Electrical and optical enhancement of ITO/Mo bilayer thin films via laser annealing

• Abdelbaki Hacini,
• Ahmad Hadi Ali,
• Nurul Nadia Adnan and
• Nafarizal Nayan

Beilstein J. Nanotechnol. 2022, 13, 1589–1595, doi:10.3762/bjnano.13.133

• roughness of the bilayer structure were studied utilizing an atomic force microscope (AFM, Bruker Dimension Edge) and the Gwyddion software. The optical transmission was measured using an UV–vis spectrophotometer (UV-3600i Plus, SHIMADZU) in the range of λ = 300–800 nm. Finally, the electrical properties

Single-step extraction of small-diameter single-walled carbon nanotubes in the presence of riboflavin

• Polina M. Kalachikova,
• Anastasia E. Goldt,
• Eldar M. Khabushev,
• Timofei V. Eremin,
• Timofei S. Zatsepin,
• Elena D. Obraztsova,
• Konstantin V. Larionov,
• Liubov Yu. Antipina,
• Pavel B. Sorokin and
• Albert G. Nasibulin

Beilstein J. Nanotechnol. 2022, 13, 1564–1571, doi:10.3762/bjnano.13.130

• stabilizing agent for aqueous SWCNT dispersions The UV–vis–NIR spectrum of CoMoCat SWCNT/riboflavin dispersion obtained by mild sonication reveals the distinctive S11 and S22 transitions of (6,4)- and (6,5)-SWCNTs, as well as other resolved optical transitions of nanotubes (Figure 1a). Notably, Van Hove

• an average diameter of 1.5 nm. The set of chiralities present in CoMoCat demonstrates a high affinity towards riboflavin, leading to a high riboflavin density on the SWCNT surface. As a result, we do not observe significant changes in UV–vis–NIR spectra or photoluminescence of dispersions before and

• ) reveals almost single (6,5)-chiral SWCNTs with traces of (7,3)-SWCNTs, which is in agreement with the UV–vis–NIR spectrum. Ab initio calculations of riboflavin binding to SWCNTs Papadimitrakopolous et al. showed that flavin mononucleotide selectively binds to (8,6)-nanotubes resulting in the formation of

Photoelectrochemical water oxidation over TiO₂ nanotubes modified with MoS₂ and g-C₃N₄

• Phuong Hoang Nguyen,
• Thi Minh Cao,
• Tho Truong Nguyen,
• Hien Duy Tong and
• Viet Van Pham

Beilstein J. Nanotechnol. 2022, 13, 1541–1550, doi:10.3762/bjnano.13.127

• ability. (i) TNAs only respond to ultraviolet (UV) light [22][23][24], and (ii) they exhibit fast carrier recombination [25]. Recently, the development of new heterojunction architectures through coupling TNAs with other semiconductor materials, especially low-bandgap semiconductors, led to a reduction of

• electrodes were a Pt counter electrode, a Ag/AgCl 3 M reference electrode, and a MoS2/TNAs or g-C3N4/TNAs working electrode in a 1 M Na2SO4 (pH 7.4) electrolyte solution. The light source used in this study was a 150 W Xe lamp (ABET Instruments) with a calibrated luminous intensity of 100 mW·cm−2 and a UV

• at 393 nm. This means that TNAs are only activated by near-UV irradiation. In contrast, the g-C3N4 sample shows an absorption edge at 464 nm. Meanwhile, MoS2 exhibits strong absorption from the UV region extending to the entire visible-light region. It can be seen that the loading of both MoS2 and g

Non-stoichiometric magnetite as catalyst for the photocatalytic degradation of phenol and 2,6-dibromo-4-methylphenol – a new approach in water treatment

• Joanna Kisała,
• Anna Tomaszewska and
• Przemysław Kolek

Beilstein J. Nanotechnol. 2022, 13, 1531–1540, doi:10.3762/bjnano.13.126

• SEM, X-ray diffraction, and ultraviolet–visible (UV–vis) analysis. The XRD and UV–vis results were published in our previous article [17]. We present this data again in this article as it is necessary for the discussion of the results. Zeta potential measurements were also presented in another

