be used

• transformative approach to enhance their efficacy [2]. Actually, incorporating nanomaterials into dental biomaterials has already offered advantages like enhanced tissue regeneration, increased mechanical strength of composites, and improved sealing of filler materials [3]. Graphene-based materials (GBMs) stand

• out for their potential in dentistry due to their high specific surface area, mechanical strength and adaptability for biological and chemical modifications [4][5]. For instance, a previous study demonstrated that incorporating 2% (w/w) graphene oxide into a resin-modified glass ionomer cement

Aprepitant-loaded solid lipid nanoparticles: a novel approach to enhance oral bioavailability

• Mazhar Hussain,
• Muhammad Farooq,
• Muhammad Asad Saeed,
• Muhammad Ijaz,
• Sherjeel Adnan,
• Zeeshan Masood,
• Muhammad Waqas,
• Wafa Ishaq and
• Nabeela Ameer

Beilstein J. Nanotechnol. 2025, 16, 652–663, doi:10.3762/bjnano.16.50

• major health problem worldwide, and cancer patients are treated by using conventional strategies such as surgery, chemotherapy, and radiotherapy, alone or in combination [1]. Chemotherapy is the basis of pharmacological cancer treatments [2]. The most common adverse effects in cancer patients induced by

• patients in the delayed phase (days 2 to 5) in their first cycle of high-dose cisplatin [5]. Aprepitant (APT) is a selective antagonist of neurokinin-1 receptor that blocks the substance P emetic effect. NK-1 receptors occur in the gastrointestinal tract on vagal afferents and in the nucleus of the

• plasma (Cmax) is reached after approx. 4 h, and the half-life is 9–13 h. An oral dose of 125 mg APT one hour before chemotherapy treatment (day 1), and 80 mg daily in the morning on days 2 and 3 are recommended [7]. APT is strongly bound to plasma protein (95%); it is absorbed slowly and crosses the

Nanoscale capacitance spectroscopy based on multifrequency electrostatic force microscopy

• Pascal N. Rohrbeck,
• Lukas D. Cavar,
• Franjo Weber,
• Peter G. Reichel,
• Mara Niebling and
• Stefan A. L. Weber

Beilstein J. Nanotechnol. 2025, 16, 637–651, doi:10.3762/bjnano.16.49

• way for the design of materials with tailored functionalities [1][2][3][4][5][6]. Dielectric properties are fundamental for understanding the behavior and performance of various material systems, as they directly influence charge storage, polarization, and energy dissipation mechanisms. For instance

• frequency space. Single-pass second-harmonic EFM in the attractive regime has been used to detect the cantilever response at the second harmonic of the electrostatic force (2ω) [68][69][70][72] generated when Δωe spans the range from 8 kHz to 2 MHz [70]. SCFM in the megahertz regime has been implemented [70

• the gradient of the energy, WC, stored in the tip–sample capacitor C with respect to the tip–sample separation z, as given by where Vtip−sample specifies the electrical voltage across the tip–sample gap. In conventional EFM with single-frequency excitation, Vtip−sample is given by Equation 2 [18

A formulation containing Cymbopogon flexuosus essential oil: improvement of biochemical parameters and oxidative stress in diabetic rats

• Ailton Santos Sena-Júnior,
• Cleverton Nascimento Santana Andrade,
• Pedro Henrique Macedo Moura,
• Jocsã Hémany Cândido dos Santos,
• Cauãn Torres Trancoso,
• Eloia Emanuelly Dias Silva,
• Deise Maria Rego Rodrigues Silva,
• Ênio Pereira Telles,
• Luiz André Santos Silva,
• Isabella Lima Dantas Teles,
• Sara Fernanda Mota de Almeida,
• Daniel Alves de Souza,
• Jileno Ferreira Santos,
• Felipe José Aidar Martins,
• Ana Mara de Oliveira e Silva,
• Sandra Lauton-Santos,
• Guilherme Rodolfo Souza de Araujo,
• Cristiane Bani Correa,
• Rogéria De Souza Nunes,
• Lysandro Pinto Borges and
• Ana Amélia Moreira Lira

Beilstein J. Nanotechnol. 2025, 16, 617–636, doi:10.3762/bjnano.16.48

• reach 700 million cases by 2045 [1]. The main causes of DM are related to a deficit in insulin production due to a loss of pancreatic β-cell function (type-1 DM) [1], or due to insulin resistance and a partial deficit in the secretion of this hormone by pancreatic β-cells (type-2 DM). Various therapies

• have been used in the treatment of patients with DM including medication using hypoglycemic agents alone or combined with the administration of exogenous insulin, associated with dietary re-education and changes in lifestyle habits, such as physical exercise [2]. Although hypoglycemic agents are widely

• temperatures (25 and 37 °C) was analyzed. The results were expressed in rheograms (Figure 2) and represent the relationship between the shear stress and the shear rate. The data were analyzed using the power law (τ = k⋅γn), where τ is the shear rate, k is the consistency index (viscosity), γ is the shear

Focused ion and electron beams for synthesis and characterization of nanomaterials

• Aleksandra Szkudlarek

Beilstein J. Nanotechnol. 2025, 16, 613–616, doi:10.3762/bjnano.16.47

• the best of times, it was the worst of times" [2] – onto a 200 × 200 micron square of plastic using an electron beam. This achievement prompts a reflection: is nowadays the best or the worst of times for the development of electron and ion beam technologies? With the hope to contribute addressing this

• deposition techniques, this thematic issue includes studies on low-energy electron interactions with metal(II) bis(acetylacetonate) complexes [5]. Another molecule investigated for its gas-phase fragmentation mechanism via dissociative ionization and dissociative electron attachment is [Au(CH3)2Cl]2. Studies