• with a Cu Kα powder diffractometer (D8 Advance, Bruker, Ettlingen, Germany) operating at 40 kV and 36 mA (λ = 0.154056 nm). The optical characterization of the catalysts was performed by using a spectrophotometer (Cary Series UV-Vis-NIR, Agilent Technologies) in the wavelength range of 190–800 nm

• up to 1h). The organic compound concentrations were evaluated by using HPLC. Analysis Changes in phenol concentration were determined by a high-performance liquid chromatography system (Shimadzu, Japan) equipped with a UV detector (SPD-10AV) and a C18 column (Knauer 250 × 4.6 mm, Eurospher II 100-5

A TiO₂@MWCNTs nanocomposite photoanode for solar-driven water splitting

• Anh Quynh Huu Le,
• Ngoc Nhu Thi Nguyen,
• Hai Duy Tran,
• Van-Huy Nguyen and
• Le-Hai Tran

Beilstein J. Nanotechnol. 2022, 13, 1520–1530, doi:10.3762/bjnano.13.125

• reactions. As a wide-bandgap (ca. 3.2 eV) semiconductor, TiO2 is a promising photocatalyst for degrading a massive range of high-molecular-weight organic pollutants under UV radiation [1]. Because of high specific surface, nanoscale TiO2 as grains or tubes can absorb UV light more substantially than

• the photocatalytic performance [4][5]. Because TiO2 only exhibits photochemical activity under UV excitation, which accounts for a small fraction (ca. 4%) of the solar energy, numerous modification methods such as doping with nonmetals, coupling with other catalysts, and attaching to supports have

• evolution of 450 µmol·h−1. Reddy et al. loaded TiO2 particles on MWCNTs via a simple hydrothermal method [13]. However, the MWNTs/TiO2 nanocomposite showed photoactivity only under UV irradiation due to the high bandgap of 3.1 eV. To the best of our knowledge, there are only a few studies on TiO2@MWCNTs

In search of cytotoxic selectivity on cancer cells with biogenically synthesized Ag/AgCl nanoparticles

• Mitzi J. Ramírez-Hernández,
• Mario Valera-Zaragoza,
• Omar Viñas-Bravo,
• Ariana A. Huerta-Heredia,
• Miguel A. Peña-Rico,
• Erick A. Juarez-Arellano,
• David Paniagua-Vega,
• Eduardo Ramírez-Vargas and
• Saúl Sánchez-Valdes

Beilstein J. Nanotechnol. 2022, 13, 1505–1519, doi:10.3762/bjnano.13.124

• pineapple peel extracts and their behavior on the breast cancer cell line MCF-7 is shown. Bioreactions were monitored at different temperatures. Fourier-transform infrared spectroscopy (FTIR), ultraviolet–visible spectroscopy (UV–vis), thermogravimetric analysis (TGA), X-ray diffraction (XRD), energy

• give rise to a collective oscillation known as surface plasmon effect [34]. This effect can be monitored by UV–vis spectroscopy, where metal nanoparticles absorb radiation at different wavelengths depending on their size [36]. The UV–vis absorption spectra of the reactions at different temperatures are

• nanoparticles as a function of temperature, the micrographs obtained by TEM in Figure 6 show different behaviors both in size and shape of the nanoparticles with respect to temperature. These results are consistent with UV–vis spectra shown in Figure 4, where each curve has a different maximum depending on the

Rapid and sensitive detection of box turtles using an electrochemical DNA biosensor based on a gold/graphene nanocomposite

• Abu Hashem,
• M. A. Motalib Hossain,
• Ab Rahman Marlinda,
• Mohammad Al Mamun,
• Khanom Simarani and
• Mohd Rafie Johan

Beilstein J. Nanotechnol. 2022, 13, 1458–1472, doi:10.3762/bjnano.13.120

• scanning electron microscopy and structural characteristics were analysed by using energy-dispersive X-ray, UV–vis, and Fourier-transform infrared spectroscopy. The electrochemical characteristics of the modified electrodes were studied by cyclic voltammetry, differential pulse voltammetry (DPV), and

• . UV–vis spectra were used to determine the presence of Gr and AuNPs/Gr in the composite. From the image (Figure 2e), Gr has a peak at 262 nm, which has been shifted to 256 nm (Figure 2e) in the composite, possibly due to interactions between AuNPs and Gr. Additionally, the distinct peak at 516 nm in

• Oxford Instrument energy dispersive X-ray spectrometer. UV–vis was performed on a Libra S80 Biochrom spectrophotometer and FTIR was performed on a Spectrum 400 PerkinElmer spectrometer (U.S.). Electrochemical studies of the electrodes The electrochemical behaviour of different modified SPCE surfaces was

Facile preparation of Au- and BODIPY-grafted lipid nanoparticles for synergized photothermal therapy

• Yuran Wang,
• Xudong Li,
• Haijun Chen and
• Yu Gao

Beilstein J. Nanotechnol. 2022, 13, 1432–1444, doi:10.3762/bjnano.13.118

• –visible (UV–vis) absorption spectra were measured with an UV–vis spectrometer (Q-5000, Quawell, America). The amounts of BDP in AB-LNPs were analyzed using UV–vis spectroscopy after the dissolution of AB-LNPs in DMSO by measuring the absorbance at a wavelength of 600 nm. The loading efficiency (LE, %) was

• taken out to measure the amount of the released drug by UV–vis spectroscopy, and an equal volume of fresh release medium was added to keep the volume constant. Photothermal measurement for AB-LNPs To study the photothermal properties of AB-LNPs, different concentrations of AB-LNPs with BDP

• in H2O. The binding of hydrophobic BDP onto Au-LNPs might affect the light absorption of Au nanoclusters. The loading efficiency of BDP in AB-LNPs determined by using UV–vis measurements (λex = 600 nm) is 51 ± 1.2% (n = 3). A TEM image of AB-LNPs is shown in Figure 1c. Particles with diameters of ca

Orally administered docetaxel-loaded chitosan-decorated cationic PLGA nanoparticles for intestinal tumors: formulation, comprehensive in vitro characterization, and release kinetics

• Sedat Ünal,
• Osman Doğan and
• Yeşim Aktaş

Beilstein J. Nanotechnol. 2022, 13, 1393–1407, doi:10.3762/bjnano.13.115

• NPs and CS/DCX-PLGA NPs through an artificial mucus layer In order to evaluate the penetration capability of NPs, wells containing artificial mucus layer were treated with DCX-loaded NP formulations. Subsequently, NPs that had penetrated the mucus layer and moved into gelatin were measured using UV

• gold and palladium and inserted on metal stubs before being dried for a 24 h SEM analysis. Determination of encapsulation efficiency, drug loading and production yield The previously reported UV–vis spectrophotometric quantification method was used to determine the DCX encapsulation efficiency of the

• of DCX was measured by UV spectrophotometry (Shimadzu UV-1800 UV–vis spectrophotometer, Shimadzu corporation, Japan) at 230 nm (λmax). Validation of the spectrophotometric method was carried out. Linearity, accuracy, precision, reproducibility, limit of detection (LOD), and limit of determination

LED-light-activated photocatalytic performance of metal-free carbon-modified hexagonal boron nitride towards degradation of methylene blue and phenol

• Nirmalendu S. Mishra and
• Pichiah Saravanan

Beilstein J. Nanotechnol. 2022, 13, 1380–1392, doi:10.3762/bjnano.13.114

• crystallographic characterization. The morphology of the obtained nanostructures was captured by high-resolution transmission electron microscopy (HRTEM, Talos F200X G2, Thermo Scientific). The optical properties were characterized with a Shimadzu UV 2600 UV–vis spectrophotometer with an integrating sphere

• photolysis of H2O2. Aliquots were drawn at regular intervals, ultracentrifuged at 7500 rpm, and then subjected to quantification of residual concentration of pollutants using a spectrophotometer (UV 2600 SHIMADZU, Japan). The intermediates formed during the photodegradation of phenol were analysed through a

• with a zeta potential of −20 mV at a neutral pH. This implies that the surface of MBN-80 is negatively charged above pH 5.08 which results in better adsorptive ability towards positively charged pollutant moieties and vice-versa. Optical studies The UV–vis light harvesting characteristics (absorbance

Supramolecular assembly of pentamidine and polymeric cyclodextrin bimetallic core–shell nanoarchitectures

• Alexandru-Milentie Hada,
• Nina Burduja,
• Marco Abbate,
• Claudio Stagno,
• Guy Caljon,
• Louis Maes,
• Nicola Micale,
• Massimiliano Cordaro,
• Angela Scala,
• Antonino Mazzaglia and
• Anna Piperno

Beilstein J. Nanotechnol. 2022, 13, 1361–1369, doi:10.3762/bjnano.13.112

• -inflammatory, and anticancer). The physicochemical characterization of the supramolecular assembly (nanoGSP) in terms of size and colloidal stability was investigated by complementary spectroscopic techniques, such as UV–vis, ζ-potential, and dynamic light scattering (DLS). Furthermore, the role of PolyCD

• , Figure 1) achieved by supramolecular assembly of the components as well as their physicochemical characterization in terms of size and colloidal stability. The drug binding ability of nanoGS with Pent has been investigated by complementary spectroscopic techniques such as UV–vis, zeta potential (ζ

• reduction of AgNO3. The formation of small gold NPs (Figure 2) was confirmed by the presence of the LSPR band detected at 531 nm in the UV–vis spectrum. The subsequent addition of AgNO3 resulted in a change of the extinction spectrum with the formation of a higher and broader absorption band at 402 nm

Near-infrared photoactive Ag-Zn-Ga-S-Se quantum dots for high-performance quantum dot-sensitized solar cells

• Roopakala Kottayi,
• Ilangovan Veerappan and
• Ramadasse Sittaramane

Beilstein J. Nanotechnol. 2022, 13, 1337–1344, doi:10.3762/bjnano.13.110

• JSM-7600F. The electronic states of the elements and their atomic ratio in the prepared samples was analyzed by using XPS (Kratos AXIS Ultra DLD) and EDX (Bruker Nano XFlash detector attached to the HRTEM). Optical properties were examined by using a UV–vis–NIR spectrophotometer (Perkin Elmer L-650 UV

• ]. The elemental Se spectrum (Figure 3f) shows the peaks of Se 3d5/2 (55.65 eV) indicating the existence of Se2− ions [27][29] .This result confirms that the synthesized QDs contain Zn2+, Ag+, Ga3+, S2− and Se2− ions forming I-II-III-VI3-type AgZnGaS1.5Se1.5 QDs. Optical studies The UV–vis absorbance

• prove the incorporation of AZGSSe QDs in the TiO2 NFs. The UV–vis absorption spectrum of the AZGSSe/TiO2-based photoanode in comparison with TiO2 NFs shown in Figure 6a. It can be observed that AZGSSe/TiO2-based photoanode has a light absorption in the NIR region. This signifies that AZGSSe/TiO2 is an

Recent trends in Bi-based nanomaterials: challenges, fabrication, enhancement techniques, and environmental applications

• Vishal Dutta,
• Ankush Chauhan,
• Ritesh Verma,
• C. Gopalkrishnan and
• Van-Huy Nguyen

Beilstein J. Nanotechnol. 2022, 13, 1316–1336, doi:10.3762/bjnano.13.109

• obtained. They found that Bi5O7Br effectively converts molecular oxygen to superoxide radicals and hydroxyl radicals in visible light. Under UV–vis irradiation, Bi5O7Br showed a higher photocatalytic activity in the degradation of rhodamine B (RhB) dye than BiOBr. The addition of Bi5O7Br photocatalysis to

• the Bi–O–X photocatalytic system improved the system. In this work, they found that the RhB elimination percentage over Bi5O7Br is 85% after 120 min of UV–visible-light irradiation, and the reaction rate constant was measured as 1.496 h−1·m−2. In contrast, the reaction rate constant for BiOBr was

• . The sample calcinated at 750 °C revealed the highest photocatalytic performance. Hamza et al. fabricated Bi2(CrO4)3 nanoparticles via a facile precipitation technique [59]. The photocatalytic activity of the Bi2(CrO4)3 nanoparticles was studied under UV, AM 1.5, and visible-light irradiation, and

Studies of probe tip materials by atomic force microscopy: a review

• Ke Xu and
• Yuzhe Liu

Beilstein J. Nanotechnol. 2022, 13, 1256–1267, doi:10.3762/bjnano.13.104

• prepared colloidal gold was identified by transmission electron microscopy and UV spectrophotometer for size and uniformity. The amount of colloidal gold-labeled HBsAg Mab protein was determined by the CVAI curve; the probe was identified by spot immunosorbent assay. The prepared 15 nm colloidal gold

• particles were homogeneous; the maximum absorption wavelength was 518 nm with narrow peak width in the UV spectrophotometer 400–700 nm scan; the purified HBsAg Mab concentration was 65 mg/mL; the optimal protein protection amount was 32.5 μg per mL of colloidal gold at pH 8.2; the quality of the probe was

Design of surface nanostructures for chirality sensing based on quartz crystal microbalance

• Yinglin Ma,
• Xiangyun Xiao and
• Qingmin Ji

Beilstein J. Nanotechnol. 2022, 13, 1201–1219, doi:10.3762/bjnano.13.100

• resonance [10], Fourier transform infrared spectrometry (FTIR) [11], UV–vis absorption spectrometry [12], mass spectrometry (MS) [13], titration microcalorimetry [14], high-performance liquid chromatography (HPLC) [15], gas chromatography (GC), capillary electrophoresis (CE) [16], and electrochemical chiral

• selector layers, which was opposite to that of 1-TNA and 1-(3-methoxyphenyl)ethylamine (3-MEPA). Combined with ultraviolet (UV) and fluorescent (FL) analysis results, these results indicated that the differences in chiral recognition are caused by diverse molecular interactions between enantiomers and SAs

• -glutamate. Combined with color changes and UV–vis spectra of the sensing solutions, the driving force for the chiral detection was mainly suggested to be due to the induced chirality of PANI film by R-CSA. Chiral recognition layer from supermolecular structures Supermolecular structures are self-assembled

Microneedle-based ocular drug delivery systems – recent advances and challenges

• Piotr Gadziński,
• Anna Froelich,
• Monika Wojtyłko,
• Antoni Białek,
• Julia Krysztofiak and
• Tomasz Osmałek

Beilstein J. Nanotechnol. 2022, 13, 1167–1184, doi:10.3762/bjnano.13.98

• plate where it quickly solidifies [151]. In the microstereolithographic method, a prepared polymer or a mixture of polymers undergoes polymerization under the influence of a high-energy light source (e.g., UV radiation) [150]. Digital light processing (DLP) is also a technology based on

• photopolymerization of photosensitive polymers, but in this case each layer of the polymer is projected as whole [152]. A more complicated method is two‑photon polymerization (TPP), which uses a near-infrared beam instead of UV radiation. TPP initiates the polymerization of the resin by multiphoton absorption [153

• ]. An alternative to methods using UV or heat is the droplet-born air blowing method (DAB). It is suitable for drug molecules that can be inactivated. In this method, polymer droplets are placed between two sheets. As the sheets are pulled apart, the droplets elongate and the resulting needle-shaped

Rapid fabrication of MgO@g-C₃N₄ heterojunctions for photocatalytic nitric oxide removal

• Minh-Thuan Pham,
• Duyen P. H. Tran,
• Xuan-Thanh Bui and
• Sheng-Jie You

Beilstein J. Nanotechnol. 2022, 13, 1141–1154, doi:10.3762/bjnano.13.96

• and also the existence of MgO in the MgO@g-C3N4 heterojunction materials. However, with a smaller bandgap, the recombination of e−–h+ pairs will be faster, which decreases the photocatalytic activity of the materials [63]. As shown in Figure 9a and Figure 9c, the materials mostly absorb in the UV

• range (200–400 nm), with a sudden decrease in the visible range. The absorbance of 3% MgO@g-C3N4 is more substantial than the absorbance of 1% MgO@g-C3N4 and 5% MgO@g-C3N4 in the UV and visible ranges. These results indicate that the higher photocatalytic NO removal efficiency of the 3% MgO@g-C3N4

• strongly depends on the optical properties. Photoluminescence Fluorescence spectra of MgO and 3% MgO@g-C3N4 are shown in Figure 10a and Figure 10b, respectively. MgO shows strong fluorescence at 270 nm with an excitation wavelength (270 nm) in the UV range. MgO also shows another emission wavelength at 380

Green synthesis of zinc oxide nanoparticles toward highly efficient photocatalysis and antibacterial application

• Vo Thi Thu Nhu,
• Nguyen Duy Dat,
• Le-Minh Tam and
• Nguyen Hoang Phuong

Beilstein J. Nanotechnol. 2022, 13, 1108–1119, doi:10.3762/bjnano.13.94

• electron microscopy, and high-resolution transmission electron microscopy. The fabricated ZnO NP samples are crystalline with a grain size of 30–100 nm. The ZnO NPs were used as catalysts for the photodegradation of methylene blue (MB) and methyl orange (MO) under visible and UV light. The results indicate

• that the prepared ZnO material excellently removed MB and MO (cinitial = 10 mg/L) with efficiencies of 100% and 82.78%, respectively, after 210 min under UV radiation with a ZnO NP dose of 2 g/L. The photocatalyst activity of the synthesized material was also tested under visible light radiation with

• photocatalysts. ZnO has a higher quantum efficiency than that of TiO2 since it absorbs more energy in the UV region [4][5][6][7]. Furthermore, ZnO is a low-cost photocatalyst with high photocatalytic activity, nontoxicity, light sensitivity, and stability [8][9][10]. The photodegradation of organic substances by

Recent advances in green carbon dots (2015–2022): synthesis, metal ion sensing, and biological applications

• Aisha Kanwal,
• Naheed Bibi,
• Sajjad Hyder,
• Arif Muhammad,
• Hao Ren,
• Jiangtao Liu and
• Zhongli Lei

Beilstein J. Nanotechnol. 2022, 13, 1068–1107, doi:10.3762/bjnano.13.93

Spindle-like MIL101(Fe) decorated with Bi₂O₃ nanoparticles for enhanced degradation of chlortetracycline under visible-light irradiation

• Chen-chen Hao,
• Fang-yan Chen,
• Kun Bian,
• Yu-bin Tang and
• Wei-long Shi

Beilstein J. Nanotechnol. 2022, 13, 1038–1050, doi:10.3762/bjnano.13.91

• cavities, and excellent thermal stability [20][21]. These advantages make it appalling to adsorption [22], gaseous capture/separation [23], sensing [24], and drug release applications [25]. Moreover, some MOFs can be excited under UV or visible light and exhibit light harvesting properties due to ligand

• photocatalyst under UV light irradiation [30]. So far, a large number of MOFs have been shown to exhibit photocatalytic activity in H2 production, organic pollutant degradation, and Cr(VI) and CO2 reduction [26][27][31][32][33]. Among MOF catalysts, MIL101(Fe) is a cage-like structure formed by self-assembly of

• centrifuged to remove photocatalysts. The concentration of CTC in the supernatant was determined by UV–vis spectrophotometry at a wavelength of 357 nm. The degradation rate can be calculated by Equation 1: where C0 and Ct represent the concentration of CTC at the initial time and time t, respectively

Design of a biomimetic, small-scale artificial leaf surface for the study of environmental interactions

• Miriam Anna Huth,
• Axel Huth,
• Lukas Schreiber and
• Kerstin Koch

Beilstein J. Nanotechnol. 2022, 13, 944–957, doi:10.3762/bjnano.13.83

• functions (Figure 1). Among other things, it protects against herbivores and pathogens, provides mechanical stability, reflects harmful UV radiation [2][3][4][5][6], and mainly protects the plant from desiccation [7][8]. The cuticular waxes contribute significantly to this barrier function. Plant waxes

• temperatures, reduced humidity, increased UV radiation, or drought stress can lead to increased wax accumulation [55][64][69][70][71]. Therefore, it was also examined whether there were differences in the wax chemistry between the greenhouse plants and the outdoor plants. The results showed hardly any

Solar-light-driven LaFe_xNi_1−xO₃ perovskite oxides for photocatalytic Fenton-like reaction to degrade organic pollutants

• Chao-Wei Huang,
• Shu-Yu Hsu,
• Jun-Han Lin,
• Yun Jhou,
• Wei-Yu Chen,
• Kun-Yi Andrew Lin,
• Yu-Tang Lin and
• Van-Huy Nguyen

Beilstein J. Nanotechnol. 2022, 13, 882–895, doi:10.3762/bjnano.13.79

• . The UV–vis absorption capability with diffuse reflectance spectroscopy (DRS) and photographs of various LaFexNi1−xO3 perovskite oxides with different proportions were shown in Figure 5a and 5b. Except for LaFeO3, which was brown, the rest of the perovskite oxides doped with Ni became black. Since

• microscopy (FESEM). The light absorption spectra of the perovskite oxides were inspected using V-670 (Jasco, Japan) to examine the UV–vis absorption capability with diffuse reflectance spectroscopy (DRS) from 200 to 800 nm. The nitrogen adsorption–desorption analyzer, ASAP 2020 PLUS (ASAP, USA), was applied

• , then filtering the samples through a 0.22 µm needle filter. The MB concentrations were evaluated using the UV–vis spectrometer U-2910 (HITACHI, Japan). The detection range was set from 200 to 800 nm. The scanning rate was 400 nm/min. The maximum absorption peaks of MB and TC solution were at 664 nm and

DNA aptamer selection and construction of an aptasensor based on graphene FETs for Zika virus NS1 protein detection

• Nathalie B. F. Almeida,
• Thiago A. S. L. Sousa,
• Viviane C. F. Santos,
• Camila M. S. Lacerda,
• Thais G. Silva,
• Rafaella F. Q. Grenfell,
• Flavio Plentz and
• Antero S. R. Andrade

Beilstein J. Nanotechnol. 2022, 13, 873–881, doi:10.3762/bjnano.13.78

• rinsed with 0.1 M HCl for 5 min, water (DNAse/RNAse free) for 1 min, then borate buffer for 5 min under 50 psi pressure before injection of the incubation mixture at 0.5 psi for 5 s. The mixture was separated under 26 kV (reverse polarity) in borate buffer at 25 °C and monitored through UV absorbance

• with ethidium bromide and imaged using a UV transluminator (UVP BioDoc-It Imaging System). The PCR asymmetric product was used to carry out counterselections with NS1 proteins of DENV (serotypes 1, 2, 3, and 4) and YFV. The protocol described by Simmons et al. with the proteins immobilized on Nunc

Self-assembly of C₆₀ on a ZnTPP/Fe(001)–p(1 × 1)O substrate: observation of a quasi-freestanding C₆₀ monolayer

• Guglielmo Albani,
• Michele Capra,
• Alessandro Lodesani,
• Alberto Calloni,
• Gianlorenzo Bussetti,
• Marco Finazzi,
• Franco Ciccacci,
• Alberto Brambilla,
• Lamberto Duò and
• Andrea Picone

Beilstein J. Nanotechnol. 2022, 13, 857–864, doi:10.3762/bjnano.13.76

• acquired at normal emission with a 150 mm hemispherical electron analyzer from SPECS GmbH. The probing depth of UPS is a few angstroms [49]. A He lamp has been employed as a source of non-monochromatized unpolarized UV photons. The He-I line, with a photon energy of 21.2 eV, has been used to excite the

Hierachical epicuticular wax coverage on leaves of Deschampsia antarctica as a possible adaptation to severe environmental conditions

• Elena V. Gorb,
• Iryna A. Kozeretska and
• Stanislav N. Gorb

Beilstein J. Nanotechnol. 2022, 13, 807–816, doi:10.3762/bjnano.13.71

• surfaces might contribute to the plant adaptation to severe environmental conditions in Antarctica due to an increase of its resistance against cold temperatures, icing, harmful UV radiation, and dehydration. The presence of the epicuticular wax on the abaxial leaf side and the ligule as well as the

• harsh environments (e.g., strong UV irradiation, low temperatures, and icing). Experimental Plant material D. antarctica plants used in this study were collected in the vicinity of Henryk Arctowski Polish Antarctic Station, King George Island, Maritime Antarctica (62°09′50″ S, 58°28′7″ W) during X

• equipped for the successful scattering of strong radiation. Experimental studies with altered levels of UV-B radiation and D. antarctica showed no significant effect of enhanced or reduced radiation on the relative growth rate and leaf photosynthesis of the plants [40]. Moisture, being one of the most